• 제목/요약/키워드: Complex Samples Analysis

검색결과 443건 처리시간 0.026초

노인의 인지기능과 구강건강상태의 관련성: 고령화연구패널조사(Korean Longitudinal Study of Aging)를 중심으로 (Relevance between cognitive function and oral health status in the elderly: Focusing on Korean Longitudinal Study of Aging)

  • 김인자;문희정
    • 한국치위생학회지
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    • 제22권5호
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    • pp.333-340
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    • 2022
  • Objectives: This study aimed to confirm the association between cognitive function and oral health status in the elderly. Methods: In this study, 5,794 respondents, aged 55 or older, who had participated in the 7th aging research panel survey were used. Statistical analyses were performed using a complex samples cross-tabulation analysis, complex samples general linear model, and a complex sample multinomial logistic regression analysis. Results: After analyzing the cognitive function of the elderly according to their oral health conditions, it was found that suspicions of dementia (19.6%) and cognitive function decline (25.9%) were more common for those who wore dentures than for those who did not wear dentures (p<0.001). Compared to those who did not wear dentures, those who wore dentures were linked to a 1.665 times higher suspicion of dementia (p<0.001). In comparison, cognitive decline was 0.964 times lower when the number of natural teeth increased by 1, and it was 0.941 times lower when the oral health evaluation index for the elderly increased by 1 point (p<0.001). Conclusions: As a result of this study, it was confirmed that cognitive function and oral health status are related in the elderly. Therefore, systematic measures for oral health management and oral health promotion should be prepared in tandem with awareness of possible cognitive decline in the elderly.

무기안료를 함유한 도료의 금속 원소 분석에 의한 유해성 분류에 관한 연구 (A Study on Hazard Classification by Metal Element analysis of Paints Containing Inorganic Pigment)

  • 한정희;이도희;이나루
    • 한국산업보건학회지
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    • 제34권3호
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    • pp.193-201
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    • 2024
  • Objectives: Paints contain various types of metal substances. However, our review of MSDS (Material Safety Data Sheets) for paints found that their components were often kept secret or exact content information was otherwise not provided. We analyzed the metal elements in various inorganic pigment-based paints available in South Korea in this study and checked whether they contain hazardous metal substances as defined by the Occupational Safety and Health Acts. We investigated issues of health hazard classification related to the metal elements. The study is intended to contribute to strengthening the management of hazardous substances by suggesting improvements to MSDS. Methods: We randomly selected 19 samples that were predicted to contain hazardous inorganic pigments after reviewing MSDS among paints currently in use. The samples were analyzed using XRF (X-ray Fluorescence spectrometry), ICP_OES (Inductively Coupled Plasma-Optical Emission Spectroscopy) and SP-ICP-MS (Single Particle-ICP-Mass Spectroscopy). Results: The most common elements in the samples were Al (aluminum), Fe (iron), Ti (titanium), Ca (calcium), and Si (silica). One sample contained more lead than allowed by the limits. There were ten samples that could potentially contain nanoforms, seven samples that contained titanium dioxide, and six samples that contained complex inorganic color pigments (CICPs). Conclusions: Inorganic pigments in paints should be evaluated for hazards separately from other metallic compounds and reflected in the MSDS because they have different characteristics than other metallic compounds. These include particle size, crystal structure, and complex substances. The results of this study can be helpful for determining whether a paint contains sufficient hazardous metal compounds to affect its classification, and it can be a guideline for improving MSDS through comparative review and rationalization with the manufacturer's MSDS. This would make it possible to contribute to the management of chemical substances in the workplace through the proper MSDS disclosure of paints.

Fault Diagnosis Method Based on High Precision CRPF under Complex Noise Environment

  • Wang, Jinhua;Cao, Jie
    • Journal of Information Processing Systems
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    • 제16권3호
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    • pp.530-540
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    • 2020
  • In order to solve the problem of low tracking accuracy caused by complex noise in the fault diagnosis of complex nonlinear system, a fault diagnosis method of high precision cost reference particle filter (CRPF) is proposed. By optimizing the low confidence particles to replace the resampling process, this paper improved the problem of sample impoverishment caused by the sample updating based on risk and cost of CRPF algorithm. This paper attempts to improve the accuracy of state estimation from the essential level of obtaining samples. Then, we study the correlation between the current observation value and the prior state. By adjusting the density variance of state transitions adaptively, the adaptive ability of the algorithm to the complex noises can be enhanced, which is expected to improve the accuracy of fault state tracking. Through the simulation analysis of a fuel unit fault diagnosis, the results show that the accuracy of the algorithm has been improved obviously under the background of complex noise.

