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Archaeological Scientific Characteristics of Patternless Pottery with Talc Temper: Baekseokdong Gojaemigol Site in Cheonan, Korea (활석비짐 무문토기의 고고과학적 특성: 천안 백석동 고재미골 유적)

  • Kim, Su Kyoung;Lee, Chan Hee
    • Journal of Conservation Science
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    • v.31 no.2
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    • pp.159-173
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    • 2015
  • The patternless potteries excavated from the Baekseokdong Gojaemigol site in Cheonan, was subdivided into talc and non-talc (including amphibole) type pottery. The potteries showed black, reddish brown and yellowish brown colors, but represent to difference with occurrences and internal texture of raw materials and temper minerals. The all potteries and paleosoils are commonly high content of temper minerals with poorly sorting and roundness of particles, and the paleosoils composed mainly of quartz, plagioclase, mica, chlorite and kaolinite. Between the talc and non-talc type potteries are very similar with magnetic susceptibility, absorption ratio and specific gravity. Geochemical behaviors of major, minor, compatible and incompatible elements in talc pottery are very similar with amphibole, non-talc pottery and paleosoils, and well correspondence with enrichment and deficiency patterns of each element, and the talc and amphibole potteries are highly enriched patterns of MgO concentration. In paleosoils of Gojaemigol site, talc and amphibole are not detected, therefore, making the pottery of the site estimate the possible to artificial additions of the temper minerals of talc and amphibole used interbedded talc layer within gneiss complex near the Baekseokdong area. Based on the phase relations, differential thermal and thermal gravimetric analyses, the potteries could be classified into two groups by firing temperature. The one group of talc temper pottery fired from 800 to $870^{\circ}C$ and the other group of amphibole and non-talc temper pottery revealed of 900 to $950^{\circ}C$.

Carotenoid Pigments of Bivalves 1. Comparison of Carotenoid Pigments from Muscle of Mussel and Blue mussel (이매패의 Carotenoid 색소성분 1. 홍합과 진주담치 근육의 Carotenoid 색소성분의 비교)

  • 하봉석;강동수
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.20 no.4
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    • pp.369-375
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    • 1991
  • Carotenoid pigments from muscle of mussel, Mytilus coruscus, and blue mussel edulis, were separated by thin layer and column chromatography. The isolated carotenoids were identified by comparative test with reference carotenoids, reduction with sodium borohydride, isomerization with iodine and absorption spectrophotometry. The carotenoid content in the muscle of mussel were 0.4mg% in male and 2.7mg% in female, and the carotenoids were composed of 23.4%, 33.4% mytiloxanthin, 26.3%, 22.5% 3, 4, 3'-trihydroxy-7', $8'-didehydro-{\beta}-carotene$, 24.8%, 22.8% pectenoxanthin, 14.0%, 9.9% pectenolone and 5.1%, 6.1% diatoxanthin in male and female, respectively. While, the carotenoid contents in the muscle of blue mussel were 1.1mg% in male and 3.2mg% in female, and the carotenoids were composed of 33.8%, 35.6% mytiloxanthin, 28.4%, 44.7% pectenoxanthin, 18.1%, 5.0% diatoxanthin, 9.7%, 8.7% pectenolone and 5.5%, 3.1%, 3, 4, 3'-trihydroxy-7', $8'-didehydro-{\beta}-carotene$ in male and female, respectively.

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Physicochemical Characteristics of Bamboo Smoke Distillates Processed by Mechanical Steel Kiln and Traditional Earth Kiln (기계식 탄화로와 재래식 토요를 이용하여 제조한 죽초액의 이화학적 특성: 식품처리제로서의 특성)

