• Title/Summary/Keyword: Compressibility characterization

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Fabrication and Characterization of Taraxacum platycarpum Extract-loaded Particles for Tablet Dosage Form (정제 제형 제조를 위한 포공영 추출물 함유 분말의 제조 및 평가)

  • Jin, Sung Giu
    • Journal of Powder Materials
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    • v.26 no.3
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    • pp.225-230
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    • 2019
  • To develop Taraxacum platycarpum extract (TP)-loaded particles for tablet dosage form, various TP-loaded particles composed of TP, dextrin, microcrystalline cellulose (MCC), silicon dioxide, ethanol, and water are prepared using a spray-drying method and fluid-bed-drying method. Their physical properties are evaluated using angle of repose, Hausner ratio, Carr's index, hardness, disintegrant time, and scanning electron microscopy. Optimal TP-loaded particles improve flowability and compressibility. Furthermore, 2% silicon dioxide gives increased flowability and compressibility. The formula of TP-loaded fluid-bed-drying particles at a TP/MCC/silicon-dioxide amount of 5/5/0.2 improves the angle of repose, Hausner ratio, Carr's index, hardness, and disintegrant time as compared with the TP-loaded spray-drying particles. The TP-loaded fluid-bed-drying particles considerably improve flowability and compressibility ($35.10^{\circ}$ vs. $40.3^{\circ}$, 0.97 vs. 1.17, and 18.97% vs. 28.97% for the angle of repose, Hausner ratio, and Carr's index, respectively), hardness (11.34 vs. 4.7 KP), and disintegrant time (7.4 vs. 10.4 min) as compared with the TP-loaded spray-drying particles. Thus, the results suggest that these fluid-bed-drying particles with MCC and silicon dioxide can be used as powerful particles to improve the flowability and compressibility of the TP.

A Study on Geotechnical Stability of the Sludge Mixed Soil (슬러지가 혼합된 지반의 공학적 안정 특성에 관한 연구)

  • Hwang, Sung-Pil;Jeoung, Jae-Hyeung
    • Journal of Korean Society of Disaster and Security
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    • v.10 no.1
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    • pp.55-60
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    • 2017
  • The dyeing sludge can be weakened by inflow of rainfall or absorption of moisture after it is buried in a waste landfill. This study tested the dyeing sludge and earth/sand mixture to check the problem when the dehydrated dyeing sludge is buried in a waste landfill. When the dyeing sludge was left idle with high water content inside a landfill with poor draining for a long period, the water permeability decreased to around 3/100 level and the compressibility increased by 1.4 times compared to the dyeing sludge at a dyeing factory. The study result indicated that it was important to reduce the water content inside the landfill for stability. Also, the facilities to secure the drainage path and eliminate leachate were needed.

Fabrication and Characterization of Gastrodia elata-loaded Particles for Increased Moisture Stability (수분 안정성 향상을 위한 천마 추출물 함유 분말의 제조 및 평가)

  • Jung, Jae Hwan;Jin, Sung Giu
    • Journal of Powder Materials
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    • v.27 no.3
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    • pp.241-246
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    • 2020
  • To develop Gastrodia elata (GE)-loaded particles for herbal extract dosage forms, various GE-loaded particles containing dextrin, isomalt, maltodextrin, and silicon dioxide as solidifying carriers in the GE water extract are prepared using the spray drying method. Their physical properties are evaluated using the repose angle, Hausner ratio, Carr's index, weight increase rate at 40℃/75% RH condition, and scanning electron microscopy (SEM). Particles made of dextrin improve the fluidity, compressibility, and water stability. In addition, 2% silicon dioxide increases the fluidity and moisture stability. The best flowability and compressibility of GE-loaded particles are observed with TP, dextrin, and silicon dioxide amounts in the ratio of 6/4/0.2 (34.29 ± 2.86°, 1.48 ± 0.03, and 38.29 ± 2.39%, repose angle, Hausner Ratio, and Carr's index, respectively) and moisture stability with a 2% weight increase rate for 14 h at 40℃/75% RH condition. Therefore, our results suggest that the particles prepared by the spray drying method with dextrin and 2% silicon dioxide can be used as powerful particles to improve the flowability, compressibility, and moisture stability of GE.

