• 제목/요약/키워드: Crystal Size

검색결과 1,494건 처리시간 0.029초

Effects of Crystal Grain Size and Particle Size on Core Loss For Fe-Si Compressed Cores

  • Takemoto, Satoshi;Saito, Takanobu
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1183-1184
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    • 2006
  • Core loss of soft magnetic powder cores have been focused on to achieve high efficiency of power supplies. In this study the effects of crystal grain size on core loss were investigated by changing heat treatment conditions. It was found that core loss is influenced by crystal grain size because eddy current loss decreased and hysteresis loss increased by making crystal grain size smaller, and it is also influenced by particle size.

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연속식결정화기 정상상태에서 탄산칼슘 결정크기 변화 (Change of Calcium Carbonate Crystal Size at steady state in CMSMPR(Continuous Mixed Suspension Mixed Produce Removal) Crystallizer)

  • 한현각
    • 한국산학기술학회논문지
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    • 제18권7호
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    • pp.714-719
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    • 2017
  • 입자의 크기와 형상을 제어할 수 있는 무기물질의 제한된 제조방법은 나노입자와, 의료, 전자부품, 반도체, 의약품, 화장품 등과 같은 다양한 산업영역에서 신물질을 개발하는데 중요한 요소이다. 탄산칼슘은 수많은 활용성 때문에 산업에서 가장 많이 주목받고 있는 물질중 하나이다. 용액결정화는 용액으로부터 녹아 있는 용질을 순수한 고체 형태로 추출하는 분리 공정으로, 화학공업과 제약공업 등에 널리 적용되어, 사용되고 있는 분리공정 중에 하나이다. 입자의 평균입경과 입도분포, 형상은 연속식 결정화기에서 중요한 요소이다. 본 연구에서는 연속식 결정화기에서 염화칼슘 공정으로 탄산칼슘 입자를 제조할 때, 정상상태에서 탄산칼슘 입자의 입도분포와 입경변화에 대하여 연구하였다. 입자의 평균입경과 입도분포는 입도분석기를 이용하여 측정하였으며, 입자의 형상과 크기는 전자현미경(SEM)을 이용하여 변화를 관찰하였다. 정상상태에서, 주입되는 시료의 농도와 혼합속도가 증가 할수록 입자의 평균입경은 증가하고, 제조되는 입자는 aragonite 보다는 calcite 입자가 주로 생성된다.

황산티타늄의 첨가가 판상 α-Al2O3의 결정성장에 미치는 영향 (Effect of Titanium Sulfate Addition on Crystal Growth of the Flaky α-Al2O3)

  • 박병기;조선미;이정민
    • 한국세라믹학회지
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    • 제42권5호
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    • pp.338-345
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    • 2005
  • To prepare the complex gel of flux and pseudo-boehmite used in precursor of the flaky ${\alpha}-A1_2O_3$ crystal, aqueous solution of the mixture of sodium carbonate and sodium phosphate was added with stirring in aqueous solution of the mixture of sodium sulfate, potassium sulfate and titanium sulfate. The complex gel was dried at $110^{\circ}C$ and was crystallized above $1,050^{\circ}C$, and then the effect of the amount of titanium sulfate on size, morphology, thickness and crystal size distribution of the flaky ${\alpha}-A1_2O_3$ crystal was investigated. Addition of titanium sulfate was prevented the aggregation and generation of twin crystal, and had an effect on the crystal size and the thickness during crystal growth. When the amount of titanium sulfate was more than 6 g, particle size was decreased but was free from crystal twining and aggregation. On the other hand, when the amount of titanium sulfate was lower than 6 g, crystal size was increased but crystal twinning and aggregation were noticed.