  • 이범수;은종방
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.31 no.2
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    • pp.251-256
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    • 2002
  • Fresh bamboo (Phyllostachys bambuoides sieb. et zucc.) was charred at the mechanical steel kiln and traditional earth kiln with subsequent condensation of its smoke to 10$0^{\circ}C$. It was settled down for 12 months to remove tar components and then the middle layer of the liquid was collected as a bamboo smoke distillates to analyze its chemical composition and physicochemical characteristics for use as food additives or processing aids. The gravity, transmittance, reflectivity, and viscosity were 1.008, 89.05%, 1.36%, and 12.48 cp in the bamboo smoke distillates processed by mechanical steel kiln (MBSD) and 1.012, 98.33%, 1.34% and 9.05 cp in the bamboo smoke distillates by traditional earth kiln (TBSD), respectively. The color of TSBD was brighter than that of MBSD. The pH and titratable acidity, tar and remains were 3.55 and 2.830%, 2.803% and 0.671%, respectively, in the MBSD and 2.93 and 3.470%, 0.051% and 0.004%, respectively, in the TBSD. The major phenolic compounds of bamboo smoke distillates (BSD) were phenol, Ο-cresol, p-cresol, and guaiacol and the major organic acids were acetic acid, propionic acid, iso-butyric acid, and n-butyric acid, and major alcohols were methanol, furfuryl alcohol, and maltol. The contents of phenolic compound and alcohol were more in MBSD than in TBSD whereas the content of organic acid was more in TBSD than in MBSD. Therefore, toxic compounds for the human body, such as methanol from BSD should be removed for use as a food ingredient in the future.

Extraction and Composition of Bound Lipids in Naked Barley (쌀보리 결합지질의 추출과 그 조성에 관한 연구)

  • Kim, Hae-Gyoung;Kim, Bok-Nam;Choi, Hong-Sik
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.18 no.1
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    • pp.109-114
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    • 1989
  • Bound lipids(BL) of naked barley(Hordeum vulgare L.) were extracted by different methods and the composition of BL was determined by the procedures of column chromatography, thin layer chromatography and gas chromatography. For the extraction, after free lipids were removed from barley flour by petroleum ether(PE) extraction and then BL were extracted from PE treated flour by the solvent systems of water-saturated butanol(WSB) at $25^{\circ}C$(WSB-LT) and at $95^{\circ}C$ (WSB-HT). BL were extracted by WSB-HT with higher extraction yield as 1.5% as dry basis of flour. The contents of neutral lipids(NL), glycolipids(GL) and phospholipid(PL) in BL were $20.7{\sim}35.5%$, $28.7{\sim}32.4%$, $32.1{\sim}50.6%$, respectively with particularly higher content of PL in WSB-HT as 50.6%. Digalactosyl-diglycerides $(40.2{\sim}44.8%)$, monogalactosyl-diglycerides $(20.3{\sim}31.1%)$, sterly glycerides$(11.2{\sim}15.2%)$ and cereb rosides$(11.6{\sim}12.9%)$ were observed in GL. Of the PL in BL, lysophosphatidyl choline, phosphatidyl choline and phosphatidyl serine, and phosphatidyl ethanolamine were the major components. The predominent fatty acids of NL, GL and PL were linoleic and palmitic acids, however, no significant difference was observed in the composition of fatty acids between two extraction methods.

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Accumulation of Crude Lipids, Phenolic Compounds and Iron in Rusty Ginseng Root Epidermis (적변삼 외피에서 지질, 페놀성물질 및 철 성분의 축적에 관한 연구)

  • Lee, Tae-Su;Mok, Sung-Kyun;Cheon, Seong-Ki;Yoon, Jong-Hyuk;Baek, Nam-In;Choe, Jyung
    • Journal of Ginseng Research
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    • v.28 no.3
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    • pp.157-164
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    • 2004
  • The study was conducted to investigate the tissue and chemical characteristics of rusty root epidermal cells. In histological study, the rusty symptoms were frequently observed in the epidermis of ginseng root and to be yellow under microscopic observation. Disks of the epidermal cell tissue of the rusty root were usually 2 and 3 times greater in the number of cell layer and thickness of cell wall than the healthy root, respectively. The color degree of methanol extracts from the rusty root epidermis was 5.5 times higher than that of the healthy root. And the extracts of rust matter in the root epidermis were easily dissolved in polar solvents compared to nonpolar solvents. UV-absorption spectra of methanol extracts in various fractions of phenolics showed a maximum peak between 275∼280 nm. The crude lipids and phenolic compounds such as acid insoluble bound phenolics, acid insoluble esterified phenolics, acid insoluble condensed phenolics, insoluble bound phenolics and free phenolics were also more in the rusty root epidermis than in the healthy one. Fe content in the rusty root epidermis was 2.7 times higher than that of healthy one. It was presumed that the phenolic compounds(precursor of the rusty) in association with lipid and iron in the root epidermis might defence the root when ginseng root was depressed by the unfavorable conditions in soil and/or portions of a root system were subjected to anoxic conditions.

