• Title/Summary/Keyword: CVI process

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Nicalon-Fiber-Reinfored SiC Composites Via Infiltration (Infiltration 공정으로 제조한 Nicalon 섬유강화 SiC 복합재료)

  • 김민수;김영욱;한경섭;박정현
    • Journal of the Korean Ceramic Society
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    • v.30 no.12
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    • pp.993-998
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    • 1993
  • Nicalon-fiber-reinforced SiC composites were fabricated via polymer solution infiltration/chemical vapor infiltration (PSI/CVI) and CVI. Specifically, data were taken and compared for flexural strength, fracture toughness, and processing time. The two process resulted in comparable mechanical properties, and PSI/CVI process resulted in significantly reduced infiltration time.

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Fracture Behaviors and Mechanical Properties of SiCf/SiC Composites Prepared by the Whisker Growing Assisted CVI Process (Whisker Growing Assisted 화학침착 공정으로 제조된 SiCf/SiC 복합체의 파괴거동과 기계강도 평가)

  • Kang, Seok-Min;Kim, Weon-Ju;Yoon, Soon-Gil;Park, Ji-Yeon
    • Journal of the Korean Ceramic Society
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    • v.46 no.5
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    • pp.484-487
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    • 2009
  • $SiC_f$/SiC composites with whiskers and pyrolytic carbon (PyC) coated whiskers in the matrix were fabricated for enhancement of the fracture behaviors by the whisker growing assisted chemical vapor infiltration (WA-CVI) process, respectively. $SiC_f$/SiC composites were also prepared by the conventional CVI process as reference material. The mechanical properties and fracture behaviors were analyzed by comparison of the two types of composites prepared by WA-CVI and conventional CVI. The densities of $SiC_f$/SiC composites were in the range of $2.6{\sim}2.65g/cm^3$. The flexural strengths of composite with whiskers and with those coated by PyC were 650 MPa and 600 MPa, respectively. The tensile strength of composites with whiskers was ${\sim}285$ MPa.

Fracture Behaviors of SiCf/SiC Composites Prepared by Hybrid Processes of CVI and PIP (화학침착법과 고분자함침 열분해법의 복합공정으로 제조한 SiCf/SiC 복합체의 제조 공정에 따른 파괴거동)

  • Park, Ji Yeon;Han, Jangwon;Kim, Daejong;Kim, Weon-Ju;Lee, Sea Hoon
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.430-434
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    • 2014
  • $SiC_f$/SiC composites were prepared using the hybrid process of chemical vapor infiltration (CVI) and polymer impregnation and pyrolysis (PIP). Before the application of PIP, partially matrix-filled preform composites with different densities were fabricated by control of chemical vapor infiltration time and temperature. The changes of the final density of the $SiC_f$/SiC composites had a tendency similar to that of preform composites partially filled by CVI. Composites with lower density after the CVI process had a larger increment of density during the PIP process. Three types of microstructures were observed on the fractured surface of the composite: 1) well pulled-out fibers and lower density, 2) slightly pulled-out fibers and higher density, and 3) only bulk SiC. The different fractions and distributions of the microstructures could have an effect on the mechanical properties of the composites. In this study, $SiC_f$/SiC composites prepared using a hybrid process of CVI and PIP had density values in the range of $1.05{\sim}1.44g/cm^3$, tensile strength values in the range of 76.4 ~ 130.7 MPa, and fracture toughness values in the range of $11.2{\sim}13.5MPa{\cdot}m^{1/2}$.

Film Boiling Chemical Vapor Infiltration of C/C Composites: Influence of Mass and Thermal Transfers

  • Delhaes, P.;Trinquecoste, M.;Derre, A.;Rovillain, D.;David, P.
    • Carbon letters
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    • v.4 no.4
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    • pp.163-167
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    • 2003
  • The "Film boiling" Chemical Vapor Infiltration (CVI) process is a rapid densification one developed in particular for the elaboration of carbon/carbon composite materials. In order to optimize this new thermal gradient process, we have carried out several studies, on one hand, about the nature of the complex chemical reactions in a confined medium, and on the other hand, relative to the role of heat and mass transfers inside the preform. We show in this study that the introduction of a permeable sheath around the preform leads to hybrid liquid/gas CVI process which presents the advantages of very high densification rates associated with a moderate input energy.

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Design and Optimization of TG-CVI Heater (TG-CVI용 히터 형상설계 및 최적화)

  • 이성호;홍성석;구형회
    • Journal of the Korea Institute of Military Science and Technology
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    • v.3 no.2
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    • pp.244-249
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    • 2000
  • Thermal gradient chemical vapor infiltration (TG-CVI) process, which is one of the CVI techniques to densify a porous fiber preform, requires for a heater to have uniform surface temperature distribution. Thus, it is essential to design the shape of the heater and to predict the temperature distribution when the heater has a profile which is not a simple cylinder. In this study, an analytical method has been used to design the inner profile of a conical heater showing uniform temperature distribution, if its outer shape is specified. Temperature distribution on the heater surface has been calculated with the finite difference method and compared with the experimental results. When a heater had a combined profile with a large cone and a small cylinder, temperature was higher in the cylindrical part. To reduce the temperature difference between these areas, a hole-machining method has been proposed including other possible ones. A shape design and optimization program has been made to improve the temperature uniformity of the TG-CVI heater better than that designed with the analytical method.

