• Title/Summary/Keyword: Compaction pressure

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Preparation of High Purity Si Powder by SHS (자전 연소 합성법에 의한 고순도 실리콘 분말제조)

  • Shin, Chang-Yun;Min, Hyun-Hong;Yun, Ki-Seok;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.44 no.2 s.297
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    • pp.93-97
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    • 2007
  • High purity Si powder was prepared in the system of $SiO_2-Mg$ combustion reaction. Various conditions of combustion reaction and leaching were investigated. As the particle size of Mg decreased and the compaction pressure increased the quantity of the unreacted power was decreased. In the acid leaching of MgO, increasing particle size, reaction temperature, rotating speed and reaction time made leaching effect low. Final Si powder produced by combustion and leaching reaction, has a high purity of 99.9% with irregular shape.

Development and characterization of graphite reinforced conductive polymer composites for PEMFC bipolar plates (고분자전해질 연료전지용 흑연계 복합소재 분리판 개발)

  • Heo Seongil;Yun Jincheol;Oh Kyeongseok;Han Kyungseop
    • 한국신재생에너지학회:학술대회논문집
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    • 2005.06a
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    • pp.248-251
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    • 2005
  • Graphite reinforced conductive polymer composites for PEMFC bipolar plates were fabricated by the compression molding technique. Graphite powder was mixed with an phenol resin to impart electrical property in composites. In this study, conductive polymer composites with high filler $loadings(>60wt.\%)$ were manufactured to accomplish high electrical conductivity above 100S/cm. The level of compaction is important because graphite powder increase electrical conductivity of composites by direct physical contact between particles. The optimum molding pressure according to filler was proposed experimentally. Various tests(electrical conductivity, flexural strength, compressive strength, leach test, etc) were carried out to verify the performance of fabricated composites for PEMFC bipolar plates. Fabricated composites have good electrical conductivity and mechanical strength. The results of leach test and contact angle measurement showed similar characteristics compared with commercial bipolar plates.

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Fabrication and Dynamic Consolidation Behaviors of Rapidly Solidified Mg Alloy Powders (급속응고 Mg 합금분말의 제조 및 동적성형특성)

  • Chae, Hong-Jun;Kim, Young-Do;Kim, Taek-Soo
    • Journal of Powder Materials
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    • v.18 no.4
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    • pp.340-346
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    • 2011
  • In order to improve the weak mechanical properties of cast Mg alloys, Mg-$Zn_1Y_2$ (at%) alloy powders were synthesized using gas atomization, a typical rapid solidification process. The powders consist of fine dendrite structures less than 3 ${\mu}m$ in arm spacing. In order to fabricate a bulk form, the Mg powders were compacted using magnetic pulse compaction (MPC) under various processing parameters of pressure and temperature. The effects of the processing parameters on the microstructure and mechanical properties were systematically investigated.

Three Dimensional Finite Element Analysis for Powder Forging Process (분말단조 공정의 3차원 유한요소해석)

  • 김형섭
    • Journal of Powder Materials
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    • v.3 no.2
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    • pp.104-111
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    • 1996
  • In order to obtain homogeneous and high quality products in powder compaction forging process, it is very important to control stress, strain, density and density distributions. Therefore, it is necessary to understand quantitatively the elasto-plastic deformation and densification behaviors of porous metals and metal powders. In this study, elasto-plastic finite element method using Lee-Kim's pressure dependent porous material yield function has been used for the analysis of three dimensional indenting process. The analysis predicts deformed geometry, stress, strain and density distribution and load. The calculated load is in good agreement with experimental one. The calculated results do not show axisymmetric distributions because of the edge effect. The core part which is in contact with the indentor and the outer diagonal edge part are in compressive stress states and the middle part is in tensile stress state. As a results, it can be concluded that three dimensional analysis is more realistic than axisymmetric assumption approach.

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Dynamic Analysis of an Immersed Tunnel using an Effective Stress Model (유효응력모델을 이용한 침매터널의 동적거동 해석)

  • Park, Sung-Sik;Moon, Hong-Duk
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.03a
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    • pp.51-58
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    • 2008
  • The George Massey immersed tunnel passes the Fraser River near Vancouver, Western Canada. In this paper, dynamic analysis of the tunnel on sandy soils was performed using an effective stress constitutive model called UBCSAND. This model is able to calculate pore pressure rise and resulting tunnel deformation due to cyclic loading. Centrifuge tests conducted at RPI are used to verify the model performance. Centrifuge tests consist of 3 models: Model 1 is designed for an original ground condition, Model 2 for a ground improvement by compaction method, Model 3 for a ground improvement by gravel drainage. The results of centrifuge Model 1 are presented and compared with predictions of UBCSAND model. This model well captured the results of centrifuge test and therefore can be used to predict dynamic behavior of similar tunnels or underground structures on sandy soils.

