• Title/Summary/Keyword: Compound distribution

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Consolidation of Thermal Electric Material Powder by MPC Process and Thermal Electric Properties (MPC 공정에 의한 열전반도체 분말의 성형 및 열전특성)

  • Yun, J.S.;Koo, J.M.;Kim, T.S.;Hong, S.J.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.454-456
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    • 2009
  • N-Type $SbI_3$ doped $95%Bi_2Te_3+5%\;Bi_2Se_3$ compounds were newly fabricated by the combination of gas atomization process and Magnetic Pulsed Compaction process. The thermoelectric properties of the MPCed bulks according to consolidation temperatures were investigated by a combination of microscopy, XRD and thermoelectric property testing. The microstructure of MPCed bulk shows homogeneous and fine distribution through consolidated bulks due to the high solidification of compound powders. The research presented the challenges toward the successful consolidation of thermoelectric powder using magnetic pulsed compaction (MPC) and analysis of thermoelectric properties of the consolidated bulks.

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Characteristics of Exfoliated Graphite Prepared by Intercalation of Gaseous SO3into Graphite

  • Lee, Beom-Jae
    • Bulletin of the Korean Chemical Society
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    • v.23 no.12
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    • pp.1801-1805
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    • 2002
  • The graphite intercalation compounds(GIC) were prepared by a dry process that led to the intercalation from the direct reaction of gaseous $SO_3$ with flake type graphite. The basal spacing of the GIC was increased from 8.3 ${\AA}$ to 12 in the gallery height. The ejection of interlayer $SO_3$ molecules by the heating for 1 minute at $950^{\circ}C$ resulted in an exfoliated graphite (EG) with surprisingly high expansion in the direction of c-axis. The expansion ratios of the exfoliated graphites were increased greatly between 220 times and 400 times compared to the original graphite particles, and the bulk density was range of 0.0053 to 0.01 $g/cm^3$, depending on reaction time. The pore size distribution of exfoliated graphite was in the range of $10-170{\mu}m$, which exhibites both mesoporosity and macroporosities. This result indicates that the direct reaction of graphite paricles with gaseous $SO_3$ can be proposed as an another route for the exfoliated graphite having excellent physical properties.

Critical Review on Evaporative Loss of Semivolatile Aerosols during Sampling

  • Kim, Seung-Won
    • Journal of Environmental Health Sciences
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    • v.36 no.3
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    • pp.171-181
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    • 2010
  • Semivolatile aerosols exist as vapor and particles at the same time in room temperature and each phase has different intake and uptake mechanisms. This characteristic requires substantial consideration during exposure assessment of semivolatile aerosol. Some sampling methods for solid particles pose high possibility of evaporative loss during sampling. Therefore, when establishing sampling strategy for them, the factors affecting the phase distribution of semivolatile aerosol should be counted including semivolatile aerosol of interest and sampling methods used. Evaluation for phase distributions of semivolatile aerosols is also recommended. Metalworking fluids, pesticides, asphalt fumes, diesel exhaust, and environmental tobacco smoke are common health-related semivolatile aerosols in workplaces.

A Study on the Optimal Design for Optical Efficiency of LED (LED의 광효율 최적설계에 관한 연구)

  • Song, Young-Jae;Hong, Min-Sung
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.3
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    • pp.361-367
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    • 2011
  • In this paper, it was attempted to analyze the optimal design of light emitting diode (LED), a source of back light unit (BLU). LED is beginning with commercialized red LED which is made by GaAsP compound semiconductor, and has been developed focusing on liquid crystal panel. In order to get the optimal design, optical simulation was made by analyzing luminosity shape, reflector angle, chip depth, and chip position of LED lighting. Final results show that the proposed LED characteristics were useful to increase light efficiency and it has been proven by distribution chart for actual exposed light on the light guide panel (LGP).

Effect of temperature gradient and residence time on droplet formation of gaseous Di-Octyl Phthalate (DOP가스의 액적형성에 미치는 온도경사 및 체류시간의 영향)

  • Lee, Myong-Hwa;Park, Byung Hyun
    • Particle and aerosol research
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    • v.6 no.1
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    • pp.1-7
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    • 2010
  • Generally, large amounts of DOP(Di-Octyl Phthalate) chemicals are used as plasticizers in PVC compound manufacturing processes. However, it is very important to collect DOP species immediately from a workplace in order to protect worker's heath and recover them. To accomplish these objectives, we need to understand the droplet formation and growth mechanisms of DOP species. In this study, two important parameters such as temperature gradient and residence time were considered to clarify these mechanisms. We found that residence time is very critical to determine the droplet size distribution of DOP, whereas temperature gradient in general operating conditions(less than $-6.8^{\circ}C/cm$) is negligible.

