• Transactions of the Korean Society of Mechanical Engineers
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• v.12 no.5
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• pp.1083-1091
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• 1988

Vacuum brazing is the most modern brazing process and is at present, far from being completely understood. By brazing under high vacuum, in an atmosphere free of oxidizing gases, a superior product with greater strength, ductility and uniformity can be obtained. In this study, the influence of brazing parameters such as base metal characteristics, joint clearance and brazing time were described in relation to the metallurgical phenomena and shear strength of vacuum-brazed joints between carbon steels and 304 stainless steel (SUS 304) brazed by copper filler metal. In copper brazing of SUS 304 to a medium carbon steel(M.C.S) the columnar Fe-Cr-Ni-Cu-C alloy structure was formed and grew from the M.C.S side and at the same time, the surface of M.C.S. was decarbonized. The driving force for the formation and growth of columnar structure was the difference of carbon content between base metals. As the joint clearance is narrower and brazing time is longer, the formation and growth of columnar phase and decarburization of carbon steels were more noticeable. Because of decarburization of carbon steels, the shear strength of brazed joints were reduced as the formation of columnar structure was increased.

• Economic and Environmental Geology
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• v.47 no.4
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• pp.351-362
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• 2014

In order to grasp the geological characteristics, the occurrence mode of ore body and development potential of Bophi Vum chromite mineralized zone in northwestern Myanmar, Korea Institute of Geoscience and Mineral Resources(KIGAM) and Department of Geological Survey and Mineral Exploration(DGSE) carried out joint exploration targeting on the $6km^2$ areas within the mineralized zone. Chromitites occur as a major Cr-ore body in the Bophi Vum area, and are enveloped by dunitic peridotites. As a result of geological survey, the geological map of Bophi Vum was drawn in the scale of 1:1,000, and we discovered that the chromitite ores are mainly distributed at the elevation range between 200 and 400 m. The soil geochemistry was conducted by collecting total 114 soil samples in the interval of 50 m after pitting ground surface under 0.7-1 m. Geochemical anomaly maps of Cr, Ni, Fe, and Mn were prepared by ICP-AES.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.35 no.3
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• pp.297-302
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• 2022

We investigated the origin of magnetic behaviors induced by an asymmetric spin exchange interaction in Fe-site engineered lead iron niobate [Pb(Fe_1/2Nb_1/2)O₃, PFN], which exhibits a room-temperature multiferroicity. The magnitude of spin exchange interaction was regulated by the introduced transition metals with a distinct Bohr magneton, i.e., Cr, Co, and Ni. All compositions were found to have a single-phase perovskite structure keeping their ferroelectric order except for Cr introduction. We discovered that the incorporation of each transition metal imposes a distinct magnetic behavior on the lead iron niobate system; antiferro-, hard ferro-, and soft ferromagnetism for Cr, Co, and Ni, respectively. This indicates that orbital occupancy and interatomic distance play key roles in the determination of magnetic behavior rather than the magnitude of the individual Bohr magneton. Further investigations are planned, such as X-ray absorption spectroscopy, to clarify the origin of magnetic properties in this system.

• Korean Journal of Environmental Agriculture
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• v.31 no.2
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• pp.122-128
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• 2012

BACKGROUND: Mine drainage from metal mining districts is a well-recognized source of environmental contamination. Oxidation of metal sulfides in mines, mine dumps and tailing impoundments produces acidic, metal-rich waters that can contaminate the local surface water and soil. METHODS AND RESULTS: This experiment was carried out to investigate the pollution assessment of heavy metal on the water quality of mine drainage, paddy soils and sediment in lower watershed affected by mine drainage of the Sambo mine. The average concentrations of dissolved Cd (0.018~0.035 mg/L) in mine drainage discharged from the main waste rock dumps(WRD) was higher than the water quality standards (0.01 mg/L) for agricultural water in Korea. Also, the average concentrations of dissolved Zn, Fe and Mn were higher than those of recommended maximum concentrations (Zn 2.0, Fe 5.0, Mn 0.2 mg/L) of trace metal in irrigation water proposed by FAO (1994). The average contents of Pb and Zn in paddy soils was higher than those of standard level for soil contamination(Pb 200, Zn 300 mg/kg) in agricultural soil by Soil Environmental Conservation Act in Korea. Also, the concentrations of Cd, Pb and Zn in sediment were higher than those of standard level for soil contamination (Cd 10, Pb 400, Zn 600 mg/L) in waterway soil by Soil Environmental Conservation Act in Korea. The enrichment factor (EFc) of heavy metals in stream sediments were in the order as Cd>Pb>Zn> As>Cu>Cr>Ni. Also, the geoaccumulation index (Igeo) of heavy metals in stream sediments were in the order as Zn>Cd>Pb>Cu>As>Cr>Ni, specially, the geoaccumulation index (Igeo) of Zn (Igeo 3.1~6.2) were relatively higher than that of other metals in sediment. CONCLUSION(s): The results indicate that stream water and sediment were affected by mine drainage discharged from the Sambo mine at least to a distance of 1 km downstream (SN-1, SN-2) of the mine water discharge point.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2018.06a
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• pp.110-110
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• 2018

