• 한국구조물진단유지관리공학회 논문집
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• 제25권3호
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• pp.100-109
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• 2021

본 연구에서는 부식에 의하여 발생하는 표면 단면손상을 고려하여 인위적인 표면 단면손상이 도입된 원형인장 부재의 인장성능 변화를 평가하였다. 인장성능 평가를 위하여 부식수준에 따른 인위적인 단면손상을 손상 폭과 높이를 변화시켜 원형강관 시험체 표면에 도입하였으며, 단면손상 수준에 따른 인장성능 변화를 평가하였다. 인장강도 실험 결과, 원형단면 강관부재의 인장강도는 강관부재의 길이 방향 손상이 아닌 부재 둘레 방향 손상의 영향을 받는 것으로 나타났으며, 부재의 파괴는 손상이 발생한 부재의 최소 단면에서 발생하는 것으로 나타났다. 표면에 불규칙한 손상이 도입된 강관 시험체의 단면조건을 명확하게 평가할 수 없으므로, 단면손상으로 인한 인장강도 변화를 정량적으로 비교하기 위하여 동일 단면 감소효과가 고려된 강관 부재에 대한 비선형 구조해석을 실시하였다. 비선형 구조해석 결과, 실제 부재 표면에 국부적 단면손상이 발생한 부재의 인장강도는 동일 단면 감소효과를 고려한 부재의 인장강도에 비하여 상대적으로 급격하게 저하하는 것으로 평가되었다. 국부부식과 같이 표면에 불규칙한 단면손상이 발생한 부재의 잔존인장성능은 인장시험과 등가손상 단면과 구조해석 결과로부터 평가된 상관계수를 이용하여 평가 및 예측될 수 있을 것이다.

• 한국기계가공학회지
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• 제21권5호
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• pp.46-52
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• 2022

Although pipe performs various functions in industrial sites and residential spaces, if it is damaged due to corrosion caused by the external environment, it may cause equipment failure or a major accident. For this reason, various studies for safety management are being conducted, but studies on detecting corrosion or cracks on the pipe surface using a laser displacement sensor have hardly been conducted. Therefore, in this study, the corrosion degree of the pipe surface was compared and classified into 4 corrosion conditions, and inspection equipment using a laser scanner was manufactured. The corrosion height was calculated from the four surface data obtained from the measuring equipment and applied to various CNN algorithms, and 91% accuracy was obtained during training using the Modified VGGNet16 code with reduced number of parameters.

• Restorative Dentistry and Endodontics
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• 제13권2호
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• pp.221-235
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• 1988

The purpose of this study was to observe characteristic properties through the polarization curves and EMPA images from 4 different types of amalgam obtained by using the potentiostats (EG & G PARC) & EPMA (Jeol JSM-35), to investigate the degree of corrosion of each phase of amalgam on the oxidation peak, and to identify corrosion products from the corroded amalgam by use of X-ray diffractometer(Rigaku). After each amlgam alloy and Hg were triturated as the direction of the manufacturer by means of the mechanical amalgamator(Shofu), the triturated mass was inserted into the cylindrical metal mold which was 12mm in diameter and 10mm in height and was condensed by means of routine manner. The specimen was removed from the mold and stored at room temperature for about 7 days. The standard surface preparation was routinely carried out. Anodic polarization measurement was employed to compare the corrosion behaviours of the amalgams in 0.9% saline solution(pH6.8~7.0) and artificial saliva (pH6.8~7.0) at $37^{\circ}C$. The open circuit potential was determined after 30 minutes' immersion of specimen in electrolyte and the potential scan was begun at the potential of 100mV cathodic from the corrosion potential. The scan rate was 1mV/sec and the surface area of amalgam exposed to the solution was 0.64$cm^2$ for each specimen. All the potentials reported are with respect to a saturated calomel electrode (SCE). EPMA images on the determined oxidation peaks of each amalgam in artificial saliva were observed. X-ray diffraction patterns of each sample were recorded before and after polarization in artificial saliva (Aristaloy, Caulk Spherical, Dispersalloy and Tytin: at +770mV, +585mV, +8.10m V and +680m V respectively) by use of a recording diffractometer. Nickel filtered Cu $K_{{\alpha}_1}$ radiation was used and sample was scanned at $4^{\circ}(2{\theta})/min.$ from $25^{\circ}$ to $80^{\circ}$. The following results were obtained. 1. Oxidation peak potential in artificial saliva shifted to more anodic direction than that in saline solution. 2. The corrosion potential of high copper amalgam was more anodic than the potential of low copper amalgam. 3. The current density was lower in artificial saliva than in saline solution. 4. One of the corrosion products, AgCl was identified by X-ray diffraction analysis. 5. ${\gamma}_2$ phase was the most susceptible to corrosion and e phase was stable in low copper amalgam and ${\eta}$' phase and Ag-Cu eutectic were susceptible to corrosion in high copper amalgam.

