• Title/Summary/Keyword: Constituent phase

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Microstructure Characterization of Nb-Si-B alloys Prepared by Spark Plasma Sintering Process (방전 플라즈마 소결(Spark Plasma Sintering) 방법에 의해 제조된 Nb-Si-B계 합금의 미세조직 특성)

  • Kim, Sang-Hwan;Kim, Nam-Woo;Jeong, Young-Keun;Oh, Sung-Tag;Kim, Young Do;Lee, Seong;Suk, Myung Jin
    • Journal of Powder Materials
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    • v.22 no.6
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    • pp.426-431
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    • 2015
  • Microstructural examination of the Nb-Si-B alloys at Nb-rich compositions is performed. The Nb-rich corner of the Nb-Si-B system is favorable in that the constituent phases are Nb (ductile and tough phase with high melting temperature) and $T_2$ phase (very hard intermetallic compound with favorable oxidation resistance) which are good combination for high temperature structural materials. The samples containing compositions near Nb-rich corner of the Nb-Si-B ternary system are prepared by spark plasma sintering (SPS) process using $T_2$ and Nb powders. $T_2$ bulk phase is made in arc furnace by melting the Nb slug and the Si-B powder compact. The $T_2$ bulk phase was subsequently ball-milled to powders. SPS is performed at $1300^{\circ}C$ and $1400^{\circ}C$, depending on the composition, under 30 MPa for 600s, to produce disc-shaped specimen with 15 mm in diameter and 3 mm high. Hardness tests (Rockwell A-scale and micro Vickers) are carried out to estimate the mechanical property.

Interface Fracture and Crack Propagation in Concrete : Fracture Criteria and Numerical Simulation (콘크리트의 계면 파괴와 균열 전파 : 파괴규준과 수치모의)

  • 이광명
    • Magazine of the Korea Concrete Institute
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    • v.8 no.6
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    • pp.235-243
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    • 1996
  • The mechanical behavior ot concrete is strongly influenced by various scenarios of crack initiation and crack propagation. Recently. the study of the interface fracture and cracking in interfacial regions is emerged as an important field, in the context of the developement of high performance concrete composites. The crack path criterion for elastically homogeneous materials is not valid when the crack advances at an interface because. in this case, the consideration of the relative magnitudes of the fracture toughnesses between the constituent materials and the interface are involved. In this paper, a numerical method is presented to obtain the values of two interfacial fracture parameters such as the energy release rate and the phase angle at the tip of an existing interface crack. Criteria based on energy release rate concepts are suggested for the prediction of crack growth at the interfaces and an hybrid experimental-numerical study is presented on the two-phase beam composite models containing interface cracks to investigate the cracking scenarios in interfacial regions. In general, good agreement between the experimental results and the prediction from the criteria is obtained.

Estimating Ocean Tidal Constituents Using SAR Interferometric Time Series over the Sulzberger Ice Shelf, W. Antarctica

  • Baek, Sang-Ho;Shum, C.K.
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.36 no.5
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    • pp.343-353
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    • 2018
  • Ocean tides in Antarctica are not well constrained mostly due to the lack of tidal observations. Especially, tides underneath and around ice shelves are uncertain. InSAR (Interferometric Synthetic Aperture Radar) data has been used to observe ice shelf movements primarily caused by ocean tides. Here, we demonstrate that it is possible to estimate tidal constituents underneath the Sulzberger ice shelf, West Antarctica, solely using ERS-1/2 tandem mission DInSAR (differential InSAR) observations. In addition, the tidal constituents can be estimated in a high-resolution (~200 m) grid which is beyond any tidal model resolution. We assume that InSAR observed ocean tidal heights can be derived after correcting the InSAR data for the effect of atmospheric loading using the inverse barometric effect, solid earth tides, and ocean tide loading. The ERS (European Remote Sensing) tandem orbit configuration of a 1-day separation between SAR data takes diminishes the sensitivity to major tidal constituents including $K_1$ and $S_2$. Here, the dominant tidal constituent $O_1$ is estimated using 8 differential interferograms underneath the Sulzberger ice shelf. The resulting tidal constituent is compared with a contemporary regional tide model (CATS2008a) and a global tide model (TPXO7.1). The InSAR estimated tidal amplitude agrees well with both models with RMS (root-mean-square) differences of < 2.2 cm and the phase estimate corroborating both tide models to within $8^{\circ}$. We conclude that fine spatial scale (~200 m) Antarctic ice shelf ocean tide determination is feasible for dominant constituents using C-band ERS-1/2 tandem mission InSAR.