The Applied Technology of Mold Transformer for Outdoor Use (옥외 주상용 몰드 변압기인 적용 기술)

  • Han, Se-Won;Cho, Han-Goo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.05a
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    • pp.23-28
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    • 2000
  • Insulator systems using resin casting apparatus are useful to realize the high capacity, small size, and combined electric power equipments, and are expected to bring various advantages. In Korea, epoxy resin molded apparatus have been restricted to indoor uses till now. On the other hand, in Europe, molded insulators and transformers and so forth have been practically used since the former half of 1960's. Recently, investigation on epoxy resin materials and molded apparatus for outdoor use have ben intensively carried out. Probably, this is because electric power outdoor apparatus such as distribution transformer can be given multi-functions by using outdoor epoxy resin compound This study describes the trend on the development of epoxy mold transformers, and important technologies applied for outdoor use.

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Crystallization of Forsterite Xerogel under Carbon Dioxide: A New Crystalline Material Synthesized by Homogeneous Distribution of Carbonaceous Component into Forsterite Xerogel

  • 송미영;김수주;권혜영;박선희;박동곤;권호진;권영욱;James M. Burlitch
    • Bulletin of the Korean Chemical Society
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    • v.20 no.5
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    • pp.517-524
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    • 1999
  • By heating the magnesiumsilicate (Mg2SiO4:forsterite) xerogel in carbon dioxide, carbonaceous component was intentionally introduced into the amorphous solid precursor. Carbon was introduced homogeneously as unidentate carbonate. Upon being heated at 800 。C in carbon dioxide, the xerogel which had homogeneously distributed carbonaceous component in it crystallized into a single phase product of a new crystalline material, which had approximate composition of Mg8Si4Ol8C. The powder X-ray diffraction pattern of the new crystalline material did not match with any known crystalline compound registered in the powder diffraction file. Crystallization from amorphous xeroget to the new crystalline phase occurred in a very narrow range of temperature, from 750 。C to 850 。C in carbon dioxide, or in dty oxygen. Upon being heated above 850 。C, carbonaceous component was expelled from the product, accompanied by irreversible transition from the new crystalline material to forsterite.

Synthesis and Crystal Structure of $UP_{2}S_{6}$

  • Do, Jung-Hwan;Kim, Jung-Wook;Lah, Sang-Moo;Yun, Ho-Seop
    • Bulletin of the Korean Chemical Society
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    • v.14 no.6
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    • pp.678-681
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    • 1993
  • The new ternary phase $UP_2S_6$ has been prepared and structurally characterized. The compound is isostructural with $ZrP_2S_6$ and $ThP_2S_6$ but is different from $TiP_2S_6$. The structure has been determined by a single crystal X-ray diffraction technique. $UP_2S_6$ crystallizes in the the tetragonal system $({C^2}_{4h}-P4_2/m,\;a=6.797(7)\;{\AA},\;c=9.738(12)\;{\AA})$ with two formula units in the unit cell. The structure can be described in terms of $U^{4+}$ and ${P_2S_6}^{4-}$ ions. This hexathiohypodiphosphate anion $({P_2S_6}^{4-})$ has ideally staggered conformation. The $U^{4+}$ cation is coordinated by 8 sulfur atoms in a slightly distorted dodecahedral geometry (42m). The distribution of sulfur atoms is very well optimized for this geometry.

Compound Image Identifier Based on Linear Component and Luminance Area (직선요소와 휘도영역 기반 복합 정지영상 인식자)

  • Park, Je-Ho
    • IEMEK Journal of Embedded Systems and Applications
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    • v.6 no.1
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    • pp.48-54
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    • 2011
  • As personal or compact devices with image acquisition functionality are becoming easily available for common users, the voluminous images that need to be managed by image related services or systems demand efficient and effective methods in the perspective of image identification. The objective of image identification is to associate an image with a unique identifier. Moreover, whenever an image identifier needs to be regenerated, the newly generated identifier should be consistent. In this paper, we propose three image identifier generation methods utilizing image features: linear component, luminance area, and combination of both features. The linear component based method exploits the information of distribution of partial lines over an image, while the luminance area based method utilizes the partition of an image into a number of small areas according to the same luminance degree. The third method is proposed in order to take advantage of both former methods. In this paper, we also demonstrate the experimental evaluations for uniqueness and similarity analysis that have shown favorable results.

Study on the Protein Binding of Anti-cancer Agent, 2"-O-benzoylcinnamaldehyde, using Ultrafilteration and Flurescence Spectrometry

  • Ren , Shan;Kim, Dae-Duk;Lee, Chi-Ho
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.242.3-243
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    • 2003
  • The compound of 2"-O-benzoylcinnamaldehyde(CB-ph) is a derivative of 2"-hydroxycinnamaldehyde whcih is a methanol extract of cinnamomum cassia blume. It"s a new anti-cancer agent which has been showed to inhibit the growth of various tumor cells in vitro and in vivo. In order to investigate the effective drug concentration and bio-distribution of CB-ph, the plasma protein binding was studied. In this study, the degree of the binding of Cb-ph to various serum proteins, the binding parameters, the binding site of CB-ph in human serum albumin, and the effect of some extensive protein-binding drugs on the protein binding of CB-ph in human serum ablumin were investigated respectively by ultrafilteration and fluorescence spectrometry. (omitted)

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