Study on the Improvement of BGA Solderability in Electroless Nickel/Gold Deposit (무전해 Ni/Au 도금에서의 BGA Solderability 특성 개선에 관한 연구)

  • 민재상;황영호;조일제
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.3
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    • pp.55-62
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    • 2001
  • With a spread of BGA, CSP and fine pitch devices, the need of flatter surface finish in bare board is becoming more critical in solderability. The electroless Ni/Au plating has a solution of these needs and also has being spread to apply to surface finish for bare board in many electronic goods. But, the electroless Ni/Au plating had several issues such as Ni oxidation and phosphorous contents. Before this study, we studied on the effect of BGA solderability in electroless Ni/Au plating and chose some major factors such as the oxidation property of NiP plating and warpage of board. Firstly, we made test board with various plating conditions and improved the plating property through the improvement of NiP oxidation reducing P content. Also, we minimized the warpage of board with the improvement of inner layer structure and the analysis of warpage. For the evaluation of solderability, we analyzed the warpage of board and the plating property after mounting BGA on the board with optimizing conditions. The solder joint of BGA is investigated by SEM(Scanning Electronic Microscope) and OM(Optical Microscope). The composition of joint is used by EDS(Energy Dispersive Spectroscopy). We analyzed the fracture strength and mode by ball shear teser.

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A study on the Thermal Filter Press for the Reduction of Pigment Sludge (안료 슬러지 감량화(減量化)를 위한 열필터프레스 기술(技術)에 관한 연구(硏究))

  • Lee, Jung-Eun;Lee, Jae-Keun
    • Resources Recycling
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    • v.18 no.3
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    • pp.55-61
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    • 2009
  • Dewatering process to remove water from pigment sludge was important in the diverse aspects of the improvement of product quality, curtailment of the drying cost and the transportation. It was difficult to dewater pigment particles with the mechanical forces because the size was fine under $5{\mu}m$. Thermal filter press dewatering equipment composed of squeezing plate and a fixed heating plate was developed to improve the dewaterability of pigment the sludge as supplying the heat from the fixed heating plate to the cake. Several tests that estimate the dewaterability for pigment sludge as with or without squeezing process and the difference of dewatering time was conducted with this equipment. Dewaterability of thermal dewatering under squeezing process was increased about 20% compared with non squeezing process. Under squeezing process, thermal dewatering tests changing dewatering time with 70 and 80 minute were conducted respectively. The water content of cake was more reduced at dewatering time of 80 minute compared with 70 minute, and dewatering velocity was also decreased, which caused the productivity of thermal filter press to drop. It was observed that clogging of filter cloth didn't almost occur because the liquid was discharged from cake layer easily. In this research, it was resulted that the squeezing process and long dewatering time were effective to improve the dewaterability of pigment sludge. So, this thermal filter press equipment was useful for dewatering the fine particle sludge like pigment.

Environment and Vegetation Characteristics of Aconitum austrokoreense Koidz. habitats (세뿔투구꽃의 자생지 식생과 환경특성)