Cancer Prevention with Green Tea and Its Principal Constituent, EGCG: from Early Investigations to Current Focus on Human Cancer Stem Cells

  • Fujiki, Hirota;Watanabe, Tatsuro;Sueoka, Eisaburo;Rawangkan, Anchalee;Suganuma, Masami
    • Molecules and Cells
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    • v.41 no.2
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    • pp.73-82
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    • 2018
  • Cancer preventive activities of green tea and its main constituent, (-)-epigallocatechin gallate (EGCG) have been extensively studied by scientists all over the world. Since 1983, we have studied the cancer chemopreventive effects of EGCG as well as green tea extract and underlying molecular mechanisms. The first part of this review summarizes groundbreaking topics with EGCG and green tea extract: 1) Delayed cancer onset as revealed by a 10-year prospective cohort study, 2) Prevention of colorectal adenoma recurrence by a double-blind randomized clinical phase II trial, 3) Inhibition of metastasis of B16 melanoma cells to the lungs of mice, 4) Increase in the average value of Young's moduli, i.e., cell stiffness, for human lung cancer cell lines and inhibition of cell motility and 5) Synergistic enhancement of anticancer activity against human cancer cell lines with the combination of EGCG and anticancer compounds. In the second part, we became interested in cancer stem cells (CSCs). 1) Cancer stem cells in mouse skin carcinogenesis by way of introduction, after which we discuss two subjects from our review on human CSCs reported by other investigators gathered from a search of PubMed, 2) Expression of stemness markers of human CSCs compared with their parental cells, and 3) EGCG decreases or increases the expression of mRNA and protein in human CSCs. On this point, EGCG inhibited self-renewal and expression of pluripotency-maintaining transcription factors in human CSCs. Human CSCs are thus a target for cancer prevention and treatment with EGCG and green tea catechins.

Universal Existence of One Chlorophyll a' Molecule in Photosystem I of Oxygenic Photosynthetic Organisms

  • Nakamura, Akimasa;Yoshida, Emi;Taki, Takashi;Watanabe, Tadashi
    • Journal of Photoscience
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    • v.9 no.2
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    • pp.367-369
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    • 2002
  • Chlorophyll (ChI) a' is the Cl3$^2$-epimer of ChI a which is the constituent of P700, the primary electron donor of Photosystem (PS) I, of a thrmophilic cyanobacterium, Synechococcus elongatus, whose structure was recently determined by X-ray crystallography. To determine whether PS I of diverse oxygenic photosynthetic organisms universally contain one molecule of ChI a ’, pigment compositions of thylakoid membranes and PS I complexes isolated from cyanobacteria, green algae, red algae and higher plants were determined by reversed-phase HPLC. The results show that involvement of one ChI a'molecule in PS I is the universal feature for Chi a-based PS I of oxygenic photosynthetic organisms.

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Microstructure Evolution of Solid State Reacted HAp/β-TCP Composite Powders by Post-Treatment Processing (후처리공정에 따른 고상반응 β-TCP/HAp 복합분체의 미세구조 변화)

  • 박영민;양태영;박상희;윤석영;박홍채
    • Journal of the Korean Ceramic Society
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    • v.41 no.8
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    • pp.582-587
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    • 2004
  • Biphasic Calcium Phosphate (BCP) consisted of hydroxyapatite (HAp) and $\beta$-tricalcium phosphate (P-TCP) has been prepared by solid state reaction. The size reduction of the resultant BCP agglomerate was carried out by reaction with hot water under atmospheric condition uld also under high pressure using an autoclave. The influence of processing conditions on the change of crystalline phase and composition, relative amount of constituent, specific surface area, and microstructure was investigated by means of XRD, FT-IR, BET method using a nitrogen adsorption and SEM.

