• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.24-28
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• 2002

Composite reinforced fiber materials are used in lots of fields such as a part of aeronautic space, ship, machinery and so on because can make structure wished for necessary condition by control fiber direction and laminated sequence. As the use of advanced composites increase, specific techniques have been developed to repair changed composite structures. In order to repair the damaged part production high quality composite reinforced fiber are completed by control the surrounding temperature and press in autoclave. The quality is influenced heat exposure degree by chemical reaction for precessing. This study considerated influence limit of using by repair structure part and change of properties according to heat exposure degree for repairing.

• Carbon letters
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• v.7 no.4
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• pp.241-244
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• 2006

Carbon/Carbon composite was been manufactured by the technology of warmer-molding process of clutter chopped carbon fiber, using phenolic resin as an adhesive. The degree of graphitization, the microstructure and the friction properties were studied. The results show that the clutter chopped carbon fiber fully scatter in the Carbon/Carbon composite and the degree of graphitization of phenolic resin can reach up to 86.2%, this matrix carbon can form the continuous and stable graphitic thin film on the friction surface during braking process so that the composite has fine friction properties and low wear rate.

• Advances in concrete construction
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• v.3 no.1
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• pp.71-90
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• 2015

In order to investigate the feasibility and advantage of tuff used as pozzolan in cement-based composite, the representative specimens of tuff were collected, and their chemical compositions, proportion of vitreous phase, mineral species, and rock structure were measured by chemical composition analysis, petrographic analysis, and XRD. Pozzolanic activity strength index of tuff was tested by the ratio of the compression strength of the tuff/cement mortar to that of a control cement mortar. Pozzolanic reaction degree, and the contents of CH and bond water in the tuff/cement paste were determined by selective hydrochloric acid dissolution, and DSC-TG, respectively. The tuffs were demonstrated to be qualified supplementary binding material in cement-based composite according to relevant standards. The tuffs possessed abundant $SiO_2+Al_2O_3$ on chemical composition and plentiful content of amorphous phase on rock texture. The pozzolanic reaction degrees of the tuffs in the tuff/cement pastes were gradually increased with prolongation of curing time. The consistency of CH consumption and pozzolanic reaction degree was revealed. Variation of the pozzolanic reaction degree was enhanced with the bond water content and relationship between them appeared to satisfy an approximating linear law. The fitting linear regression equation can be applied to mutual conversion between pozzolanic reaction degree and bond water content.

• Restorative Dentistry and Endodontics
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• v.21 no.2
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• pp.642-651
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• 1996

The purpose of this study was to evaluate the relationship between monomer compositions and the changes in the degree of conversion in the various layers of composites after additional heat curing. Four types of composites and 3 types of inlay ovens were used in this study. Composite was placed in a 4-mm thick teflon mold, and light cured from the top for 60 seconds. Ten samples were prepared for each composite ; 5 of these were additionally heat cured in an inlay oven as the manufacturer recommended. After light curing or light and heat curing, the samples were sectioned into four parts and assigned to groups A, B, C, or D according to their distance from the light source. These sections were then thinned to 50-$70{\mu}m$, and these wafers were analyzed with a Fourier Transform Infrared Spectrometer(FI-IR) to determine the degree of conversion. A standard baseline technique was used to calculate the degree of conversion. $^{13}C$ NMR spectra of bis-GMA, TEGDMA and bis-EMA, were acquired using a Varian Gemini spectrometer operated at 200 MHz. $CDCl_3$ solvent was used for qualitative analysis. The degree of conversion was affected by bis-GMA : TEGDMA ratio but it seemed to be also affected by other factors. When the composites were heat cured, significant increases in the degree of conversion were noted throughout the samples, but the amount of increase differed between materials. Thus, clinical performance of a heat-treated composite inlay may be different depending on materials.