분자동역학을 이용한 나노구조물의 크기와 결정방향에 따른 응력-변형률 관계 해석 (Analysis of Stress-Strain Relationship of Nano Structures According to the Size and Crystal Orientation by Using the Molecular Dynamics Simulation)

  • 강용수;김현규
    • 대한기계학회논문집A
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    • 제32권12호
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    • pp.1047-1054
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    • 2008
  • In this paper, the molecular dynamics (MD) simulations are performed with single-crystal copper blocks under simple shear and simple tension to investigate the effect of size and crystal orientation. There are many variances to give influences such as deformation path, temperature, specimen size and crystal orientation. Among them, the crystal orientation has a primary influence on the volume averaged stress. The numerical results show that the volume averaged shear stress decreases as the specimen size increases and as the crystal orientation changes from single to octal. Furthermore, the Schmid factor and yield stress for crystal orientation are evaluated by using the MD simulation on the standard triangle of stereographic projection.

Crystallization of High Purity Ammonium Meta-Tungstate for production of Ultrapure Tungsten Metal

  • Choi, Cheong-Song
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1997년도 Proceedings of the 13th KACG Technical Meeting `97 Industrial Crystallization Symposium(ICS)-Doosan Resort, Chunchon, October 30-31, 1997
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    • pp.1-5
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    • 1997
  • The growth mechanism of AMT(Ammonium Meta-Tungstate) crystal was interpreted as two-step model. The contribution of the diffusion step increased with the increase of temperature, crystal size, and supersaturation. The crystal size distribution from a batch cooling crystallizer was predicted by the numerical solution of a mathematical model which uses the kinetics of nucleation and crystal growth. Temperature control of a batch crystallizer was studied using Learning control algorithm. The purity of AMT crystal producted in this investigation was above 99.99%.

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폴리머 분산 액정의 전기 광학적 스위칭 특성에 대한 액정방울 크기의 효과 (Effect of droplet size on electro-optical switching properties of polymer dispersed liquid crystals)

  • 김인태;유연석
    • 한국광학회지
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    • 제17권1호
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    • pp.23-30
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    • 2006
  • 폴리머 분산 액정의 전기광학 스위칭 특성에 대한 액정 방울 크기의 효과를 실험적으로 연구하였다. 액정 방울의 크기는 상 분리를 위해 조사하는 레이저 광원의 세기와 LC/oligomer의 혼합 비율에 따라 변화되었다. 전기 광학적 스위칭 전압은 LC/oligomer의 혼합비율과 액정의 방울 크기에 크게 의존하였다. 실험 결과를 보면 상 분리용 조사 레이저광의 세기가 클 때 액정방울의 크기는 작아졌고 포화투과도 전압은 상승했지만 rise time은 짧아 졌다.

Size Effect of Light Scattering on the Nano-Sized Color Filter Pigment in Liquid Crystal Display

  • Jhun, Chul Gyu;Gwag, Jin Seog
    • Journal of the Optical Society of Korea
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    • 제18권2호
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    • pp.184-187
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    • 2014
  • This study examined the effects of particle size on the light scattering of a nano-sized color filter pigment used to obtain a range of colors in liquid crystal displays. The contrast ratio is one of the most important characteristics of liquid crystal displays. When a color filter is located between two crossed polarizers, the size of the pigment can give rise to a decrease in the contrast ratio due to Rayleigh scattering by the nanoparticles in the filter. The size effect of the color filter pigment on the contrast ratio was investigated in terms of the depolarization parameter. As an experimental result, the depolarization parameter increased with decreasing pigment size. Therefore, a smaller pigment size can reduce light leakage caused by light scattering in the color filter between two crossed polarizers. The depolarization function was also proposed as a useful function for predicting the decrease in the contrast ratio of the color filter.