• Restorative Dentistry and Endodontics
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• 제12권1호
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• pp.39-49
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• 1986

The purpose of this study was to observe characteristic properties through the polarization curves and SEM images from 4 different types of amalgam obtained by using the potentiostats (Princeton EG & G) & SEM (Jeol/35), and to investigate the degree of corrosion on the oxidation peak of the each phase of amalgam. After each amalgam alloy and Hg was triturated as the direction of the manufacturer by means of the mechanical amalgamator (Shofu Co.), the triturated mass was inserted into the cylindrical metal mold which was 12mm in diameter and 10.0mm in height and was condensed by using routine manner. The specimen was removed from the mold and stored at room temperature for about 24 hours. The standard surface preparation was routinely carried out. Anodic polarization measurement was employed to confirm the corrosion behaviour of the amalgams in a 0.9% saline solution (P.H: 6.8-7.0) at $37^{\circ}C$. The initial rest potential (corrosion potential) was determined after 30 minutes of immersion of specimen in electrolyte, and the potential scan was begun at the point of 100mV cathodic from the corrosion potential. The scan rate was 0.17mV/sec. in the study to observe the degree of corrosion of each phase. SEI and EPMA images on the determined oxidation peaks of each amalgam were observed. The results were as follows: 1. In the four anodic polarization curves, low copper amalgams have three oxidation peaks and high copper amalgams have two oxidation peaks, -270mV, +26mV and +179mV(SEC) in the low copper lathe cut, and -300mV, +39mV and +163mV(SEC) in the low copper spherical. -4mV and +154mV(SEC) in the Dispersalloy, and +17mV and +180mV(SEC) in the Tytin as high copper amalgams. 2. ${\gamma}_2$ phase in the low copper amalgam and ${\eta}$ phase in the high copper amalgam were the most corrodible phases and Ag-Cu eutectic in high copper amalgam was the most slowly corroded phase. 3. Low copper amalgam was more susceptible in corrosion than high copper amalgam.

• Restorative Dentistry and Endodontics
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• 제19권1호
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• pp.1-26
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• 1994

The purpose of this study was to investigate the dissolution components during corrosion of amalgams and to identify surface corrosion products in the modified Fusayama artificial saliva. Four type of amalgam alloys were used: low copper lathe cut amalgam alloy (Cavex 68), low copper spherical amalgam alloy (Caulk Spherical Alloy), high copper admixed amalgam alloy (Dispersalloy) and high copper single composition amalgam alloy (Tytin). Each amalgam alloy and Hg were triturated according to the manufacturer's direction by means of mechanical amalgamator (Capmaster, S.S.White), and then the triturated mass was inserted into the cylindrical metal mold which was 10mm in diameter and 2.0mm in height and condensed with compression of 150kg/$cm^2$ using oil pressor. The specimens were removed from the mold and stored at room temperature for 7 days and cleansed with distiled water for 30 minutes in an ultrasonic cleaner. The specimens were immersed in the modified Fusayama artificial saliva for the periods of 1 month, 3 months and 6 months. The amounts of Hg, Cu, Sn and Zn dissolved from each amalgam specimen immersed in the artificial saliva for the periods of 1 month, 3 months and 6 months were measured using Inductivity Coupled Plasma Atomic Emission Spectrometry (ICPQ-1000, Shimadzu, Japan) and amount of Ag dissolved from amalgam specimen was measured using Atomic Absorption Spectrophotometry (Atomic Absorption/Flame emission spectrophotometer M-670, Shimadzu, Japan). A surface corrosion products of specimens were analysed using Electron Spectroscopy Chemical Analyser (ESCA PHI-558, PERKIN ELMER, U.S.A.). The secondary image and back scattered image of corroded surface of specimens was observed under the SEM, and the corroded surface of specimens was analysed with the EDX. The following results were obtained. 1. The dissolution amount of Cu was the most in high copper admixed amalgam(Dispersalloy) and the least in high copper single composition amalgam(Tytin). 2. Sn and Zn were dissolved during all the experiment periods, and dissolution amounts were decreased as the time elapsed. 3. Initial surface corrosion products were ZnO and SnO. 4. Corrosion of ${\gamma}$ and ${\gamma}_2$ phase in low copper amalgams was observed and Ag-Cu eutectic alloy phase was corroded in low copper spherical amalgam(Caulk Sperical Alloy). 5. Corrosion of ${\gamma}$ and $\eta$' phase in high copper amalgams was observed and Ag-Cu eutectic alloy phase was corroded in high copper admixed amalgam(Dispersalloy). 6. Sn-Cl was produced in the subsurface of low copper amalgams and high copper admixed amalgam.

• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.1-33
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• 1997

The objective of this study was to analyze the in vitro and in vivo corrosion products of low and high copper amalgams. The four different types of amalgam alloy used in this study were Fine cut, Caulk spherical, Dispersalloy, and Tytin. After each amalgam alloy and Hg were triturated according to the directions of the manufacturer by means of the mechanical amalgamator(Amalgam mixer. Shinhung Co. Korea), the triturated mass was inserted into a cylindrical metal mold which was 12mm in diameter and 10mm in height. The mass was condensed by 150Kg/cm compressive force. The specimen was removed from the mold and aged at room temperature for about seven days. The standard surface preparation was routinely carried out by emery paper polishing under running water. In vitro amalgam specimens were potentiostatically polarized ten times in a normal saline solution at $37^{\circ}C$(potentiostat : HA-301. Hukuto Denko Corp. Japan). Each specimen was subjected to anodic polarization scan within the potential range -1700mV to+400mV(SCE). After corrosion tests, anodic polarization curves and corrosion potentials were obtained. The amount of component elements dissolved from amalgams into solution was measured three times by ICP AES(Inductive Coupled Plasma Atomic Emission Spectrometry: Plasma 40. Perkim Elmer Co. U.S.A.). The four different types of amalgam were filled in occlusal and buccal class I cavities of four human 3rd molars. After about five years the restorations were carefully removed after tooth extraction to preserve the structural details including the deteriorated margins. The occlusal surface, amalgam-tooth interface and the fractured surface of in vivo amalgam corrosion products were analyzed. In vivo and in vitro amalgam specimens were examined and analyzed metallographically by SEM(Scanning Electron Microscope: JSM 840. Jeol Co. Japan) and EDAX(Energy Dispersive Micro X-ray Analyser: JSM 840. Jeol Co. Japan). 1. The following results are obtained from in vitro corrosion tests. 1) Corrosion potentials of all amalgams became more noble after ten times passing through the in vitro corrosion test compared to first time. 2) After times through the test, released Cu concentration in saline solution was almost equal but highest in Fine cut. Ag and Hg ion concentration was highest in Caulk spherical and Sn was highest in Dispersalloy. 3) Analyses of surface corrosion products in vitro reveal the following results. a)The corroded surface of Caulk spherical has Na-Sn-Cl containing clusters of $5{\mu}m$ needle-like crystals and oval shapes of Sn-Cl phase, polyhedral Sn oxide phase. b)In Fine cut, there appeared to be a large Sn containing phase, surrounded by many Cu-Sn phases of $1{\mu}m$ granular shapes. c)Dispersalloy was covered by a thick reticular layer which contained Zn-Cl phase. d)In Tytin, a very thin, corroded layer had formed with irregularly growing Sn-Cl phases that looked like a stack of plates. 2. The following results are obtained by an analysis of in vivo amalgam corrosion products. 1) Occlusal surfaces of all amalgams were covered by thick amorphous layers containing Ca-P elements which were abraded by occlusal force. 2) In tooth-amalgam interface, Ca-P containing products were examined in all amalgams but were most clearly seen in low copper amalgams. 3) Sn oxide appeared as a polyhedral shape in internal space in Caulk spherical and Fine cut. 4) Apical pyramidal shaped Sn oxide and curved plate-like Sn-Cl phases resulted in Dispersalloy. 5) In Tytin, Sn oxide and Sn hydroxide were not seen but polyhedral Ag-Hg phase crystal appeared in internal space which assumed a ${\beta}_l$ phase.