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Translation Study of Miller Assessment of Preschoolers (MAP) for Using in Korea (Miller Assessment for Preschoolers(MAP)의 국내 적용을 위한 번역 연구)

  • Hong, Eunkyoung;Kim, Kyeong-Mi
    • The Journal of Korean Academy of Sensory Integration
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    • v.16 no.1
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    • pp.35-44
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    • 2018
  • Objective : This study aimed to perform a translation, backward translation, item modification, and test of content validity for Korean version of Miller Assessment for Preschoolers (MAP). Methods : Professors in department of occupational therapy, translators, or occupational therapists participated in the processes of translation, comparison and synthesis I, backward translation, comparison and synthesis II, test of understanding, and modify of items. Content Validity Indices (CVI) was calculated for data analysis by using Microsoft Office Excel. Results : Results of comparison between the original MAP and Korean MAP in professor panels were mean $3.66{\pm}0.40$, item-level CVI (I-CVI) 0.94, and overal scale CVI (S-CVI) 0.83. In agreement, result of comparison between of the original MAP and backward translated MAP (version English) was mean 3.14. The erroneous content was omission 13 times, the addition 3 times, the substitution 6 times, erroneous terms 11 times, and reordering 6 times. Average of understanding test in the therapist panels was $3.66{\pm}0.27$. The agreements were I-CVI 0.93 and S-CVI 0.58. Conclusion : Using assessment tools that developed in another country is important to do test of content validity and systematic translation process in Korea. For developing Korean version of MAP, validity and reliability studies need to be followed in near future.

A Study on Translation Process into Korean Version of the Life-Space Assessment to Assess Community Mobility for Elderly (노인의 지역사회 이동성을 측정하는 Life-Space Assessment(LSA)의 한국어 번역에 대한 적합성 검증연구)

  • Kim, Jeong-Hui;Chang, Moon-Young
    • The Journal of Korean society of community based occupational therapy
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    • v.7 no.1
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    • pp.49-57
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    • 2017
  • Objective : The purpose of this study to create a translation of Life Space Assessment(LSA) for elderly, which was then tested for content related validity and understanding test. Methods : The translation and content validation process involved direct and backward translation, and the collection of content-related evidence from 6 expert panels and 13 clinician panels. A content validity indices (CVI), means, and standard deviations were used for the analysis of the content validity. Results : The results of the comparison between the original LSA and the Korean LSA with the expert panels were I-CVI showed a very high value of .93. and 1.00, and S-CVI/Ave 0.99. The results of the understanding test were showed a very high value of .92 and 1.00, and S-CVI/Ave 0.97. Conclusion : Korean LSA showed content related validity and understanding test, and illustrated the applicability of LSA in a Korean clinical setting. The results showed LSA can be used a useful tool for evaluating the community mobility of elderly.

Densification of Carbon/Carbon Composites by Pulse CVI with and without Residence (펄스화학기상침트법에 의한 탄소/탄소 복합재료의 치밀화에 있어서 가스유지시간 유무의 영향)

  • 이용근;류호진;박희동
    • Journal of the Korean Ceramic Society
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    • v.33 no.8
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    • pp.935-941
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    • 1996
  • Two-dimensional carbon/carbon preforms made of PAN-based carbon yarn and phenolic resin were densified with pyrolysis of propane by pulse chemical vapor infiltration where repeated the cycle of gas introduction residence and evacuation. Maximim density increment was 14% when infiltration temperature and time were 100$0^{\circ}C$ and 21.25 hrs respectively. The distribution of deposits of pyrocarbon by this process has been occurred uniformly in the bottom middle and top of carbon/carbon composite preform Pulse CVI with residence is most effective in increasing density and shortening infiltration time among isothermal CVI and pulse CVI with and without residence.

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A Study on Ultrasonic Evaluation of Material Defects in Carbon/carbon Composites

  • Im, Kwang-Hee;David K. Hsu;Cha, Cheon-Seok;Sim, Jae-Ki;Yang, In-Young
    • Journal of Mechanical Science and Technology
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    • v.16 no.12
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    • pp.1652-1663
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    • 2002
  • It is desirable to perform nondestructive evaluation to assess material properties and part homogeneity because manufacturing of carbon/carbon (C/C) composites requires complicated and costly processes. In this work several ultrasonic techniques were applied to carbon/carbon composites for the evaluation of spatial variations in material properties that are attributable to the manufacturing process. In a large carbon/carbon composite manufactured by chemical vapor infiltration (CVI) method, the spatial variation of ultrasonic velocity was measured and found to be consistent with the densification behavior in CVI process in order to increase the density of C/C composites. Ultrasonic velocity and attenuation depend on a density variation of materials. Low frequency through-transmission scans based on both amplitude and time-of-flight of the ultrasonic pulse were used for mapping out the material property inhomogeneity These results were compared with that obtained by dry-coupling ultrasonics. Pulse-echo C-scans was used to image near-surface material property anomalies such as the placement of spacers between disks during CVI. Also, optical micrograph had been examined on the surface of C/C composites using a destructive way.

Numerical study on heat transfer and densification for SiC composites during thermal gradient chemical vapour infiltration process

  • Ramadan, Zaher;Im, Ik-Tae
    • Carbon letters
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    • v.25
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    • pp.25-32
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    • 2018
  • In this study, a thermal-gradient chemical vapor infiltration (TG-CVI) process was numerically studied in order to enhance the deposition uniformity within the preform. The computational fluid dynamics technique was used to solve the governing equations for heat transfer and gas flow during the TG-CVI process for two- and three-dimensional (2-D and 3-D) models. The temperature profiles in the 2-D and 3-D models showed good agreement with each other and with the experimental results. The densification process was investigated in a 2-D axisymmetric model. Computation results showed the distribution of the SiC deposition rate within the preform. The results also showed that using two-zone heater gave better deposition uniformity.