란타늄 옥살레이트 반응성 결정화에서 반응조건에 따른 결정입자 연구 (Effect of Reaction Conditions on Crystals in the Reaction Crystallization of Lanthanum Oxalate)

  • 김홍주;김운수;김우식
    • 공업화학
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    • 제9권7호
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    • pp.1004-1010
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    • 1998
  • Single-jet 반회분식 결정화 반응기에서 동력투입량, 반응물의 주입시간 및 주입방법등 반응조건의 변화가 란타늄 옥살레이트 결정입자의 반응성 결정화에 미치는 영향에 대해 실험적으로 조사하였다. 란타늄 옥살레이트 결정입자의 크기분포는 반응조건에 관계없이 monomodal 형태의 크기분포를 나타내었으나 평균결정크기는 반응조건에 크게 영향을 받았다. 동력투입량이 증가할수록, 반응물의 주입속도가 빠를수록, 란타늄 옥살레이트의 결정입자크기는 감소하였으나 상대적 유도시간은 증가하였다. 반응물의 주입방법에 있어서 옥살산 용액이 주입되는 경우보다 염화란타늄 용액이 주입되는 경우에 결정입자는 크게 나타났으며 상대적 유도시간은 감소하였다. 그리고 결정입자의 형태는 모두 침상형으로 반응조건의 변화에 크게 영향을 받지 않았다.

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Particle Size, Morphology and Color Characteristics of C.I. Pigment Red 57:1 : 2. Effect of Salt Milling Process

  • Seo, Hee Sung;Lee, Hyun Kyung;Yoo, Eui Sang
    • 한국염색가공학회지
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    • 제27권4호
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    • pp.245-260
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    • 2015
  • The effect of salt milling process on the crystal size, morphology, and color characteristics of C.I. Pigment Red 57:1 was studied. The primitive morphology and color properties of the pigment after synthesis were studied in the former series work. The size and morphology of primary particles and the second aggregation features should be considered because they are very important to determine pigment quality. We compared the primary morphology of pigment particles before drying with the secondary aggregated morphology of pigment particles after drying and salt milling process. Morphological properties were investigated by particle size analysis, X-ray diffraction, and scanning electron microscopy and color measurement was carried out. Significant reduction in particle size as well as enhanced crystallite size after salt milling process was observed. This result might give a difference in color of the pigment, turning into brighter and more blue-toned red color. It was revealed that synthesis condition affect the morphology and color of the pigment even after milling. Increase in HCl concentration in the synthesis process enhanced crystal size and quality forming bluer-red pigments but an increase in $CaCl_2$ concentration resulted in more amorphous crystals forming darker-red pigments after salt milling.

Ge-Se-Te계 Chalcogenide 유리의 결정화 및 결정화가 물성에 미치는 영향 (Controlled Crystallization and its Effects on Some Properties of Ge-Se-Te Chalcogenide Glass)

  • 송순모;최세영;이용근
    • 한국세라믹학회지
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    • 제33권8호
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    • pp.855-862
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    • 1996
  • The nucleation and the crystal growth rates of Ge-Se-Te chalcogenide glass by two step heat-treatment and its effect on the mechanical optical properties and water-resistance were determined. The maximum nuclea-tion and crystal growth rate were 2.1$\times$103/mm3 .min at 28$0^{\circ}C$ and 0.4${\mu}{\textrm}{m}$/min at 33$0^{\circ}C$ respectively. When the crystal volume fraction with crystal size $1.5mutextrm{m}$ was about 4% the (hardness and fracture toughness were about 117kg/mm2 and 6.0 MPa.mm1/2)respectively. The weight loss of crystallized glass in water was lower than parent glass($25^{\circ}C$ for 32 hrs : 0.03% 8$0^{\circ}C$ for 16 hrs : 0.1%) as 0.01% at $25^{\circ}C$, 0.03% at 8$0^{\circ}C$ for 16 hrs : 0.1%) at $25^{\circ}C$ 0.03% at 8$0^{\circ}C$ respectively. The IR-transmittance decreased with increasing crystal size and crystal volume fraction. The IR-transmittance of crystallized glass with the crystal size of $1.5mutextrm{m}$ (crystal volume fraction : 4%) presented 56% which was about 4% lower than that of parent glass.

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