• 제목/요약/키워드: Capillary method

검색결과 507건 처리시간 0.024초

식육중 Chlorfluazuron의 잔류분석법 및 잔류량에 관한 연구 (Studies on the Analytical Methods and Quantity of Residual Chlorfluazuron in Meat)

  • 박건상;홍무기;백선영;정병곤;박종세
    • 한국식품위생안전성학회지
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    • 제12권4호
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    • pp.288-293
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    • 1997
  • Analytical method using capillary GC/ECD was developed to determine trace residues of chlofluazuron, 1-[3, 5-dichloro-5-trifluoromethyl-2-pyridyloxy)phenyl]-3-(2, 6-difiuorobenzoyl), in meat, and applied to analyze the residues in domestic and imported meats. The analytical scheme developed does not require column chromatographic cleanup; chlorfiuazuron was extracted with diethyl ether and petroleum ether (50: 50), partitioned against acetonitrile, cleaned up with silica Sep-Pak cartridge, identified GC/ECD, and comfirmed by GC/MS. The mean recoveries of the pesticide in meat fortified with standard solution 0.1, 0.5, 0.1 mg/kg were ranged from 82 to 95%. The limit of detection and limit of quantitation were 0.001 and 0.005 mg/kg, respectively. Chlorfluazuron residues were not found in domestic samples, but found in imported Australian beef ranging from 0.02 to 0.17 mg/kg, detected by 18% among the samples.

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Furnace Atomizer를 이용(利用)한 미량혈액중(微量血液中) Pb검출(檢出)에 관(關)한 연구(硏究) (Lead Determinaiton in $25{\mu}l$ Whole Blood Sample by Atomic Absorption Spectrophotometer with Furnace Atomizer)

  • 김형석;박양원;구도서
    • Journal of Preventive Medicine and Public Health
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    • 제15권1호
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    • pp.111-114
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    • 1982
  • To determine Pb level in blood, we usually .used to pull out about 5ml blood from venous vessel and this sample was digested with acids to decompose organic matter and then determined the Pb contents by Atomic Absorption Spectrophotometer with flame. But recent trend in quan titating Pb in small amount of sample is very much recommended in clinical chemistry specially pediatrics, and industrial hygiene and occupational health area. Authors tried to determine Pb contents in small amount blood of $25{\mu}l$ by using capillary tube method and got the possibility of determination of ng amount of Pb in $25{\mu}l$ whole blood sample without any pretreatment of sample.

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Capillary Hysteresis Model in Unsaturated Flow : State of the Art

  • Park, Chan-Kun;Sonu, Jun-Ho
    • Korean Journal of Hydrosciences
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    • 제4권
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    • pp.33-49
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    • 1993
  • The Purpose of this study is to classify existing hysteresis models and to discuss a possibility of a new type of the hysteresis model. The existing hysteresis models are classified into three types: the interpolation model, the scaling model and the domain model, of which only domain model is to simulate hysteresis curves based on the theoretical approach, It is useful to develop a hysteresis model that requires only one branch of hysteresis curves for the model calibration because obtaining hysteresis curves by experiments is expensive and time-concept by many investigators, however their models are not successful to accurately simulate real data of Rubicon Sandy Loam and Dune Sand. There is a possibility that a new model is based on the dependent domain concept considering the weighting factor, $P_a$($\theta$), which accounts for the pore blockage effect against air entry. Conclusively, a new model where the weighting factor $P_a$($\theta$) in Model III-1 (Mualem, 1984) reduces to a known variable through an appropriate method is an alternative model which required only one branch of main curves for the model calibration.

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박막펌핑을 이용한 Nano Fountain-Pen의 유동 특성에 관한 수치적 연구 (Numerical Analysis of the Flow Characteristics in the Nano Fountain-Pen Using Membrane Pumping)

  • 이진형;이영관;이석한;김훈모;김윤제
    • 한국유체기계학회 논문집
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    • 제9권2호
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    • pp.19-24
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    • 2006
  • Nano fountain-pen is a novel device to make the constant patterning in micro process using new designed probe. Fountain-pen nanolithography (FPN) is applied for constant supply of liquid in conjunction of patterns and surface variation in the micro process. In this study, nuo fountain-pen is composed with reservoir, micro channels, tip and scondary chamber. Instead of traditional method only using capillary force, liquid can be definitely and exactly injected with membrane pumping by the repulse force of tip. It is dfficult to perform experiments in the micro range so that we carried out a numerical analysis for internal flow, using a commercial code, FlUENT, The velocity, pressure and flow rate are obtained under laminar, unsteady, three-dimensional incompressible flow with no-slip condition, and results are graphically described.

DIP 기법과 전기비저항을 이용한 불포화토의 포화도 예측 (A Prediction of Degree of Saturation using DIP and Electrical Resistivity)

  • 임동기;민덕기;신호성
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2010년도 추계 학술발표회
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    • pp.1177-1181
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    • 2010
  • Unsaturated soil can describe soil particles, air-water and contact face between air and water. The providing a simple method to predict water content in Geotechnical mechanics is very important. In this experiment, DIP (Digital Image Processing) and electrical resistivity techniques were used simultaneously to predict the saturation degree, and the results of two techniques will be compared each other to get conclusion. The experiment was carried out for Jumunjin standard sand. The picture of experimental column of soil and water was taken at different times, then using DIP technique to measure Color number-the height of capillary in soil column. At the same time, measure electrical resistivity of the soil.