• Journal of Welding and Joining
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• 제30권2호
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• pp.54-58
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• 2012

Al-coated steel sheets with excellent heat and corrosion resistance are widely used in various applications. In welding of thin plate, some defects such as unmelted zone and metal-through occur easily in the beginning and ending of welding line. In the study, the welding defects in Al-coated steel sheets were investigated with respect to plasma arc current, height between Cu block and base metals, and using a roller to align the height of the base metal. Full penetration and voids free welds were obtained with a plasma arc current 52A and weld speed 2.3m/min. An unmelted zone increased and Ericshen rate decreased as the height between Cu block and base metal increased from 0 to 0.6mm. Using a roller moving ahead of the plasma arc, the length of unmelted zone decreased from 1.7mm to 0.5mm.

• 한국가스학회지
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• 제11권4호
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• pp.64-72
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• 2007

충수된 지상 탱크 저판부에서 발생하는 AE 신호 특성을 관찰하여 누수 등 손상에 대한 신호를 분석, 평가하였다. EMI 잡음신호를 에너지, 카운트. 지속시간 등과 누적진폭 분포상의 기울기를 비교 분석하여 제거하였다. EMI 신호는 높은 에너지 카운트, 지속시간을 나타내며, 누적 분포상에서 큰 기울기를 갖는 특성을 보였다. 남은 AE 신호의 위치표정과 클러스터 분석을 통해 부식손상의 가능성을 추정할 수 있었으며 총 20개의 클러스터로 에너지는 최대 11,990에서 8,565까지 이벤트는 최대 8에서 5까지 나타났다. 개방에 의한 손상확인을 하지 못했으나 보다 높은 고감도의 센서와 문턱값을 60dB 이상 높여서 평가한 다면 보다 정확한 발생위치 추정이 가능하리라 본다.

• Structural Engineering and Mechanics
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• 제47권2호
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• pp.167-183
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• 2013

Methods for estimating structural reliability using probability ideas are well established. When the residual ultimate strength of a buried pipeline is exceeded the limit, breakage becomes imminent and the overall reliability of the pipe distribution network is reduced. This paper is concerned with estimating structural failure of underground flexible pipes due to corrosion induced excessive deflection, buckling, wall thrust and bending stress subject to externally applied loading. With changes of pipe wall thickness due to corrosion, the moment of inertia and the cross-sectional area of pipe wall are directly changed with time. Consequently, the chance of survival or the reliability of the pipe material is decreased over time. One numerical example has been presented for a buried steel pipe to predict the probability of failure using Hasofer-Lind and Rackwitz-Fiessler algorithm and Monte Carlo simulation. Then the parametric study and sensitivity analysis have been conducted on the reliability of pipeline with different influencing factors, e.g. pipe thickness, diameter, backfill height etc.

• 한국농공학회지
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• 제42권4호
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• pp.106-114
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• 2000

An investigation was conducted to get the basic data for establishing maintenance strategy of pipe framed greenhouses. The contents of the investigation consisted of actual state of structures, maintenance status, meteorological disaster, and corrosion characteristics of pipe framework in greenhouses. the number of greenhouses investigated was 108 in total. Most multi-span greenhouses had narrower width and lower height than the standared 1-2W greenhouse, and most of single-span greenhouses were tunnel type. In multi-span greenhouses, the size and interval of frameworks such as rafter, purline, column , and cross beam were mostly suitable, but frameworks of single-span greenhouses were mostly insufficient. After about 7 years in grounds, 8 years in joints, 10 years in bending parts. and 13 years in columns. pipe surface was mostly rusted. Most weak parts in corrosion were pipes in contact with the ground, joints, roll-up shaft pipes, and pipes close to the gutter. Almost all of the greenhouse farmers didn't pay any attention to maintenance affair in a regular interval for pipe framed grenhouses. Many greenhouses have experienced the meteorologicla diaster such as uplift of foundation, partial or complete failure by the hyphoon and/or high winds.