• 한국수소및신에너지학회논문집
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• 제33권6호
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• pp.684-691
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• 2022

Hydrogen fuel cell electric vehicles are typically refueled at a wide range of temperatures (-40℃ to 85℃) in the hydrogen refueling station in accordance with the worldwide accepted standard. Currently, there is no traceable method by which to verify and calibrate the hydrogen flowmeters to be used at hydrogen refueling stations except for a water calibration process as a conventional method. KRISS hydrogen field test standard based on the gravimetric principle was developed to verify the measurement accuracy of the mass flowmeter to be used at hydrogen refueling stations for the first time in Korea.

• 천문학회보
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• 제45권1호
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• pp.66.4-67
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• 2020

Gyeonggi science high school for the gifted (GSHS) installed 60cm telescope, which is waiting for student observers. It is essential to understand the characteristics of the photometric system, consisting of telescope, filter, and CCD, to get reliable data. CCD images of SA98 Landolt standard field and M67 were obtained on 19th March 2020. The images of each field were combined by filters, i.e., we ignored the monochromatic atmospheric extinction since the photometric objects themselves are standard stars. 24 standard stars in SA98 field and 12 standard stars in M67 were used to derive the tentative transformation equation between our bv photometric system and Johnson BV photometric system. In this poster, we present the preliminary standardization result for Johnson BV photometric system in GSHS 60cm telescope. The reproductivity is discussed by comparing color coefficients of two fields. We plan to extend this process to Johnsons-Cousins BVRI photometric system and narrow-band filters for flux calibration.

• 생약학회지
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• 제54권1호
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• pp.38-43
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• 2023

A simple and accurate assay was developed for the quantitative analysis of 1-deoxynojirimycin (1-DNJ) derived from the silkworm (Bombyx mori). Normal-phase high-performance liquid chromatography coupled with an evaporative light scattering detector (HPLC-ELSD) and a hydrophilic interaction liquid chromatography column was used. Various parameters were applied to optimize the analysis method. The limits of detection and quantification of 1-DNJ were 2.97 × 10^-3 and 9.00 × 10^-3 mg/mL, respectively. The calibration curve showed good linearity results. The concentration range and the r² value were 0.0625-1.0 mg/mL and 0.9997, respectively. The accuracy test demonstrated a significantly high recovery rate (89.95-103.22%). The relative standard deviation was ≤ 1.00%. Thus, a method for the accurate identification and quantitative analysis of 1-DNJ in silkworms was developed. Moreover, in this procedure, the process of derivatization of 1-DNJ, which was required in previous experiments, could be eliminated. This technique may be actively utilized for the development of pharmaceuticals and health functional foods using 1-DNJ.

• 분석과학
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• 제36권6호
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• pp.281-290
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• 2023

Zidovudine is an antiretroviral agent prescribed for the prevention and treatment of human immunodeficiency virus/acquired immune deficiency syndrome (HIV/AIDS). It is typically recommended to be used in combination with other antiretroviral drugs. Zidovudine has the potential to generate N-nitrosodimethylamine (NDMA) in the presence of dimethylamine and nitrite salt under acidic reaction conditions during the drug manufacturing process. NDMA is a potent human carcinogen that may be detected in drug substances or drug products. An analytical method was developed to determine NDMA in pharmaceuticals including zidovudine using high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS). The analysis involved reversed-phase chromatography on a Kinetex F5 column with a mobile phase comprising water-acetonitrile mixtures. The detection of positively charged ions was conducted using atmospheric pressure chemical ionization (APCI). The calibration curve demonstrated excellent linearity (r = 0.9997) across the range of 1-50 ng/mL with a highly sensitive limit of detection (LOD) at 0.3 ng/mL. The developed method underwent thorough validation for specificity, linearity, accuracy, precision, robustness, and system suitability. This sensitive and specific analytical method was applied for detecting NDMA in zidovudine drug substance and its formulation currently available in the market, indicating its suitability for drug quality management purposes.

• International Journal of Naval Architecture and Ocean Engineering
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• 제6권2호
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• pp.459-470
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• 2014

During ship design, welding-induced distortions are roughly estimated as a function of the size of the component as well as the welding process and residual stresses are assumed to be locally in the range of the yield stress. Existing welding simulation methods are very complex and time-consuming and therefore not applicable to large structures like ships. Simplified methods for the estimation of welding effects were and still are subject of several research projects, but mostly concerning smaller structures. The main goal of this paper is the application of a multi-layer welding simulation to the block joint of a ship structure. When welding block joints, high constraints occur due to the ship structure which are assumed to result in accordingly high residual stresses. Constraints measured during construction were realized in a test plant for small-scale welding specimens in order to investigate their and other effects on the residual stresses. Associated welding simulations were successfully performed with fine-mesh finite element models. Further analyses showed that a courser mesh was also able to reproduce the welding-induced reaction forces and hence the residual stresses after some calibration. Based on the coarse modeling it was possible to perform the welding simulation at a block joint in order to investigate the influence of the resulting residual stresses on the behavior of the real structure, showing quite interesting stress distributions. Finally it is discussed whether smaller and idealized models of definite areas of the block joint can be used to achieve the same results offering possibilities to consider residual stresses in the design process.

