• Title/Summary/Keyword: Ceramic matrix

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Morphology Development of HAp Crystallites in GEL Matrix

  • Chang, Myung-Chul
    • Journal of the Korean Ceramic Society
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    • v.44 no.3 s.298
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    • pp.133-136
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    • 2007
  • The crystal morphology of hydroxyapatite [HAp] phase in gelatin [GEL] matrices was investigated with the condition of a GEL precursor treatment in an aqueous solution of $H_{3}PO_{4}$ at $37-80^{\circ}C$. Needle-shaped nanocomposite particles were prepared through a dynamic reaction during a coprecipitation process using a phosphoric GEL solution. Various types of mineralized morphology appeared with a phosphorylated condition of the GEL solution. HAp/GEL nanocomposite slurries showed the existence of an octacalcium phosphate [OCP] phase during the process.

Microstructure Control of Sr-Ferrite by Seed Addition (Seed 첨가에 의한 Sr-Ferrite의 미세구조 제어)

  • 박준홍;신효순;이병교
    • Journal of the Korean Ceramic Society
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    • v.32 no.1
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    • pp.90-94
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    • 1995
  • In Sr-ferrite system, it has been attempted to inhibit the abnormal grian growth using Sr-ferrite powders synthesized by molten salt method as the matrix and the seeds, respectively. At each sintering temperature, the addition of seed more than 15% suppressed the abnormal grain growth, and the uniform microstructure resulted. Particularly, at 12$25^{\circ}C$, it was observed that the maximum number of the abnormal grain growth nuclei was achieved since the abnormal grain growth was suppressed even by the addition of 10% seed.

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Influence of Particle Size of Quartz on the Strength of Porcelain Body (자기질 요지의 강도에 미치는 석영입도의 영향)

  • 이은상;김진영
    • Journal of the Korean Ceramic Society
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    • v.21 no.3
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    • pp.209-216
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    • 1984
  • The influence of the particle size of quartz and the change of cooling rate to the strength of conventional triaxial porcelain was studied, . The results indicate that 1. The residual quartz content was increased by particle size increasing. And the strength was increased by increas-ing residual quartz content which increased the total stress in the specimen. But the influence of residual quartz was lessened by the extent of crack between quartz particle and glass matrix 2. In order to increase the strength of the body fast cooling is suitable to small quartz particle and slow cooling is suitable to large quartz particle.

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Characteristics of Carbon Fiber Composites for the Application of Smart Sensor (I) (스마트 센서로의 적용을 위한 탄소섬유 복합체의 특성평가 (I))

  • 김유택
    • Journal of the Korean Ceramic Society
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    • v.38 no.1
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    • pp.52-55
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    • 2001
  • Polyacrylonitrile(PAN)-based 탄소섬유와 epoxy resin matrix 내에 장착된 PAN-based 탄소섬유의 전기저항을 탄소섬유와 파괴될 때까지 인장강도를 증가시키며 측정하였다. 탄소섬유가 끊어져 측정 계기가 open-circuit을 나타내기 전까지 탄소섬유의 전기저항 값은 strain이 증가할수록 증가하였으며, epoxy resin은 탄소섬유의 저항값 측정에 거의 영향을 미치지 않았다. 탄소섬유의 저항값 변화는 strain에 대해 정확도 1% 이내로 예측(calibrate)할 수 있었으며 재현성 또한 우수하였다. 따라서 탄소섬유는 재료의 기계적 강도를 증가시키기 위해 사용될 수 있을 뿐만 아니라 구조재료의 파괴를 예측할 수 있는 스마트 센서로서도 사용할 수 있다는 가능성을 확인하였다.

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Preparation and Property of Ceramic/Polymer 3-3 Composites with Matrices (각종 Matrix를 이용한 Ceramic/Polymer 3-3 Composies의 제작 및 특성)

  • Park, J.H.;SaGong, G.
    • Proceedings of the KIEE Conference
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    • 1993.07b
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    • pp.1122-1124
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    • 1993
  • In this study, piezoceramics/polymer composites with 3-3 connectivity were made by BURPS(Burnout Plastic Sphere) technique with PZT ceramics and PVA sphere. And physical and dielectric properties dependent on the PVA wt.% were investigated. The density of porous piezoceramic and pieaoceramic/polymer composites were decreased almost linearly with increasing the PVA wt.%.

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Rotor Dynamics Analysis of a Spindle System for a High speed Grinding Machine (고속 연삭기 주축 시스템의 회전체 역학 해석)

  • 최영휴
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2000.04a
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    • pp.714-719
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    • 2000
  • This paper describes a transfer matrix approach to analyze the dynamics of a high sped flexible rotor system supported at 2 positions by five ceramic bearings. The rotor system is modelled as lumped parameters in which many factors are considered not only lumped inertia or mass, bending moment, shear force but also gyroscopic effect and unbalance. The equation of motion is derived in the transfer matrix form, from which the eigenvalues equation is also derived. The transfer natural frequencies and modes. The eigenvalues, eigenmodes, campbell diagram, whirling critical speed, whirling modes, and the response of unbalance are calculated and discussed.