Analysis of γ-Aminobutyric Acid Content in Fermented Plant Products by HPLC/UV

  • Lee, Dong Gu;Cho, Sunghun;Lee, Jamin;Cho, Seon Haeng;Lee, Sanghyun
    • Journal of Applied Biological Chemistry
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    • v.58 no.4
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    • pp.303-309
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    • 2015
  • ${\gamma}$-Aminobutyric acid (GABA) content in fermented plant products and their main plant materials (aerial part of Acanthopanax sessiliflorus, fruit of Crataegus pinnatifida, and whole plant of Morus alba) was determined by high-performance liquid chromatography. GABA was quantified using a reverse-phase column with a gradient elution program (water:acetonitrile =90:10 to 0:100 for 40 min). UV detection was conducted at 280 nm. GABA content was measured in fermented plant products (15.07 mg/g), aerial part of A. sessiliflorus (4.49 mg/g), fruit of C. pinnatifida (10.59 mg/g), and whole plant of M. alba (2.31 mg/g). The presence of GABA in fermented plant products, including A. sessiliflorus, C. pinnatifida, and M. alba is important in industrial application for health supplements.

A postprocessing method for korean optical character recognition using eojeol information (어절 정보를 이용한 한국어 문자 인식 후처리 기법)

  • 이영화;김규성;김영훈;이상조
    • Journal of the Korean Institute of Telematics and Electronics C
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    • v.35C no.2
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    • pp.65-70
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    • 1998
  • In this paper, we will to check and to correct mis-recognized word using Eojeol information. First, we divided into 16 classes that constituents in a Eojeol after we analyzed Korean statement into Eojeol units. Eojeol-Constituent state diagram constructed these constitutents, find the Left-Right Connectivity Information. As analogized the speech of connectivity information, reduced the number of cadidate words and restricted case of morphological analysis for mis-recognition Eojeol. Then, we improved correction speed uisng heuristic information as the adjacency information for Eojeol each other. In the correction phase, construct Reverse-Order Word Dictionary. Using this, we can trace word dictionary regardless of mis-recongnition word position. Its results show that improvement of recognition rate from 97.03% to 98.02% and check rate, reduction of chadidata words and morpholgical analysis cases.

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MEASUREMENT OF SYNTHESIS RATE OF LONG-CHAIN ACYL-COENZYME A ESTER IN BOVINE LIVER BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY

  • Mitsuhashi, T.;Mitsumoto, M.;Yamashita, Y.;Ozawa, S.
    • Asian-Australasian Journal of Animal Sciences
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    • v.1 no.2
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    • pp.99-106
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    • 1988
  • A high performance liquid chromatographic procedure is described for the direct determination of the picomole amount of palmitoyl-Coenzyme A and stearoyl-Coenzyme A, using a stainless steel column packed with C-18 derivatized porous silica ($5{\mu}m$), an isocratic elution with a mixture of 33 mM $KH_2PO_4$/acetonitrile as a mobile phase and a UV detector. The long-chain acyl-Coenzyme A esters were determined in incubated microsomal fractions of a bovine liver to demonstrate the utility of this method for monitoring acyl-CoA synthesis in biological samples. The reaction rate of palmitate was higher than that of stearate. After a 60 minute incubation period, the generated amount of palmitoyl-Coenzyme A and stearoyl-Coenzyme A were approximately 70 and 20 n mol/mg micresomal protein, respectively. The advantage of this method are in that no decomposition of the CoA esters is involved, while the constituent molecular species is detected.

Long-term Monthly Variations of Tide in Pusan Harbour (부산항 조석의 장기 월별 변동 특성)

  • 김종규;강태순
    • Journal of Ocean Engineering and Technology
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    • v.16 no.2
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    • pp.6-9
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    • 2002
  • The long-term monthly variations of tide with tidal harmonic analysis in Pusan Harbour are investigated. The present spring tidal range decreased 1.4 cm and the variation of phase lag increased than 1974. The high and low water level of yearly mean sea level is show during the February to March and August to September, respectively. It is important to note that the larger lunar elliptic N2 is large in comparison with lunisolar diurnal K1 and principal lunar diurnal O1. The ratios (Correction Factors) of monthly mean sea level and the main 4 tidal constituents are evaluated to correct the shortly (monthly) observed tide for the design of harbour facilities.