• 대한치과의사협회지
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• 제11권11호
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• pp.707-710
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• 1973

The Author studied hisopathologically on the pulpal changes to the 3 kinds of Composite resin restorations in dog's teeth. The experimented materials were Blendant Adaptic and Composite. The results were as follows. 1. Inflammatory changes has been observed in all of the experimented materials. 2. Adaptic showed no cases of severe pulpal response such as highly destruction of odontoblastic layer or abscess formatoin in pulp tissues. 3. Composite induced slightly more cases of severe pulpal reaponse than other composite resins.

• 대한치과의사협회지
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• 제24권7호통권206호
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• pp.633-642
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• 1986

In order to evaluate the effects of various finishing devices (Sof-Lex disc, diamond point, rubber point, fussure bur) on the surface roughness or two composite resins (Restodent, Enamelite 500), 15 specimens for each composite resin were made in the mold. Composite resin was prepared on the mixing pad by manufacturer's direction and filled in the mold cavity. A sheet of matrix is immediately placed on it and hold for 5 minutes to polymerize the resin. Surface finish was done after 10 minutes from the start of mixing. Scanning electron microscopy and surface profilometer were used to evaluate the surface roughness, porositites and striations of dental composite resins. The following results were observed; 1. The best finished surface was formed by celluloid matrix band. 2. Rubber point was excellent polishing device for Restodent. 3. Sof-Lex disc was the device of choice for polishing Enamelite 500. 4. Different polishing methods were effective for different composite resins. 5. SEMs of variously finished surfaces supported the profilometer measurements.

• Restorative Dentistry and Endodontics
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• 제5권1호
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• pp.7-12
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• 1979

After applying three types of composite resins - Hi-Pol composite with Enamel bond, Hi-Pol composite without Enamel bond, Restodent - to the intact and the ground surface of tooth that had been acid etched for one or two minutes, the author observed the penetration of these resins into the acid etched enamel surface with scanning electron microscope. The results were as follows. 1. All the experimented materials showed the penetration into the acid etched enamel surface, and the average depth of penetration was 7 microns. 2. There was no significant difference in the penetration of these three resins despite different etching, time. 3. The grinding of the Enamel surface before acid - etching was not effective in altering the depth of penetration of these materials.

• Restorative Dentistry and Endodontics
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• 제19권2호
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• pp.513-533
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• 1994

The smooth surface after polishing of composite resin contributes to the patient's comfort, and appearance and longevity of the restoration. This study was performed for the quantitative analysis of the effects of the various finishing and polishing instruments on the surface roughness and reflectivity of the microfill, and hybrid composite resins. Cylindrical specimens 2mm thick and 10mm in diameter of Silux Plus, Durafill VS ; Z100, Prisma TPH, Brilliant, and Herculite XR composite resin were polymerized under the matrix strip. 18 specimens for each composite resin materials were divided into 6 groups ; 5 experimental groups were abraded with # 600 sand paper to remove resin-rich layer, except control. Thereafter, using diamond bur(Mani Dia-Burs), carbide bur(E. T. carbide set 4159), rubber point(Composite polishing kit), aluminum-oxide disk(Sof-Lex disk), polishing paste(Enhance system) ; each specimen was polished to its best achievable surface according to manufacturer's directions. Final polished surfaces were evaluated for the surface roughness with profilometer(${\alpha}$-step 200, Tencor instruments, USA) and for the reflectivity with image analyser(Omniment Image Analyser, Buehler, USA). The results were as follows. 1. Polishing paste or aluminum-oxide disk finish in the microfill, and hybrid composite resins was as smooth as matrix strip finish on the surface roughness test. 2. Polishing paste or aluminum-oxide disk finish in the microfill ; polishing paste finish in the hybrid composite resins was as reflective as matrix strip finish on the refectivity test. 3. For the polishing paste, there were no significant differences between the composite resin materials on the surface roughness and refectivity tests. 4. For the aluminum-oxide disk, the best result was obtained with the microfill composite resin on the surface roughness and reflectivity test. 5. Diamond bur, carbide bur, and rubber point were inappropriate for the final polishing instruments.