Fabrication and Characterization of Bangpungtongseong-San Extract-loaded Particles for Tablet Dosage Form (생약 추출물 함유 정제 제조를 위한 이산화규소 함유 분말의 제조 및 평가)

  • Park, Jinwoo;Jin, Sung Giu
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.227-232
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    • 2021
  • The purpose of this study is to optimize the powder formulation and manufacturing conditions for the solidification of an extract of the herb Bangpungtongseong-san (BPTS). To develop BPTS-loaded particles for the tablet dosage form, various BPTS-loaded particles composed of BPTS, dextrin, microcrystalline cellulose (MCC), silicon dioxide, ethanol, and water are prepared using spray-drying and high shear granulation (high-speed mixing). Their physical properties are evaluated using scanning electron microscopy and measurements of the angle of repose, Hausner ratio, Carr's index, hardness, and disintegration time. The optimal BPTS-loaded particles exhibit improved flowability and compressibility. In particular, the BPTS-loaded particles containing silicon dioxide show significantly improved flowability and compressibility (the angle of repose, Hausner ratio, and Carr's index are 35.27 ± 0.58°, 1.18 ± 0.06, and 15.67 ± 1.68%, respectively), hardness (18.97 ± 1.00 KP), and disintegration time (17.60 ± 1.50 min) compared to those without silicon dioxide. Therefore, this study suggests that particles prepared by high-speed mixing can be used to greatly improve the flowability and compressibility of BPTS using MCC and silicon dioxide.

Engineering characterization of intermediate geomaterials - A review

  • T. Ashok Kumar;Ramanandan Saseendran;V. Sundaravel
    • Geomechanics and Engineering
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    • v.33 no.5
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    • pp.453-462
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    • 2023
  • Intermediate Geomaterials (IGMs) are natural formation materials that exhibit the engineering behavior (strength and compressibility) between soils and rocks. The engineering behavior of such material is highly unpredictable as the IGMs are stiffer than soils and weaker/softer than rocks. Further, the characterization of such material needs exposure to both soil and rock mechanics. In most conventional designs of geotechnical structures, the engineering properties of the IGMs are either aligned with soils or rocks, and this assumption may end up either in an over-conservative design or under-conservative design. Hence, many researchers have attempted to evaluate its actual engineering properties through laboratory tests. However, the test results are partially reliable due to the poor core recovery of IGMs and the possible sample disturbance. Subsequently, in-situ tests have been used in recent years to evaluate the engineering properties of IGMs. However, the respective in-situ test finds its limitations while exploring IGMs with different geological formations at deeper depths with the constraints of sampling. Standard Penetration Test (SPT) is the strength-based index test that is often used to explore IGMs. Moreover, it was also observed that the coefficient of variation of the design parameters (which represents the uncertainties in the design parameters) of IGMs is relatively high, and also the studies on the probabilistic characterization of IGMs are limited compared with soils and rocks. With this perspective, the present article reviews the laboratory and in-situ tests used to characterize the IGMs and explores the shear strength variation based on their geological origin.

Analysis of load-settlement behaviour of shallow foundations in saturated clays based on CPT and DPT tests

  • Mir, Mouna;Bouafia, Ali;Rahmani, Khaled;Aouali, Nawel
    • Geomechanics and Engineering
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    • v.13 no.1
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    • pp.119-139
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    • 2017
  • Static Penetration Test (CPT) and Dynamic Penetration Test (DPT) are commonly used in-situ tests in a routine geotechnical investigation. Besides their use for qualitative investigation (lithology, homogeneity and spatial variability), they are used as practical tools of geotechnical characterization (resistance to the penetration, soil rigidity) and modern foundation design as well. The paper aims at presenting the results of an extensive research work on the evaluation of the 1D primary consolidation settlement of saturated clayey soils on the basis of the CPT or DPT tests. The work is based on an analysis of the correlations between the tip resistance to penetration measured in these tests and the parameters of compressibility measured by the compressibility oedometer test, through a local geotechnical database in the northern Algeria. Such an analysis led to the proposal of two methods of calculation of the settlement, one based on the CPT test and the other one on the DPT. The comparison between the predicted settlements and those computed on the basis of the oedometer test showed a good agreement which demonstrate the possbility to use the CPT and DPT tests as reliable tools of computation of foundation settlements in clayey soils.

