• 제목/요약/키워드: Characterisation

검색결과 124건 처리시간 0.024초

Synthesis of Silicon Carbide Nanowhiskers from Coconut Fibres and Sol-Gel Derived Silica

  • Raman, V.;Bhatia, G.;Mishra, A.;Saha, M.;Sengupta, P.R.;Srivastava, A.K.
    • Carbon letters
    • /
    • 제7권3호
    • /
    • pp.166-170
    • /
    • 2006
  • Silicon carbide whiskers ($SiC_w$) having the diameter in the range of 20-80 nm were synthesised from coconut fibres through sol-gel process. The coconut fibres were impregnated with tetraethoxysilane and methyltriethoxysilane derived sol and pyrolyzed at $1400^{\circ}C$ in argon. X-ray of the pyrolyzed samples showed the formation of ${\beta}$-SiC.

  • PDF

Validation of Radioanalytical Techniques for Nuclear Waste Characterisation

  • Warwick, Phillip E.
    • 방사성폐기물학회지
    • /
    • 제17권4호
    • /
    • pp.363-373
    • /
    • 2019
  • Waste characterisation associated with nuclear site decommissioning relies on radiochemical analysis of a diverse range of sample types, requiring extensive validation of analytical techniques using matrix-matched materials. The absence of relevant reference materials has hindered robust method development and validation. The paper discusses how method validation in support of nuclear waste characterisation can be achieved without using reference materials. The key stages in an analytical procedure are evaluated and a multi-stage approach is proposed with the ultimate aim of determining an operational envelope for an analytical procedure.

Dynamic characterisation of a two-link flexible manipulator: theory and experiments

  • Khairudin, M.;Mohamed, Z.;Husain, A.R.;Mamat, R.
    • Advances in robotics research
    • /
    • 제1권1호
    • /
    • pp.61-79
    • /
    • 2014
  • This paper presents theoretical and experimental investigations into the dynamic modelling and characterisation of a two-link flexible manipulator incorporating payload. A planar two-link flexible manipulator that moves in a horizontal plane is considered. A dynamic model of the system is developed using a combined Euler-Lagrange and assumed mode methods, and simulated using Matlab. Experiments are performed on a lab-scaled two-link flexible manipulator for validation of the dynamic model and characterisation of the system. Two system responses namely hub angular position and deflection responses at both links are obtained and analysed in time and frequency domains. The effects of payload on the dynamic characteristics of the flexible manipulator are also studied and discussed. The results show that a close agreement between simulation and experiments is achieved demonstrating an acceptable accuracy of the developed model.

Engineered Surfaces Part 1. - A Philosophy of Manufacture

  • Stout, Kenneth. J.
    • Journal of Mechanical Science and Technology
    • /
    • 제14권1호
    • /
    • pp.72-83
    • /
    • 2000
  • In recent years considerable progress has been made in the characterisation of surface finish in three dimensions, and in the development of protocols which can be used for international standardisation. Although the subject as it has currently developed has much further to go if the process of surface characterisation is to impact on manufacture, control and specification of the manufacturing process itself. Researchers in this important area are beginning to realise that if the subject is to have great impact on manufacturing industries, surface characterisation must be broadened to include measures of surface integrity of the component and in addition be related to the functional demands imposed on the surface. The functional demands being a requirement of the engineering situation in which the components are employed. If these three factors are considered simultaneously, surface characterisation, surface integrity and component function, then a new and important subject is born, the subject of the Engineered Surface. Part 1 of this paper attempts to draw together the elements which go together to create the subject, 'The Engineered Surface'. The paper presents a method by which this important subject can be developed to the benefit of manufacturing industries. The paper also discusses the importance of a co-ordinated approach to the subject and the way that information can be documented to eventually provide a useful atlas of controlling parameters which are essential for a range of material processing industries as they strive to meet the ever more stringent and cost effective requirements of the manufacture.