• The Journal of Korean Academy of Prosthodontics
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• v.26 no.1
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• pp.85-98
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• 1988

The primary aim of this study was to access the degree of marginal leakage in composite resin inlay restorations. Class V cavities were prepared on sixty extracted premolars. They were classified as control group and experimental group 1, 2 and each group was filled with BIS-FIL $I^{(R)}$ and $Silux^{(R)}$ composite resins. In the control group, the composite resin was inserted directly, the experimental group 2 was inserted as composite resin inlay after heat treatment on $125^{\circ}C$, 10 minutes. Then thermocycling was performed 1000 times. After staining with 1% Basic Fuchsin, they were cut in Buccolingual direction and the degree of penetration of the dye was examined under L/M. The following results were obtained : 1. In occlusal margin area, difference in marginal leakage was not observed in all groups. 2. In gingival margin area, cavities filled with composite resin inlay was less marginal leakage than filled directly in BIS-FIL $I^{(R)}$ group, and statistical significant difference was not existed in $Silux^{(R)}$ group. 3. The statistical significance was not existed between composite resin inlay and composite resin inlay heated secondarily. 4. In all groups, gingival margin area reveals more marginal leakage than occlusal margin area and statistical significance was existed.

• Restorative Dentistry and Endodontics
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• v.20 no.2
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• pp.827-831
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• 1995

This study was designed to etermine the changes in the degree of conversion for composite resins after heat curing following the methods proposed by Lee & Park(1995). 8-mm diameter hole was made in 1mm teflon plate and one of three types of composites (Charisma, Brilllant, Z100) was placed and light cured for 60seconds. The samples were devided into 3 groups according to the placing composites. After light curing, the samples were separated from the moulds. Using this method, 10 samples were prepared in each group; 5 samples from each group were heat cured according to the methods proposed by manutfactures, These samples were then thinned to 50-$70{\mu}m$ and analysed with a Fourier Transform Infrared Spectrometer. Standard baseline technique was used to calculate the degree of conversion. When the samples were light cured, the degrees of conversion in each groups were 47.1 % (charisma), 53.3% (Z100), and 70.1 % (Brilliant). The degree of conversion after heat curing were; 60.1 % (Charisma), 71.1 % (Z100), and 73.3 % (Brillant). Once the samples were heat cured, there were significant increases in degree of conversion.

• Computers and Concrete
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• v.29 no.3
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• pp.127-144
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• 2022

To investigate the flexural stiffness of the steel-composite beam, the contributions of the concrete slab and steel beam to the stiffness were considered separately. The method for flexural stiffness of the composite beam, considering the stiffness of the concrete slab and steel beam, was proposed in this paper. In addition, finite element models of the composite beams were established and validated. Parametric analyses were carried out to study the effects of different parameters on the neutral axis distance reduction factors of the concrete slab and steel beam. Afterward, the neutral axis distance reduction factors were fitted, and the stiffness combination coefficients of the two parts were solved. Based on the stiffness combination coefficients, the flexural stiffness of the composite beam can be obtained. The proposed method was validated by the tested and analyzed results. The method has a simple form and high accuracy in predicting the flexural stiffness of the steel-concrete composite beam, even though the degree of shear connection is less than 0.5.

• Steel and Composite Structures
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• v.49 no.1
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• pp.19-30
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• 2023

Steel-concrete composite slabs represent a very efficient floor solution combining the key performance of two different materials: the steel and the concrete. Composite slab response is governed by the degree of the interaction between these two materials, mainly depending by chemical and mechanical bond. The latter is characterized by a limited degree of confinement if compared with the one of the rebars in reinforced concrete members while the former is remarkably influenced by the type of concrete and the roughness of the profiled surface, frequently lubricated during the cold-forming manufacturing processes. Indeed, owing to the impossibility to guarantee a full interaction between the two materials, a key parameter governing slab design is represented by the horizontal shear-bond strength, which should be always experimentally estimated. According to EC4, the design of the slab bending resistance, is based on the simplified assumption that the decking sheet is totally yielded, i.e., always in plastic range, despite experimental and numerical researches demonstrate that a large part of the steel deck resists in elastic range when longitudinal shear collapse is achieved. In the paper, the limit strain for composite slab, which corresponds to the slip, i.e., the debonding between the two materials, has been appraised by means of a refined numerical method used for the simulation of experimental results obtained on 8 different composite slab types. In total, 71 specimens have been considered, differing for the properties of the materials, cross-section of the trapezoidal profiled metal sheets and specimen lengths.

