• Title/Summary/Keyword: Cu Powder

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A Study of Debinding Behavior and Microstructural Development of Sintered Al-Cu-Sn Alloy

  • Kim, J.S.;Chang, I.T.;Falticeanu, C.L.;Davies, G.J.;Jiang, K.C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.722-723
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    • 2006
  • A new method has been developed to fabricate microcomponents by a combination of photolithography and sintering of metallic powder mixtures, without the need for compression and the addition of Mg. This involves (1) the fabrication of a micromould, (2) mould filling of the powder/binder mixture, (3) debinding and (3) sintering. The starting powdered materials consisted of a mixture of aluminium powder(average size of 2.5 um) and alloying elemental powder of Cu and Sn(less than 70nm), at appropriate proportions to achieve nominal compositions of Al-6wt%Cu, Al-6wt%Cu-3wt%Sn. This paper presents detailed investigation of debinding behaviour and microstructural development.

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Hydrogen Reduction Behavior of Al2O3/CuO Powder Mixtures Prepared from Different Raw Powders and Their Microstructural Characteristics (원료분말에 따른 Al2O3/CuO 분말혼합체의 수소환원 거동 및 미세조직 특성)

  • Oh Sung-Tag;Kim Jung-Nam;Kang Kae-Myung
    • Korean Journal of Materials Research
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    • v.14 no.10
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    • pp.696-700
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    • 2004
  • The reduction behavior of $Al_{2}O_3/CuO$ powder mixtures, prepared from $Al_{2}O_3/CuO$ or $Al_{2}O_3/Cu-nitrate$, was investigated by using thermogravimetry and hygrometry. The powder characteristics were examined by BET, XRD and TEM. Also, the influence of powder characteristics on the microstructure and properties of hot-pressed composites was analyzed. The formation mechanism of nano-sized Cu dispersions was explained based on the powder characteristics and reduction kinetics of oxide powders. In addition, the dependence of the microstructure and mechanical properties of hot-pressed composites on powder characteristics is discussed in terms of the initial size and distribution of Cu particles. The practical implication of these results is that an optimum processing condition for the design of homogeneous microstructure and required properties can be established.

Fabrication of Gradient Porous Al-Cu Sintered Body (경사 다공성 Al-Cu 소결체의 제조)

  • Byun, Jong-Min;Kim, Se-Hoon;Kim, Jin-Woo;Kim, Young-Moon;Kim, Young-Do
    • Journal of Powder Materials
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    • v.18 no.4
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    • pp.365-371
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    • 2011
  • In this study, gradient porous Al-Cu sintered body was fabricated by powder metallurgy processing. Al-Cu powder mixtures were prepared by low energy ball milling with various milling time. After ball milling for 3h, the shape of powder mixtures changed to spherical type with size of 100~500 ${\mu}m$. Subsequently, Al-Cu powder mixtures were classified (under 150, 150~300 and over 300 ${\mu}m$) and compacted (20, 50 and 100 MPa). Then, they were sintered at $600^{\circ}C$ for various holding time (10, 30, 60 and 120 min) in $N_2$ atmosphere. The sintered bodies had 32~45% of porosity. As a result, the optimum holding time was determined to be 60 min at $600^{\circ}C$ and sintered bodies with various porosity were obtained by controlling the compacting pressure.

A study on the Manufacture of the CuO Powder from Copper Chloride Solution by Spray Pyrolysis Process (분무열분해법에 의한 구리염화물 용액으로부터 CuO 분말 제조에 관한 연구)

  • Yu, Jae-Geun;Park, Hui-Beom
    • Korean Journal of Materials Research
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    • v.12 no.1
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    • pp.58-67
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    • 2002
  • In this study copper chloride(CuCl$_2$) solution was used as raw material to produce the fine copper oxide powder which has less than 1 $\mu\textrm{m}$ average particle size and has uniform particle size distribution by spray pyrolysis process. In the present study, the effects of reaction temperature, the injection speed of solution and air, the nozzle tip size and the concentration of raw material solution on the properties of produced powder were studied. The structure of the powder became much more compact with increasing the reaction temperature regardless of copper concentration of the raw material solution. The particle size of the powder increased accordingly with increasing the reaction temperature in case of 30 g/$\ell$ copper concentration of the solution. The particle size of the powder increased accordingly, and the surface structure of the powder became more porous with increasing the copper concentration of the raw material solution. When copper concentration in raw material solution was more than 100 g/$\ell$, all produced powder was CuCl regardless of reaction temperatures. When copper concentration in solution was below 30 g/$\ell$ and reaction temperature was higher than 90$0^{\circ}C$, CuO was the main phase. The surface of the powder tended to become porous with increasing the injection speed of solution. Particle size was increased and the surface of the powder showed severely disrupted state with increasing the nozzle tip size. The particle size was decreased and the particle size distribution was more uniform with increasing the air pressure through the nozzle.