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유연하고 신속한 표면미세가공기술을 이용한 Micro-fluidic Channel 제작 (Fabrication of Micro-fluidic Channels using a Flexible and Rapid Surface Micro-machining Technique)

  • 김진산;성인하;김대은
    • 한국공작기계학회논문집
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    • 제11권4호
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    • pp.97-101
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    • 2002
  • Recently, the need for transporting and manipulating minute amount of fluids in microscale channels (so-called micro-fluidics) has been increasing, especially in biotechnology and biochemical processing. This work demonstrates that the so-called mechano-chemical process which consists of mechanical abrasive action combined with chemical process can be used to f뮤ricate micro-fluidic channels more rapidly and cost effectively than other methods. In this work, capillary filling of fluids in micro-channels was investigated by theoretical approaches and experiments. From the experimental results, it is expected that a complex micro-fluidic system can be fabricated using the micro-fabrication technique and microsystem packaging method described in this work.

마이크로채널 전사성 향상을 위한 사출성형공정 최적화 기초연구 (An Experimental Study on the Transcription Characteristics of Injection-Molded Micro Channel)

  • 김종선;고영배;민인기;유재원;김종덕;윤경혼;황철진
    • 소성∙가공
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    • 제15권9호
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    • pp.692-696
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    • 2006
  • Micro fabrication of polymeric materials becomes increasingly important. And it is considered as a low-cost alternative to the silicon or glass-based Micro Electro-Mechanical System(MEMS) technologies. In the present study, micro channels were fabricated via LiGA(Lithographie, Galvanoformung, Abformung) process used for Capillary Electrophoresis(CE) chip. Taguchi method was applied to investigate the effects of process conditions in injection molding(melt temperature, injection speed, mold temperature and packing pressure) on the transcription characteristics of the micro channel. It was found that the skin layer disturbs a formation of micro channel. Furthermore, mold temperature and injection speed were two important factors to affect the replication characteristics of micro channel.

稀搏溶液에서의 Polymer의 機械的 切斷. 混合溶媒의 영향 Ⅱ (Mechanical Degradation of Polymers in Dilute Solution. The Influence of the Mixed Solvents II.)

  • 원영무
    • 대한화학회지
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    • 제16권1호
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    • pp.50-55
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    • 1972
  • The mechanical degradation of $poly(\alpha-methyl$ styrene) in several mixed solvents (chlorobenzene-n-butyl alcohol, chlorobenzene-sec-butyl alcohol, chlorobenzene-Kerosene, chlorobenzene-methylketone) was studied using the capillary flow method. The velocity constant of scission reaction (K) and the limited degree of polymerization (g) were compared at the same value of [${\eta}$], which is considered as the parameter of molecular dimension of polymers in solution. As results, (K) did not change much, even if the species and the volume fraction of poor(non-) solvents changed, while the value of (g) changed according to the species of poor (non-) solvents and the value of [${\eta}$] these results were discussed.

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능동제어모세관을 이용한 유정압테이블의 운동정도 향상

  • 송영찬;박천홍;김수태
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1997년도 춘계학술대회 논문집
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    • pp.250-256
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    • 1997
  • For compensating the error motion of hydrostatic tables, we have introduced a way that the clarance of table is actively controlled corresponding to the amount of error with the nariable capillary,anmed as ACC. In previous paper,through the basic test, it was confirmed that by the use of ACC,the error motion within 2.7 .mu.m of a hydrostatic table could be compensated with the resolution of 27nm, 1/100 contollable range, and with the freqency bandwidth of 5.5Hz structurally. In this paper,we performed practital compensation of the linear and angular motion error of hydrostatic table using ACC. For improving the compensated motion accuracy,iterative control method is put into the control system. The experimental results show that by the simultaneous compensation of error,the linear and angular motion error are improved upto 0.25 .mu.m and 0.4arcsec,which are about 1/10 and 1/3 of the non-compensated motion errors respectively.

Investigation on the Flow Field Characteristics of a Highly Underexpanded Pulsed Plasma Jet

  • Kim, Jong-Uk;Kim, Youn J.
    • Journal of Mechanical Science and Technology
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    • 제15권12호
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    • pp.1691-1698
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    • 2001
  • In recent years, significant progress has been made in modeling turbulence behavior in plasma and its effect on transport. It has also been made in diagnostics for turbulence measurement; however, there is still a large gap between theoretical model and experimental measurements. Visualization of turbulence can improve the connection to theory and validation of the theoretical model. One method to visualize the flow structures in plasma is a laser Schlieren imaging technique. We have recently applied this technique and investigated the characteristics of a highly underexpanded pulsed plasma jet originating from an electrothermal capillary source. Measurements include temporally resolved laser Schlieren imaging of a precursor blast wave. Analysis on the trajectory of the precursor blast wave shows that it does not follow the scaling expected for a strong shock resulting from the instantaneous deposition of energy at a point. However, the shock velocity does scale as the square root of the deposited energy, in accordance with the point deposition approximation.

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