  • PDF

Characterisation and Durability of a Vitrified Wasteform for Simulated Chrompik III Waste

  • Walling, Sam A.;Gardner, Laura J.;Pang, H.K. Celine;Mann, Colleen;Corkhill, Claire L.;Mikusova, Alexandra;Lichvar, Peter;Hyatt, Neil C.
    • 방사성폐기물학회지
    • /
    • 제19권3호
    • /
    • pp.339-352
    • /
    • 2021
  • Legacy waste from the decommissioned A-1 nuclear power plant in the Slovak Republic is scheduled for immobilisation within a tailored alkali borosilicate glass formulation, as part of ongoing site cleanup. The aqueous durability and characterisation of a simulant glass wasteform for Chrompik III legacy waste, was investigated, including dissolution experiments up to 112 days (90℃, ASTM Type 1 water). The wasteform was an amorphous, light green glassy product, with no observed phase separation or crystalline inclusions. Aqueous leach testing revealed a suitably durable product over the timescale investigated, comparing positively to other simulant nuclear waste glasses and vitreous products tested under similar conditions. Iron and titanium rich precipitates were observed to form at the surface of monolithic samples during leaching, with the formation of an alkali deficient alteration layer behind these at later ages. Overall this glass appears to perform well, and in line with expectations for this chemistry, although longer-term testing would be required to predict overall durability. This work will contribute to developing confidence in the disposability of vitrified Chrompik legacy wastes.

Radioactive waste sampling for characterisation - A Bayesian upgrade

  • Pyke, Caroline K.;Hiller, Peter J.;Koma, Yoshikazu;Ohki, Keiichi
    • Nuclear Engineering and Technology
    • /
    • 제54권1호
    • /
    • pp.414-422
    • /
    • 2022
  • Presented in this paper is a methodology for combining a Bayesian statistical approach with Data Quality Objectives (a structured decision-making method) to provide increased levels of confidence in analytical data when approaching a waste boundary. Development of sampling and analysis plans for the characterisation of radioactive waste often use a simple, one pass statistical approach as underpinning for the sampling schedule. Using a Bayesian statistical approach introduces the concept of Prior information giving an adaptive sample strategy based on previous knowledge. This aligns more closely with the iterative approach demanded of the most commonly used structured decision-making tool in this area (Data Quality Objectives) and the potential to provide a more fully underpinned justification than the more traditional statistical approach. The approach described has been developed in a UK regulatory context but is translated to a waste stream from the Fukushima Daiichi Nuclear Power Station to demonstrate how the methodology can be applied in this context to support decision making regarding the ultimate disposal option for radioactive waste in a more global context.

Processing and Characterisation of Bulk Melt-Textured YBCO Monoliths and Function Elements

  • Habisreuther, T.;Zeisberger, M.;Litzkendorf, D.;Surzhenko, O.;Kracunovska, S.;Bierlich, J.;Kosa, J.;Vajda, I.;Gawalek, W.
    • Progress in Superconductivity
    • /
    • 제6권1호
    • /
    • pp.1-6
    • /
    • 2004
  • Melt-textured YBCO in high quantity and good quality is prepared in a batch process. A mean trapped field >1. IT at 77K is achieved in batch processed material. Studying the microstructure is a necessary tool to understand the growth mechanisms and thus to opimise the material. From the growth induced structures in the material the anisotropy in growth speed is 1.37. From batch processed material function elements for different cryomagnetic applications are constructed. Motors with an output power > 200 kW at 77 K and bearings that can lift more than 200 kg were equipped with melt-textured YBCO.

  • PDF

Towards A Dichotomy for the List Switch Homomorphism Problem for Signed Graphs

  • Hyobeen Kim;Mark Siggers
    • Kyungpook Mathematical Journal
    • /
    • 제63권3호
    • /
    • pp.355-372
    • /
    • 2023
  • We make advances towards a structural characterisation of the signed graphs H for which the list switch H-colouring problem List-S-Hom(H) can be solved in polynomial time. We conjecture two different characterisations, the second refining the first, in the case that the graph H can be switched to a graph in which every negative edge is also positive. Using a recent proof of the first characterisations for reflexive signed graphs, by Bok et. al., we prove the second characterisation for reflexive signed graphs. We also provide several tools for reducing the problem to the bipartite case, and prove a full complexity dichotomy for a related problem.