창원지역 지하수의 수질특성

  • 김무진;함세영;황한석;성익환
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2001년도 총회 및 춘계학술발표회
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    • pp.191-193
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    • 2001
  • This paper presents the result of groundwater analysis in Changwon area and the characteristics of the groundwater properties. Changwon city conducted groundwater analysis at 551 sites in 1996 and 1997. The water quality is suitable as groundwater use at 466 sites (84.6 %) and exceeds maximum contaminant levels (MCLs) at 85 sites (15.4 %). Major contaminants are total bacteria, coliform and nitrate-N. DNAPLs, e.g. TCE and PCE are detected in the areas of industrial complex and residence. The detection of TCE and PCE is due to organic solvents from manufacturing companies. They are also derived from laundries, Photographer's studios, septic tanks, etc. In addition, fifty groundwater samples were analyzed. Iron, manganese, zinc, copper, lead, aluminum and fluorine are detected in nearly all the groundwater samples. The groundwaters shown on the Piper diagram mostly belong to Ca-HCO$_3$ type.

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Streaming potential and groundwater contamination

  • Baker Simon S.;Cull James P.
    • 지구물리와물리탐사
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    • 제7권1호
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    • pp.41-44
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    • 2004
  • Measurements of streaming potential can provide a means for the detection and quantification of contaminants in groundwater prior to remediation. However, laboratory determinations of specific electrolyte properties are required for an adequate analysis of the hydraulic gradient in complex situations. Data obtained for the King River in Tasmania confirm a linear relationship linking streaming potential data and hydraulic gradients. Laboratory samples at low concentration (0.001M KCl) indicate values in the range 20-80 mV/cm of water pressure, while for higher concentrations (0.01M KCl) values are less than 25 mV/cm. Similar ion concentrations are observed in the King River, consistent with field correlations indicating values for streaming potential close to 15 mV/cm. In-situ fluid samples are required for more detailed analysis of local anomalies that may be associated with variations in recharge and migration of contaminants.

Analyses of phenolics in cigarette smoke by GC-MS with the multiple ion selction technique

  • Park, Jeen-Woo
    • Archives of Pharmacal Research
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    • 제5권2호
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    • pp.71-77
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    • 1982
  • Improvements in the analytical methodology used in the gas chromatographic/mass spectral analysis of phenolic compounds from cigarette smoke are described. For the direct analysis of crude samples, pyridine extraction and the glass capillary column GC was used for the separation of phenolics as trimethylsilyl derivativatives. The separations of cigarette smoke on Carbowax 20M and SE-54 wall coated open tubular columns are given. Improved methodology for the routine quantitation of the identified components using the computer-controlled multiple ion selection technique of MS presented. Considerations pertaining to routine analyses of a multitude of complex smoke samples are also discussed.

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Tween80 미셀 용액에서 Ni(Ⅱ)의 분광광도법 정량 (Spectrophotometric Determination of Nickel (Ⅱ) in Tween80 Micellar Medium)

  • 이승권;최희선
    • 대한화학회지
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    • 제44권3호
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    • pp.207-211
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    • 2000
  • Tween80 미셀용액에서 착화제로서 APDC틀 이용하여 Ni(II)를 정량하는 방법에 대해 연구하였다. Ni(PDC)$_2$ 착물의 홉수 스펙트럼 chloroform에서 보다는 Tween80에서 더 좋은 모양과 더 좋은 감도를 보여 주었다. Ni(PDC)$_2$ 착물은 pH 7.0에서 그리고 100분 정도까지 매우 안정하였으며, APDC를 Ni(II)의 몰수의 10배 이상 넣어 주면 정량적으로 착물이 형성되었다. Tween80의 농도는 0,1%가 적절하였고,0.1% Tween80 용액에서 Ni(PDC)$_2$ 착물의 검정곡선은 좋은 직선성(R2=0.9955)을 보여주었다. 이 분석법의 검출한계와 정량한계는 각각 0.09 ${\mu}g$/mL와 0.28${\mu}g$/mL이었으며, 강물시료에 적용한 회수율은 100% 보다 조금 크게 나타났다. 비록 여러 금속이온들이 방해를 하지만, 실제시료에 들어있는 Ni(II)을 정량하는데 이용할 수 있을 것이다.