여러 니켈합금 중 인코넬 600은 원전 가압경수로(PWR)의 튜브 재료로 널리 사용되는 재료이다. 스테인리스강과 비교하여 우수한 내식성과 기계적 특성으로 인해 화학설비, 발전설비, 그리고 해양설비 등과 같은 여러 산업분야에서도 널리 사용되고 있다. 그러나 가압경수로용 증기 발생기의 튜브 재료와 같은 특수 환경에서 예민화에 따른 입계부식 및 입계응력부식 등의 문제가 흔히 보고되고 있다. 이러한 내구성 문제는 설비 및 장비의 수명, 내구성 그리고 안정성 등의 치명적인 영향을 미친다. 따라서 용접, 열처리, 그리고 가공과정에서 발생하는 Inconel 600의 예민화 및 입계부식에 관한 연구가 활발히 진행되고 있다. 그러나 100시간 이상 장시간 열화된 시편에 대한 예민화 연구는 전무한 실정이다. 본 연구에서는 장시간 열화된 Inconel 600의 예민화를 평가하기 위해 최대 1,000시간까지 열화를 실시하였으며, 이에 대한 평가방법으로 Double-Loop Electrochemical Potentiokinetic Reactivation(DL-EPR) 시험법을 적용하였다. 본 실험에서 사용된 인코넬 600의 화학성분(wt, %)은 0.01 C, 0.05 Si, 0.14 Mn, 15.3 Cr, 0.5 Cu, 0.015 S, 그리고 나머지는 Ni 이다. 예민화 평가를 위한 등온 열화는 전기열처리로를 이용하여, $550^{\circ}C$와 $650^{\circ}C$에서 최대 1000시간까지 실시하였다. 열화에 따른 미세조직 변화는 scanning electron microscope와 energy dispersive x-ray spectroscopy를 이용하여 실시하였다. DL-EPR 실험은 $25^{\circ}C$의 0.1M $H_2SO_4$ + 0.001M KSCN(potasium thiocyanate) 수용액 하에서 실시하였으며, 분극은 OCP로부터 600 mV(SSE vs.)까지 1.67mV/s 주사속도로 forward scan을 실시 후, 동일한 속도로 OCP까지 reverse scan을 실시하였다. Degree Of Sensitization(DOS)값은 anodic scan peak($I_a$) 값과 reverse scan peak($I_r$) 값의 비로 산출하였다. $$i.e.\;DOS=I_r/I_a{\times}100$$. 그 결과, 온도 변수에 따른 Inconel 600강의 예민화 거동은 서로 상이한 경향을 나타내었다. $550^{\circ}C$의 경우, 열화가 진행됨에 따라 DOS값은 급격하게 증가하는 경향을 나타냈다. 반면, $650^{\circ}C$에서는 일정시간 이후부터 Cr 확산 현상에 의한 탈 예민화 현상이 관찰되었다.

• Journal of Technologic Dentistry
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• v.14 no.1
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• pp.55-65
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• 1992

The purpose of this study was to investigate the comparison of physical properties of nonprecious metal alloys colored goldish yellow. The experimental groups were copper based dental alloy and control group was Ni-Cr based dental alloy used crown and bridges frameworks. Hardness was tested by vickers hardness tester, tensile strength was tested by universal tension tester. After testing the tensile strength of castings, the microstrucure and the pattern of fracture were investigated by scanning electron microscope and metallurgical microscope. The results were as follows : Hardness of Ni based alloy was higher than Cu based alloys. Hardness number of A group was 200.41$\pm$16.10 Hv, B group was 194.33$\pm$1.69 Hv, C group was 139.29$\pm$2.19 Hv and D group was 293.81$\pm$27.17 Hv, respectively. Tensile strength of D group was 56.42$\pm$6.17 $kg/m^2$, A group was 50.39$\pm$5.68 $kg/m^2$, C group was 45.13$\pm$4.53 $kg/m^2$, B group was 45.25$\pm$9.25 $kg/m^2$, in order, and D group was maximum tensile strength. The fractured surfaces of tensile specimens in the all groups showed the tendency to form large voids in the center of specimens. Thus the ductile fracture was changed into the brittle fracture with the fine grain size.