  • Park, Jeong-Geun;Pi, Jung-hun;Jung, Ji-young;Park, Jeong-seok;Yang, Hyung-ho;Lee, Cheul-ho;Suh, Gang-uk;Son, Sung-won
    • Korean Journal of Environment and Ecology
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    • v.30 no.5
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    • pp.896-907
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    • 2016
  • The habitat characteristics of Aconitum austrokoreense Koidz. were investigated to provide basic data for conservation and restoration. The altitude ranged from 260m to 728m with inclinations of $4-39^{\circ}$. As a result of vegetation survey within natural populations, a total of 147 taxa were identified inside 20 quadrates in 7 natural habitats. The importance value of Aconitum austrokoreense was 23.0% based on the coverage and frequency of the herbaceous layer and sat is more dominant. Species diversity was 1.23, and dominace and evenness were found to be 0.22 and 0.77, respectively. The soil type were silty loam (four sites), sandy loam (two sites) and loam (one site). The average field organic matter was 7.83% and the total nitrogen and pH were 0.35, and 5.69. Correlation analysis between environmental factors and population characteristic showed the correlations between chlorophyll content and slope, flowering rate and soil humidity. Conservation on habitats conditions is important for stable maintenance the flora and the surrounding area including habitats has to be designated a protection area for habitats conservation.

A Study on the Effect of Compaction Energy on Soil Compaction (흙의 다짐에너지가 다짐효과(效果)에 미치는 영향(影響)에 관(關)한 연구(硏究))

  • Kim, Sang Mok;Kang, Yea Mook
    • Korean Journal of Agricultural Science
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    • v.10 no.1
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    • pp.97-109
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    • 1983
  • In this study, the effects on the soil compaction were investigated through the various testing method by changing the number of layers, the number of blows per layer and drop height. The results obtained in this study were summarized as follows. 1. Soil compaction was largely influenced by maximum grain size of soil in case of small testing mold diameter. 2. The compaction effect showed best in the well graded soil. In this test, compaction effect showed the best value in the soil which contained about 30~40% of particles finer than No. 200 sieves although it would vary according to the content of coarse grained soil. 3. Though the compaction method was changed at the level of compaction energy fixed, the effect of soil compaction showed little. 4. The increment of compaction energy increased the effect of soil compaction, but over a certain limit the soil compaction showed little on the effect. 5. In the method to increase the compaction energy for the purpose of the most reasonable effect, the soil compaction effect was differently shown according to the grain size distribution of the soil.

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DIFFERENCE OF CALCIUM FLUORIDE FORMATION BETWEEN THE ENAMEL AND DENTIN AFTER FLUORIDE APPLICATION IN VITRO (불소적용시 법랑질과 상아질에서 불화칼슘형성의 차이에 관한 실험적 연구)

  • Kim, Jae-Gon;Kweon, Seon-Ja;Yun, Hyun-Du;An, Soo-Hyeon;Baik, Byeong-Ju
    • Journal of the korean academy of Pediatric Dentistry
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    • v.25 no.1
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    • pp.209-224
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    • 1998
  • The purpose of this study was to compare the amount of calcium fluoride deposited on the enamel and dentin surface and to obtain information on the morphological change and crystallographic details of mineral deposition after 12,000ppm APF application in vitro. The bovine enamel and dentin blocks were randomly assigned to eight groups according to artificial caries lesion formation and difference of fluoride application time. The fluoride concentration and morphological characteristics on the treated enamel and dentin surface were investigated by using fluoride quantitative analysis and SEM. The powdered enamel and dentin of the intact bovine incisors were prepared for the X-ray diffraction analysis. The following results were obtained. 1. The amounts of KOH-soluble fluoride on the carious enamel and dentin surface after 24h APF application were higher than after only 5min APF application(p<0.05), but in the case of the sound enamel and dentin surface were similar after 5min and 24h application (P>0.05). The fluoride content was highly increased in the carious dentin as compared with sound dentin after APF application(P<0.05). 2. The carious enamel surface after APF application, the demineralized enamel surface were recovered a more dense enamel surface and precipitation of crystal was observed a distintive surface layer of spherical globules of about 1 m diameter. In the case of the fluorided carious dentin surface, precipitation of calcium fluoride-like material was deposited both inside the dentinal tubules as well as in the intertubular regions. 3. The crystallographic structure of powdered enamel and dentin after 24h APF application had large crystallities of apatite and CaF2 diffraction peaks in the enamel as compared with dentin. The diffraction data collected from the 27.50-29.50(2) angular range of the powdered enamel, the (105) apatite, (225) apatite and (111) CaF2 peaks of the enamel crystallities were detected after 24h APF application.

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