• Restorative Dentistry and Endodontics
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• v.25 no.1
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• pp.17-40
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• 2000

Resin cements are used for cementing indirect esthetic restorations such as resin or porcelain inlays. Because of its limitations in curing of purely light cured resin cements due to attenuation of the curing light by intervening materials, dual cured resin cements are recommended for cementing restorations. The physical properties of resin cements are greatly influenced by the extent to which a resin cures and the degree of cure is an important factor in the success of the inlay. The purpose of this study was to evaluate the influence of porcelain thickness and exposure time on the polymerization of resin cements by measuring the microhardness and the degree of conversion, to investigate the nature of the correlation between two methods mentioned above, and to determine the exposure time needed to harden resin cements through various thickness of porcelain. The degree of resin cure was evaluated by the measurements of microhardness [Vickers Hardness Number(VHN)] and degree of conversion(DC), as determined by Fourier Transform Infrared Spectroscopy(FTIR) on one light cured composite resin [Z-100(Z)] and three dual cured resin cements [Duo cement(D), 3M Resin cement(R), and Dual cement(DA)] which were cured under porcelain discs thickness of 0mm, 1mm, 2mm, 3mm with light exposure time of 40sec, 80sec, 120sec, and regression analysis was performed to determine the correlation between VHN and DC. In addition, to determine the exposure time needed to harden resin cements under various thickness of porcelain discs, the changes of the intensity of light attenuated by 1mm, 2mm, and 3mm thickness of porcelain discs were measured using the curing radiometer. The results were obtained as follows ; 1. The values of microhardness and the degree of conversion of resin cements without intervening porcelain discs were 31~109VHN and 51~63%, respectively. In the microhardness Z was the highest, followed by R, D, DA. In the degree of conversion, D and DA was significantly greater than Z and R(p<0.05). 2. The microhardness and the degree of conversion of the resin cements decreased with increasing thickness of porcelain discs, and increased with increasing exposure time, D and R showed great variation with inlay thickness and exposure time, whereas, DA showed a little variation. 3. The intensity of light through 1mm, 2mm, and 3mm porcelain inlays decreased by 0.43, 0.25, and 0.14 times compared to direct illumination, and the respective needed exposure times are 53 sec, 70 sec, and 93 sec. In D and R, 40 sec of light irradiation through 2mm porcelain disc and 80 sec of light irradiation through 3mm porcelain disc were not enough to complete curing. 4. The microhardness and the degree of conversion of the resin cements showed a positive correlationship(R=0.791~0.965) in the order of R, D, Z, DA. As the thickness of porcelain discs increased, the decreasing pattern of microhardness was different from that of the degree of conversion, however.

• Membrane and Water Treatment
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• v.4 no.2
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• pp.83-93
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• 2013

In the present investigation, were synthesized composite membranes prepared by simultaneous casting of two polymer solutions using the technique of phase inversion by immersion / precipitation. The support layer was prepared using polyethersulfone and polysulfone as base polymer and for the top layer was used sulfonated polysulfone (SPSU) with 50% sulfonation degree. The morphology of the resulting membranes were characterized by scanning electron microscopy (SEM). The final results showed that it is possible to prepare composite membranes by simultaneous casting of two polymer solutions with adherence between the two layers. Regarding the permeation tests, the developed membranes presented values of hydraulic permeability within the range of commercial nanofiltration (NF) membranes. Values rejection of 80% ammonium ions can be increased by using a SPSU with a greater degree of sulfonation.