Characterization of a carbon black rubber Poisson's ratio based on optimization technique applied in FEA data fit

  • Lalo, Debora Francisco;Greco, Marcelo;Meroniuc, Matias
    • Structural Engineering and Mechanics
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    • v.76 no.5
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    • pp.653-661
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    • 2020
  • The paper presents a study regarding rubber compressibility behavior. The objective is to analyze the effect of compression degree of rubber on its mechanical properties and propose a new methodology based on reverse engineering to predict compressibility degree based on uniaxial stretching test and Finite Element Analysis (FEA). In general, rubbers are considered to be almost incompressible and Poisson's ratio is close to 0.5. Since this property is intimately related to the rubber packing density, little changes in Poisson's ratio can lead to significant changes regarding mechanical behavior. The deviatory hyperelastic constants were obtained through experimental data fitting by least squares method for the most relevant constitutive models implemented in commercial software Abaqus, such as: Neo-Hooke, Mooney-Rivlin, Ogden, Yeoh and Arruda-Boyce, whereas the hydrostatic part was determined through an optimization algorithm implemented in the Abaqus environment by Python scripting. The simulation results presented great influence of the Poisson's ratio in the rubber specimen mechanical behavior mainly for high strain levels. A conventional pure volumetric compression test was also carried out in order to compare the results obtained by the proposed methodology.

Investigation of Membrane Fouling in Microfiltration by Characterization of Flocculent Aggregates (응집플록의 특성분석을 통하여 관찰된 정밀여과 막오염 현상에 관한 연구)

  • Choi, Yang-Hun;Kweon, Ji-Hyang
    • Journal of Korean Society of Environmental Engineers
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    • v.28 no.3
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    • pp.337-344
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    • 2006
  • Characteristics of flocculent aggregates have great effects on membrane fouling. Floc from kaolin particles gave higher permeate throughputs than floc from natural particles at the same conditions. Therefore, the objectives of this study are to thoroughly analyze characteristics of flocculated aggregates and to investigate effects of flocculated aggregates on membrane fouling. Image analysis, specific rake resistance and cake compressibility were used for characterization of flocs. Different flocculent aggregates formed with natural and kaolin particles were employed in this study. The fractal dimensions from the image analysis were $D_2=1.79{\pm}0.07$ for floc from natural particles and $D_2=1.84{\pm}0.06$ for floc from kaolin particles. The lower fractal dimension($D_2$) of floc from natural particles indicated that the aggregates were more porous and less compact than floe from kaolin particles. In addition, both the specific cake resistances and compressible degrees of flocs from natural particles showed greater values than those of flocs from kaolin particles. The results implied that the porous and loose flocs from natural particles were more easily compressed on membrane surface than the dense and compact flocs from kaolin particles. The compressed flocs yielded the great hydraulic resistances by hindering the water flow through the cake layer.

Ultrasonic Characterization of Fluid Mud: Effect of Temperature (부유퇴적물의 초음파 특징: 온도의 효과)

  • Kim, Gil-Young;Kim, Dae-Choul;Kim, Jeong-Chang
    • The Journal of the Acoustical Society of Korea
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    • v.23 no.4E
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    • pp.140-145
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    • 2004
  • A laboratory study was carried out to investigate the change of ultrasonic velocity as a function of temperature for fluid mud (i.e., suspension). Pulse transmission technique with ultrasonic wave was used for ultrasonic velocity measurement. The five samples for fluid mud were prepared for concentration range of $30.6{\%}\;(1.24\;g/cm^{3}\;in\;density),\;23.3{\%}\;(1.19\;g/cm^{3}),\;11.5{\%}(1.10\;g/cm^{3}),\;7.8{\%}\;(1.08\;g/cm^{3}),\;and\;3.8{\%}\;(1.05\;g/cm^{3})$ by weight. The ultrasonic velocity in fluid mud was investigated to increase $(approximately\;2.83\;to\;4.95\;m/s/^{\circ}C)$ with increasing temperature, due to the effect of viscosity and compressibility of water with changing temperature. But the increasing rate tends to decrease at temperature higher than $30^{\circ}C,$ caused by the effect of viscosity. The concentration of fluid mud more affect to the ultrasonic velocity at higher temperature range than that at lower temperature. Overall the temperature effect on the ultrasonic velocity in fluid mud was a similar rate as for distilled water and seawater, suggesting fluid mud significantly depends on the behavior of water.

Particle Size and Shape Analysis : The Key to Success in Metal Powder Production

  • Pankewitz, Axel;Park, Yong-Jae
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.702-703
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    • 2006
  • The particle size distribution and shape are among the important parameters for characterisation of quality of metal powders. Specific material properties such as ability to flow, reactivity as well as compressibility and its hardening potentials hence the most important characteristics of sintered metals - are determined by the size distribution and shape. The correct particle size distribution and particle shape information are the key to best product quality in atomisation processes of aluminium, milling of pure metals and other processes. This paper presents state-of-the-art technology for characterization of particle size distribution and shape.

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