• 대한소아치과학회지
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• 제28권1호
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• pp.54-66
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• 2001

기존의 불소방출 복합레진보다 많은 양의 불소를 방출시키기 위해 총 복합레진 중 불소의 함량이 각각 8, 16, 24wt%가 되도록 $SrF_2$계 충진재를 첨가하여 3종의 수복용 불소방출 복합레진 시험군(VF8, VF16, VF24)을 제조하고 이에 대한 물리적 성질과 세포독성 및 불소방출량을 기존의 복합레진 제품인 Heliomolar(HE), Veridonfil(VE), Z100(ZH), Aelitefil(AE) 등의 대조군과 비교 시험하여 다음과 같은 결과를 얻었다. 1. 시험군의 3점 굽힘강도는 ZH에 비해서는 낮았으나, 다른 대조군인 AE, VE와 비슷하였고, HE보다는 우수하였으며, 시험군 간의 유의차는 없었다(p<0.05). 2. 시험군의 표면경도는 ZH보다 낮았고, AE, VE와 유사하였으며, 불소 방출 대조군인 HE보다는 높았다(p<0.05). 시험군 중에서는 VF16, VF24가 VF8에 비해 표면경도가 높았다(p<0.05). 3. 시험군의 마모도는 대조군인 HE, ZH보다 낮았으며, 시험군 중에서는 VF16, VF24가 VF8에 비해 낮은 마모도를 나타내었다(p<0.05). 4. 시험군의 물흡수도는 대조군인 HE, VE, AE와 유사하였으며 ZH보다는 낮았다(p<0.05). 시험군의 용해도는 대조군인 HE와 유의차가 없었으며, VE, ZH, AE보다 높은 용해도를 나타내었다(p<0.05). 5. 시험군은 대조군인 HE보다 $9\sim23$배 많은 양의 불소를 방출하였으며, 시험군의 불소방출량은 $SrF_2$계 충진재의 함유량과 비례하였다. 6. 시험군과 대조군은 모두 약한 정도의 세포독성을 나타내었다. 이상의 실험결과에서 $SrF_2$계 충진재를 첨가한 불소방출 복합레진 시험군의 물리적 성질과 세포독성은 기존의 복합레진과 유사한 것으로 나타났으며, 불소방출량은 기존의 불소방출 복합레진보다 현저히 높아 이차우식증에 대한 항우식효과도 높을 것으로 사료되었다.

• Restorative Dentistry and Endodontics
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• 제20권1호
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• pp.214-234
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• 1995

The purpose of this work was to study the compatibility of several commercially available dentin adhesives with composite resins. In this study, V-shaped cavity preparations were created on both buccal and lingual surfaces of 60 extracted human premolars($3mm{\times}3mm{\times}2mm$ deep). Preparations were located such that the occlusal margins were on the enamel and the gingival margins were on the cementum(1mm below the CEJ). These specimens were randomly divided into three equal groups. Three dentin adhesives(Scotchbond Multi-Purpose, All Bond 2, Prisma Universal Bond 3)were applied to the cavity in accordance with each manufacturer's instructions. The teeth in each group were restored with four composite resins(Silux plus, Z100, Bisfil, Prisma TPH) in three increments, with each increment light-cured for 40 seconds. All specimens were exposed to 500 cycles of thermal stress. Specimens then placed in a silver nitrate solution(50% by weight) and stored in darkness for 24 hours. They were then immersed for 6 hours in photographic developing solution under flourescent light. Specimens were sectioned buccolingually through the center of the restoration and observed under a binocular stereoscope. To compare the marginal leakage, ANOVA and Dunkan's multiple range tests were used in analysis. Selected samples were further studied using scanning electron microscopy(XL20, Philips, The Netherlands). The results were as follows. 1. In all groups, the enamel margin showed significantly less leakage than the cementum margin. 2. No statistically significant differences were found in microleakage when composite resins were used with their proprietary dentin adhesives. 3. In comparison between dentin adhesives, Prisma Universal Bond 3 showed significantly less leakage at the enamel margin and Scotch bond multi-purpose showed significantly less leakage at the cementum margin than the other groups. 4. In comparison between composite resins, Silux Plus showed significantly more leakage than other groups at the enamel margin and no statistically significant differences were found in microleakage at the cementum margin. 5. According to the backscattered scanning electron microscope, microleakage occurred via gaps at the dentin adhesives/dentin interface.