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Influence of Pile Cap On The Behaviors of End Bearing Pile Groups (말뚝캡이 선단지지 무리말뚝의 지지거동에 미치는 영향)

  • 최영석;이수형;정충기;김명모
    • Proceedings of the Korean Geotechical Society Conference
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    • 2000.11a
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    • pp.245-252
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    • 2000
  • Model tests on free standing pile groups and piled footings with varying a pile spacing in two layered soils are carried out. The influence of pile cap on the behaviors of end bearing pile groups is analyzed by comparing the bearing behavior in piled footings with those in a single pile, a shallow footing(cap alone) and free standing pile groups. From the test results, it is found that the bearing characteristics of cap-soil-pile system are related with load levels and pile spacings. Before yield, the bearing resistance by cap is not fully mobilized, however, as the applied load increases, the bearing resistance of cap approaches to that of cap alone and settlement hardening occurs after yield due to the compaction caused by the contact pressure between cap and soil. By the cap-soil-pile interaction, shaft friction and point resistance of piles considerably increase with dependency of pile spacings. In two layered soil, the increasing effect of dilatancy in dense sandy soil adjacent to pile tips, increases the point resistance of pile.

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In-Situ Measurement of Densification Behavior of Nano Cu Powders during Sintering (In-Situ 측정에 의한 나노 Cu 분말의 소결 공정 시 치밀화 거동)

  • Yoon, S.C.;Bok, C.H.;Kwak, E.J.;Rhee, C.K.;Kim, H.S.
    • Transactions of Materials Processing
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    • v.16 no.3 s.93
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    • pp.210-214
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    • 2007
  • Manufacturing bulk nanostructured materials with least grain growth from initial powders is challenging because of the bottle neck of bottom-up methods using the conventional powder metallurgy via compaction and sintering. In the study, densification behavior of nano Cu powders during pressureless sintering was investigated using an in-situ optical dilatometer technique. The initial heating and steady temperature stages during the sintering of nano Cu powder compacts were observed. At the initial heating stage, the powder compact has many porosities and full densification needs high temperature and/or high pressure sintering. In the experimental analysis, changes in geometry and density were measured and discussed for optimal consolidation and densification by the in-situ optical dilatometer.

Yield Surface and Hardening Laws of Unsaturated Clayey Soils for Isotropic Compression (불포화 점성토의 등방압축 상태에서 발생하는 항복곡면과 경화감수)

  • 송창섭
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.39 no.1
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    • pp.93-101
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    • 1997
  • This paper presents yield surfaces and hardening laws for describing the state of an unsaturated soil under isotropic compression and suction changes. The yield surface is formulated within the framework of hardening plasticity using two independent sets of stress variables : the excess of total stress over air pressure and the suction. And the application of the yield surfaces and hardening laws are confirmed from the result of the experiment. To this end a series of suction-controlled isotropic tests are conducted on clayey soils. Matric suction is controlled by the axis translation technique using high air entry ceramic disk. The specimens are compacted using a half of Proctor compaction energy with 5 % lower of water content than the optimum moisture contents. From test results, existence of the yield surfaces and an application of hardening laws to samples are confirmed by comparison between test and predicted results. And it is confirmed that LC yield locus is extened with the total plastic deformations induced by suction or stress changes, however, SI yield locus is only extended with the plastic deformations by induced suction changes.

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Geotechnical Characteristics of Major Earth and Rockfill Dams in Korea (우리나라 주요 록휠 댐의 지반공학적 특성)

  • 유태성
    • Proceedings of the Korean Geotechical Society Conference
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    • 2002.10a
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    • pp.3.2-27
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    • 2002
  • This paper presents the status of dam construction in Korea, along with a brief assessment of the dam design and construction practice. The assessment is based on publically available design and construction records of the major existing rockfill dams which have been constructed since early 1970's, and focussed in identifying geotechnical characteristics of design and construction parameters of the dams. Though the assessment, two representative dams, having unique geotechnical characteristics, are selected for comprehensive comparison of their geotechnical engineering behavior during construction and operation. The comparison yields very interesting findings on the effects of various design and construction parameters on dam behavior.

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Various Master Sintering Curve Concepts and its Applications

  • Park, Seong-Jin;Blaine, Deborah C.;German, Randall M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.66-67
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    • 2006
  • The master sintering curve (MSC) is derived from densification data over a range of heating rates and temperatures. To improve the accuracy, several modifications were proposed: multi-phase MSC for solid state sintering with phase changes, MSC for liquid phase sintering, and MSC with consideration of grain growth. The developed MSC models were applied to several material systems such as molybdenum, stainless steels, and tungsten heavy alloys (WHA), in order to evaluate the effect of compaction pressure, phase change, grain growth, and composition on densification, to classify regions having different sintering mechanism, and to help engineer design, optimize, and monitor sintering cycles.

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