• Journal of Welding and Joining
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• v.13 no.2
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• pp.139-149
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• 1995

Many pressure vessels for the power plants are fabricated from low alloy ferritic steels. The inner sides of the pressure vessels are commonly weld_cladded with austenitic stainless steels to minimize problems of corrosive attack. The submerged-arc welding(SAW) process is now used in preference to other processes because of the possibilities open to automation to reduce the overaII welding times. The most reliable way to avoid underclad cracks(UCC) which are often detected at the overlap of the clad beads is to use nonsusceptible steels such as SA508 class 3. At present domestically developed forging steel of SA508 cl.S is now being cladded with single layer by using 90mm wide strip, which transfers higher heat input into the base metal compared to the conventional two layers strip cladding which has been in wide use with 30-60 mm wide strip. But the current indices for the influence of heat input on crack susceptibility are not accurate enough to express the subtle difference in crack susceptibility of the steel. Therefore, the purpose of this present study is: l) To determine UCC susceptibility on domestic forging steel, SA508 cl.S cladded with single layer by using submerged arc 90mm strip and, 2) To optimize heat input range by which the crack susceptibility could be eliminated.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.16 no.12 s.117
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• pp.1272-1278
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• 2006

This paper presents a novel MEMS condenser microphone with rigid backplate to enhance acoustic characteristics. The MEMS condenser microphone consists of membrane and backplate chips which are bonded together by gold-tin(Au/Sn) eutectic solder bonding. The membrane chip has $2.5mm{\times}2.5mm$, 0.5${\mu}m$ thick low stress silicon nitride membrane, $2mm{\times}2mm$ Au/Ni/Cr membrane electrode, and 3${\mu}m$ thick Au/Sn layer. The backplate chip has $2mm{\times}2mm$, 150${\mu}m$ thick single crystal silicon rigid backplate, $1.8mm{\times}1.8mm$ backplate electrode, and air gap, which is fabricated by bulk micromachining and silicon deep reactive ion etching. Slots and $50{\sim}60{\mu}m$ radius circular acoustic holes to reduce air damping are also formed in the backplate chip. The fabricated microphone sensitivity is 39.8 ${\mu}V/Pa$(-88 dB re. 1 V/Pa) at 1 kHz and 28 V polarization voltage. The microphone shows flat frequency response within 1 dB between 20 Hz and 5 kHz.

• Journal of Welding and Joining
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• v.10 no.1
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• pp.12-19
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• 1992

용접능률의 향상을 위한 대입열용접법의 적용은 과도한 입열량으로 인하여 용접부의 인성이 저 하한다는 점에서 그 적용에 주의를 요한다. 본 보에서는 대입열용접시 열영향부의 인성 저하의 원인과 그 대책을 강재의 측면에서 검토하였다. 고장력강을 용접하면 입열량이 증가함에 따라 오스테나이트 결정립이 조대화되고 상부 베이나이트와 도상 마르텐사이트가 생성되어 인성이 저하한다. 그 대책으로서는 용접 열싸이클과정중 안정한 질화물, 산화물등을 모재에 미세분산시켜 오스테나이트 결정립 성장을 억제하고, 페라이트, 펄라이트 변태를 촉진시킨다. 이러한 석출물의 형성을 위해서는 주로 Ti, Ca, REM, B등의 합금원소가 이용된다. 소입성이 높은 주질고장력 강에서는 석출물의 분산에 의한 페라이트의 변태 촉진 보다는 Mn, Ni, Cr, Mo, V등의 합금원 소를 첨가하여 소입성을 높여 인성이 우수한 하부 베이나이트 조직을 형성하든가, 탄소량을 저 감시켜 도상 마르텐사이트의 생성을 억제하므로서 인성을 확보한다. 현재 국내에서 제조되고 있는 대입열용접용강중 인장강도 50kgf/mm$^{2}$급강은 기본적으로 용접부 인성이 우수한 TMCP법으로 제조되며, Ti등을 첨가하여 석출물의 효과를 이용하고 N을 억제하여 기지의 인 성을 향상시키는 등의 방법을 병용하고 있다. 인장강도 60kgf/mm$^{2}$ 급강은 조질처리에 의하여 제조되며, 50kgf/mm$^{2}$급강과 같이 Ti, B등의 첨가에 의한 석출물의 효과를 이용 하고 있다.

• Applied Microscopy
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• v.7 no.1
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• pp.45-49
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• 1977

For obtaining high manganese steel plates, the study has been made on the optimum conditions in melting, forging, rolling and water toughning treatment practices. The optimum water toughning temperature and time was found to be $1030^{\circ}C$ and 30 min. respectively for the plates of 1 mm thickness. The argon atmosphere is very effective for the prevention of decarburization which can be easily occured in open air. There is a close relation between the degree of c 이 d working and the hardess. The greater the cold reduction ratio is, the smaller the grain size is and it results in the increase of hardness. The improvement of tensile and bending properties can be made by the addition of small amount of nickel, chromium and vanadium.