• 한국산학기술학회논문지
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• 제14권7호
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• pp.3127-3134
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• 2013

본 연구는 DME 연료를 사용할 수 있도록 변경된 엔진의 제어 알고리즘, 로직구성 및 차량상태에서 검증결과를 나타낸 것으로써, 제어구조 및 자동코드 생성기법에 의한 제어로직 설계과정과 제어 맵을 소개하고 최종적으로 제어의 신뢰성 및 성능을 검증한 것이다. 제어구조는 운전자 요구를 엔진발생토크로 구현하기위한 분사제어부와 배기가스 및 동력특성을 만족시키기 위한 공기제어 시스템부로 크게 구성되며, 제어로직은 제어응답성을 향상시키기 위하여 각 제어 기능별로 앞먹임 및 뒤먹임 제어부로 설계되었고, 앞먹임 제어부의 제어 맵은 엔진모델을 이용하여 생성한 뒤, 이를 엔진 및 차량 시험과정에서 보정하였다. 개발된 제어기를 장착하여 차량 시험모드를 완주하였으며, EGR, VGT 및 분사시기 보정에 의하여 배출가스 저감효과를 확인하였다.

• 대한화학회지
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• 제58권3호
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• pp.283-288
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• 2014

A column solid phase extraction procedure based on modified polyurethane foam (PUF) by a newly synthesized Schiff base ionophore, named 2,2'-{iminobis[propane-3,1-diylnitrilo(1E)prop-1-yl-1-ylidene]}diphenol, was developed for preconcentration step of trace amounts determination of copper ions in water samples by atomic absorption flame spectroscopy. The influence of parameters on the adsorption process such as sample pH, amount of modified PUF packed in the column, type and volume of stripping reagent and its flow rate were investigated and optimized. Under optimum experimental conditions, the calibration graph was linear in a relatively wide range ($0.005-210{\mu}g/ml$) with a limit of detection $0.002{\mu}g/ml$ of copper. The proposed method allows achieving to a concentration factor of >133. The capacity of a column (1.6 cm i.d.) packed by 6 g of PUF modified by 12 mg of the Schiff base was found to be $247.7({\pm}2.1){\mu}g$ of copper. It was found that the adsorption process was highly selective towards copper ions with respect to some associated metal ions. The presented procedure was successfully applied for determination of copper in some water samples.

• 대한기계학회논문집B
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• 제29권9호
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• pp.1022-1031
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• 2005

Temporal behavior of the laser induced incandescence (LII) signal is often used for soot particle sizing, which is possible because the cooling behavior of a laser heated particle is dependent on the particle size. In present study, LII signals of soot particles are modeled using two non-linear coupled differential equations deduced from the energy- and mass-balance of the process. The objective of this study is to obtain an appropriate calibration curve for determining primary particle size by comparing the gated signal ratio and double-exponential curve fitting methods. Not only the effects of laser fluence and gas temperature on the cooling behavior but also heat transfer mechanisms of heated soot particle have been investigated. The second-order exponential curve fitting showed better agreements with the LII signals than the gated signal ratio method which was based on the lust-order exponential curve fit. And the temporal decay rate of the LII signal and primary particle size showed nearly linear relationship, which was little dependent on the laser fluence. And it also could be reconfirmed that vaporization was dominant process of heat loss during first loons after laser pulse, then heat conduction played most important role while thermal radiation had little influence all the time.

• 한국컴퓨터그래픽스학회논문지
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• 제22권4호
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• pp.1-9
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• 2016

본 논문은 빛을 이용한 영상 투사 매체인 프로젝터와 사용자의 신체를 인식하는 키넥트 센서를 이용하여 움직이는 사람의 손에 영상을 프로젝션 매핑하는 시스템 개발을 제안한다. 기존 프로젝션 매핑은 고정된 물체에 영상을 투사하는 경우가 대부분이지만, 본 시스템은 움직이는 손을인식해 손바닥의 중심점에 영상을 투사하여 사용자에게 새로운 인지 경험을 제공하기 위해 개발되었다. 본 논문에서는 시스템 제작 과정과 이를 기반으로 제작된 콘텐츠와 응용 예에 대해 설명한다. 하드웨어구성과 조립방법을 구체적으로 제시하고객체지향개발 방법을 통한 오픈 소프트웨어 구조 개발과정에 대해 자세히 서술한다. 안정적인 사영을위해 3차원 공간상에서 프로젝터와 키넥트 센서 좌표 캘리브레이션, 그리고 키넥트 센서 좌표 노이즈, 손떨림으로 인해 발생하는 노이즈 감소 방법을 실험 결과와 함께 제시한다.

• 한국군사과학기술학회지
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• 제23권6호
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• pp.639-649
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• 2020

Air data systems measure airspeed, pressure altitude, angle of attack and angle of sideslip. These measurements are essential for operating flight control laws to ensure safe flights. Since the loss or corruption of air data measurements is considered as catastrophic, a high level of operational reliability needs to be achieved for air data systems. In the case of unmanned air vehicles, failure of any of air data sensors is more critical due to the absence of onboard pilot decision aid. This paper presents design of a dual redundancy air data system and the integration process for an unmanned air vehicle. The proposed dual-redundant architecture is based on two independent air data probes and redundancy management by central processing in two independent flight control computers. Starting from unit testing of single air data sensor, details are provided of system level tests used to meet overall requirements. Test results from system integration demonstrate the efficiency of the proposed process.