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Wear Characteristics of Particulate Reinforced Metal Matrix Composites Fabricated by a Pressureless Metal Infiltration Process (무가압함침법으로 제조된 입자강화 금속복합재료의 마모특성)

  • 김재동;정순억;김형진
    • Journal of Ocean Engineering and Technology
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    • v.17 no.1
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    • pp.55-60
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    • 2003
  • The effect of size and volume fraction of ceramic particles, with sliding velocity on the wear properties were investigated for the metal matrix composites fabricated by the pressureless infiltration process. The metal matrix composites exhibited about 5.5 - 6 times the wear resistance compared with AC8A alloy at high sliding velocity, and by increasing the particle size and decreasing the volume fraction, the wear resistance was improved. The wear resistance of metal matrix composites and AC8A alloy exhibited different aspects. Wear loss of AC8A alloy increased with sliding velocity, linearly : whereas, metal matrix composites indicated more wear loss than AC8A alloy at the slow velocity region. However, a transition point of wear loss was found at the middle velocity region, which shows the minimum wear loss. Further, wear loss at the high velocity region exhibited nearly the same value as the slow velocity region. In terms of wear mechanism, the metal matrix composites generally exhibited abrasive wear at slow to high sliding velocity; however, AC8A alloy showed abrasive wear at low sliding velocity and adhesive and melt wear at high sliding velocity.

Wear Characteristics of Particulate Reinforced Metal Matrix Composites Fabricated by Pressureless Metal Infiltration Process (무가압함침법으로 제조된 입자강화 금속복합재료의 마모특성)

  • Kim, Jae-Dong;Jung, Sun-Uk;Kim, Hyung-Jin
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2002.10a
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    • pp.379-384
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    • 2002
  • The effect of size and volume fraction of ceramic particles with sliding velocity on the wear properties were investigated for the metal matrix composites fabricated by pressureless infiltration process. The particulate metal matrix composites exhibited about 5.5 - 6 times of excellent wear resistance compared with AC8A alloy at high sliding velocity, and as increasing the particle size and decreasing the volume fraction the wear resistance was improved. The wear resistance of metal matrix composites and AC8A alloy exhibited different aspects. Wear loss of AC8A alloy increased with sliding velocity linearly. whereas metal matrix composites indicated more wear loss than AC8A alloy at slow velocity region, however a transition point of wear loss was found at middle velocity region which show the minimum wear loss, and wear loss at high velocity region exhibited nearly same value with slow velocity region. In terms of wear mechanism, the metal matrix composites exhibited the abrasive wear at slow to high sliding velocity generally, however AC8A alloy showed abrasive wear at low sliding velocity and adhesive and melt wear at high sliding velocity.

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THERMAL EFFECTS ON THE STRAIN ENERGY RELEASE RATE FOR EDGE DELAMINATION IN CRACKED LAMINATED COMPOSITES

  • Soutis, C.;Kashtalyan, M.
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2001.04a
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    • pp.1-6
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    • 2001
  • In this paper, edge delaminations in cracked composite plates are analytically investigated. A theoretical model based upon a sub-laminate approach is used to determine the strain energy release rate, $G^{ed}$, in [$\pm$$\theta_m$/$90_n$]$_s$ carbon/epoxy laminates loaded in tension. The analysis provides closed-form expressions for the reduced stiffness due to edge delamination and matrix cracking and the total energy release rate. The parameters controlling the laminate behaviour are identified. It is shown that the available energy for edge delamination is increased notably due to transverse ply cracking. Also thermal stresses increase substantially the strain energy release rate and this effect is magnified by the presence of matrix cracking. Prediction for the edge delamination onset strain is presented and compared with experimental data. The analysis could be applied to ceramic matrix composite laminates where similar mechanisms develop, but further experimental evidence is required.

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Material Characteristics and Clay Source Interpretation of the Ancient Ceramic Artifacts from the Wonsinheungdong Site in Daejeon, Korea (대전 원신흥동 유적 출토 고대 세라믹 유물의 재료학적 특성과 원료의 산지해석)

  • Kim, Ran-Hee;Jung, Hae-Sun;Jung, Sang-Hoon;Lee, Chan-Hee
    • Journal of Conservation Science
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    • v.27 no.2
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    • pp.163-179
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    • 2011
  • This study was to identify the material characteristics and provenance of the crucibles, potteries and roof tiles from the Wonsinheungdong site in Daejeon, Korea. Similar mineral composition of each samples showed by microscopic observation and X-ray diffraction analysis. However, wall thickness and mineral characterization of each ceramic artifacts are quite different. The pottery is characterized by thin wall with 0.5 to 0.7 cm and fine grained clay matrix. While the crucible and roof tile has thick wall with 1.3 to 2.5 cm, poorly sorted texture of many quarz, orthoclase and plagioclase whithin ceramic fabric. And large elonagated voids formed by hydrocarbone of straw during the firing and loose matrix obseved in crucible. All ceramic samples and ground soil of the site show similar mineralogical characteristics geochemical behavior and clay-mineralization degree. This indicates making that the soil is probable to be a raw material of all ceramic from the Wonsinheungdong site. Also, firing temperature of most ceramic artifacts are estimated as 850 of all ceramic from the Wonsinheungdong site. Also, firing temperature of most ceramic artifacts are estimated as 850 to $950^{\circ}C$ but hardest pottery fired high temperature between 1,050 to $1,150^{\circ}C$. The vitreous molten materials interpreted in slag included segregation of copper and tin. But it can not exclude the possibility that the glass molten material because observed reddish and greenish vitreous fine structure under microscopic.