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공공임대주택에 거주중인 노령인구 인지특성에 관한 연구 (A Study on the Older Residents' Cognitive Characteristics of Public Rental Housing Complex)

  • 오예인;정다운;권순정
    • 의료ㆍ복지 건축 : 한국의료복지건축학회 논문집
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    • 제24권4호
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    • pp.17-25
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    • 2018
  • Purpose: Korean society is undergoing the rapid increase and poverty of elderly population. Therefore, the appropriate supply and planning of public rental housing for the low-income elderly is more important. The purpose of this study is to present the basic data for the study and planning of the elderly housing complex by analyzing the cognitive characteristics of the elderly residing in the rental housing. Methods: A questionnaire survey was conducted to identify health characteristics of the elderly living in the 'Gongreung SH Apartment'. 100 random samples were collected and 82 valid samples were analysed. Statistical analysis was performed using Excel and R for the age, sex, health, outdoor walking frequency and characteristics of Cognitive map of the elderly. Results: The characteristics of cognitive map were classified into point shapes and linear shapes. The linear group was lower in average age than the point group and tended to draw the map wider. The wider the map was, the more the number of elements in cognitive map was. The number of elements on the cognitive map decreased as respondents' age increased. On the other hand it was not related to residence period and gender of the elderly. Implication: The cognitive extent of the residential environment tends to decrease with age. Men's cognitive range is wider than women's. There is no corelation between the number of cognitive elements and cognitive map type. Men tend to have a systematic image of city, whereas women focus on relational and social urban factors. For sustainable apartment complex design, various characteristics of the group including men and women, different age and different health status should be considered.

Fluorometric Quantitative Analysis of Al(III) Ion Using 5-Methoxy-2-phenyliminomethylphenol

  • Kim, Sun-Deuk;Lee, Hye-Won
    • Bulletin of the Korean Chemical Society
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    • 제30권5호
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    • pp.1026-1030
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    • 2009
  • A novel Schiff base ligand (N, O system) 5-methoxy-2-phenyliminomethylphenol ($5-CH_3O-PMP$) was synthesized. Using the synthesized ligand as a fluorescent reagent, a fluorometric method was developed for the quantitative analysis of Al(III) ion. The quantitative analysis of Al(III) ion was performed by making the complex compound between Al(III) ion and $5-CH_3O-PMP$ in ethanol-water solution (85/15, v/v, pH 6.2). The excitation wavelength (${\lambda}em$) of the complex compound was 397 nm while the emmision wavelength (${\lambda}em$) was 498 nm. The quantitative analysis of Al(III) ion was carried out by estimating the fluorescence intensity. The various calibration curves were used for the quantitative analysis in the range of 0.27$\sim$27 ng/mL Al(III) ion concentrations. The detection limit was 0.027 ng/mL. Using the fluorometric method developed in this study, satisfying results were obtained from various samples such as tap water, hot spring water, river water, sea water and waste water, which contained considerable amounts of interfering ions.

Investigation of Partial Least Squares (PLS) Calibration Performance based on Different Resolutions of Near Infrared Spectra

  • Chung, Hoe-Il;Choi, Seung-Yeol;Choo, Jae-Bum;Lee, Young-Il
    • Bulletin of the Korean Chemical Society
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    • 제25권5호
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    • pp.647-651
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    • 2004
  • Partial Least Squares (PLS) calibration performance has been systematically investigated by changing spectral resolutions of near-infrared (NIR) spectra. For this purpose, synthetic samples simulating naphtha were prepared to examine the calibration performance in complex chemical matrix. These samples were composed of $C_6-C_9$ normal paraffin, iso-paraffin, naphthene, and aromatic hydrocarbons. NIR spectra with four different resolutions of 4, 8, 16, and 32$cm^{-1}$ were collected and then PLS regression was performed. For PLS calibration, five different group compositions (such as total paraffin content) and six different pure components (such as benzene concentration) were selected. The overall results showed that at least 8$cm^{-1}$ resolution was required to resolve the complex chemical matrix such as naphtha. It was found that the influence of resolution on the PLS calibration was varied by the spectral features of a component.