• 대한치과기공학회지
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• 제39권1호
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• pp.9-16
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• 2017

Purpose: The purpose of this study was to evaluate flexural strength, composite surface and fractured surface of three different indirect composite resins. Methods: Fifteen bar-shaped specimens ($25mm{\times}2mm{\times}2mm$) were fabricated for each FL group (Flow type and Light curing) and PLP group (Putty type and Light, Pressure curing) and PL group (Putty type and Light curing) according to manufacturer's instructions and ISO 10477. Fabricated specimens were stored in the distilled water for 24 hours at the temperature of $37^{\circ}C$. Three-point bending strength test was performed to measure flexural strength using universal testing machine at a crosshead speed of 1mm/min (ISO 10477). Surface and fractured surface of specimens were observed by digital microscope. Results were analyzed with Kruskal-wallis tests (${\alpha}=0.05$). Results: Mean (SD) of three different indirect composite resins were 83.38 (6.67) MPa for FL group, 139.90(16.53) MPa for PLP group and 171.72(16.74) MPa for PL group. Flexural strength were statistically significant (p<0.05). Differences were not observed at fractured surface among three groups. However, many pores over $100{\mu}m$ were observed at PL group in observing surface of specimen. Conclusion: Flexural strength of composite resins was affected by second polymerization method and content of inorganic filler.

• 대한치과의사협회지
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• 제10권12호
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• pp.785-794
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• 1972

• 대한기계학회논문집A
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• 제24권2호
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• pp.464-471
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• 2000

The fracture and wear behavior of dental composite resins containing prepolymerized particle fillers were investigated. Composite resins such as Metafil, Silux Plus, Heliomolar and Palfique Estelite were selected as specimens and contents of filler in specimens in order to evaluate the effect of prepolymerized particle fillers in fracture and wear characteristics. Ball on flat wear tester was used for the wear test at room temperature. The friction coefficient of Metafil was quite high relatively, and the wear resistances of Silux Plus and Palfique Estelite were better than those of Metafil and Heliomolar at the same experimental condition. It was found that the main wear mechanism was abrasive wear containing of plastic deformation of dental material.

• Restorative Dentistry and Endodontics
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• 제16권2호
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• pp.197-212
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• 1991

The purpose of this study was to roughness on the polished surface of visible light composite resins and was to observe the polished surfaces under Scanning Electrom Microscope(ISI DS 130 AKASHI Co. JAPAN). The surface roughness tester(Surfcom 700A Seimtsu profilometer Tokyo, Japan) was used to measure roughness of polished surfaces. In this study, 5 brands of visible of composite resins were examined, Pyrofile light bond Anterior Lite fil anterior Photo clearfil anterior & posterior Palfique light Anterior and posterior Silux Anterior. White point, Silicure point, Super snap Sof-Lex medium disk as cutting instrument, and celluloid matrix were used. The results obtained were as follows. 1. The Celluloid matrix produced the smoothest surfaces. 2. The surfaces made by Soflex medium disk was smoother than the surfaces made by any other polishing instruments. 3. The values of surface roughness made by White point, Silicon point and Super snap were similer. 4. Palfique light (AP) visible light composite resin showed the smoothest surface after polishing with Silicone point, Super snap disk and Soflex mediuem disk in all tested materials.