• Title/Summary/Keyword: CV measurement

검색결과 175건 처리시간 0.026초

강철보호를 위한 폴리아닐린 분산 코팅의 전기화학 및 부식특성 (Electrochemistry and Corrosion Characteristics of Polyaniline Dispersion Coating for Protection of Steels)

  • 허재훈;오응주;조정환
    • 전기화학회지
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    • 제6권2호
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    • pp.113-118
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    • 2003
  • 폴리아닐린 분말과 고분자 계면활성제, cyclohexanone용매를 micro-milling장치내에서 분산시켜 (m입자 크기를 갖는 가공용이한 분산액을 제조하였다. 분산액을 백금 전극 위에 코팅하여 얻은 분산박막의 전기화학적 특성들은 순환전압전류법(CV)을 이용하여 조사하였다. CV의 결과에 의하면 폴리아닐린 분산박막이 순수한 폴리아닐린 박막과 유사한 전기화학적 특성을 갖는 것으로 나타났다. $3wt.\%$ NaCl용액에서 수행한 분극실험과 열린회로전위 측정 실험에서는 PANI분산액을 철표면에 코팅하면 부식전위가 증가하였다. 분산박막/철 전극의 열린회로전위값(OCP, Voc)이 분산액의 제조 조건에 따라 변화가 있음을 관찰하였다. 이러한 결과들은 본 연구에서 사용한 전도성 고분자 분산액이 철의 부식방지코팅물질로서 유용성을 갖고 있다는 것을 보여주고 있다.

A Clinical Study on the Diagnosis and Observation of Functional Dyspepsia - Focused on Algometer

  • Gi-Hwan Rho;Gyu-Ho Choi;Sang-Hyun Lee;Hyeon-Min Noh;Seo-Hyung Choi
    • 대한한의학회지
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    • 제43권4호
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    • pp.1-7
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    • 2022
  • Objectives: This study aimed to determine whether comparing the pressure pain threshold (PPT) with an algometer before and after treatment for functional dyspepsia is of diagnostic value and investigate a possible correlation between PPT measured using an algometer and symptom improvement before and after treatment. Methods: A total of 99 patients with functional dyspepsia symptoms admitted to the OO Korean Medical Hospital from April 14, 2020 to January 21, 2021 were investigated. On the 1st and 14th days of hospitalization, the pressure of the first pain complaint at acupuncture points Juque (巨厥, CV14), Shangwan (上脘, CV13), Zhongwan (中脘, CV12), Xiawan (下脘, CV10), Guanuan (關元, CV4), Tianshu (天樞, ST25), and Daju (大巨, ST27) was measured using the algometer, and the visual analog scale (VAS) scores for patient's symptoms were evaluated. The algometer PPT and patient-symptom VAS scores were compared by repeated measures corresponding to the sample t-test to analyze the changes after treatment. A correlation analysis was performed to identify the correlation between patient-symptom VAS scores and algometer PPT. Results: The PPT measured using the algometer significantly increased after treatment in the 99 patients. The patient-symptom VAS score decreased significantly in most cases as treatment progressed. Analysis of the correlation between algometer PPT and patient-symptom VAS scores revealed some notable negative correlations. Conclusion: The algometer can help to set the diagnostic and treatment baselines for patients with functional dyspepsia.

인간 $\alpha$-fetoprotein (AFP)에 대한 폴리클로날 항체의 생산 및 $\alpha$-fetoprotein 측정용 효소면역분석법 (competitive ELISA)의 개발 (Production of Polyclonal Antibody against $\alpha$-Fetoprotein and Polyclonal Antibody-Based Competitive Enzyme-Linked Immunosorbent Assay for $\alpha$-Fetoprotein)

  • Michung Yoon
    • 대한의생명과학회지
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    • 제3권2호
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    • pp.115-123
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    • 1997
  • 인간 $\alpha$-fetoprotein (AFP)은 간암, 위암, 생식기 종양 및 신경관 이상인 환자를 검사하고 진단하는데 유용한 지표로 알려져 있다. 본 연구에서는 사람의 AFP를 분리정제 하여 폴리클로날 항체를 생산하고 인간 혈장과 양수내의 AFP를 측정하기 위한 경쟁적 효소면역 분석법을 개발하고자 하였다. 친화크로마토그래피법과 SDS-polyacrylamide 전기영동법을 이 용하여 양수로부터 AFP를 분리하였다. 정제된 AFP를 토끼에 주사하여 폴리클로날 항체를 생산하였으며, 이중면역확산법과 Western blot 분석법을 사용하여 본 연구실에서 제조된 항체의 항원 특이성이 대단히 높음을 확인하였다. AFP와 항혈청을 이용하여 표준곡선을 얻었으며, 민감도는 5ng/ml이었고, 작용범위는 5~l,000ng/ml이었다. 분석내 CV는 4.5%이었고, 분석간 CV는 8.5%이었다. 따라서 이러한 결과로 보아 본 연구에서 개발된 경쟁적 효소면역분석법이 AFP를 측정하기에 적절하며, 간암 등의 기초연구에도 많은 기여를 할 것으로 생각된다.

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충격파-부분방전(SI-PD) 시험방법을 이용한 케이블 진단에 관한 기초 연구 (A Possible diagnostic method of cable system using SI-PD measurement)

  • 김정태;구자윤;장은;조연옥;김상준;송일근;김주용
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1996년도 하계학술대회 논문집 C
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    • pp.1774-1777
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    • 1996
  • In this paper, applicability of SI-PD(switching impulse - partial discharge) testing method was put on an attempt as a newly proposed diagnostic method for the underground distribution power cable system in Korea. For this purpose, SI-PD testing equipment was designed, and tests were performed using artificial needle-type defects integrated into the 22.9 kV CN/CV cables in drder to prove its reliability. As a result, arc noises, generated from spark gap, were considerably decreased by use of a pneumatic switch immersed into oil, and artificial needle-type defects were well detected with impulse voltage level under $2U_0$. These results imply that it is likely possible to apply SI-PD measurement method as a the nondistructive test for the 22.9 kV CN/CV cable system in Korea.

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A Relationship of Tone, Consonant, and Speech Perception in Audiological Diagnosis

  • Han, Woo-Jae;Allen, Jont B.
    • 한국음향학회지
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    • 제31권5호
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    • pp.298-308
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    • 2012
  • This study was designed to examine the phoneme recognition errors of hearing-impaired (HI) listeners on a consonant-by-consonant basis, to show (1) how each HI ear perceives individual consonants differently and (2) how standard clinical measurements (i.e., using a tone and word) fail to predict these differences. Sixteen English consonant-vowel (CV) syllables of six signal-to-noise ratios in speech-weighted noise were presented at the most comfortable level for ears with mild-to-moderate sensorineural hearing loss. The findings were as follows: (1) individual HI listeners with a symmetrical pure-tone threshold showed different consonant-loss profiles (CLPs) (i.e., over a set of the 16 English consonants, the likelihood of misperceiving each consonant) in right and left ears. (2) A similar result was found across subjects. Paired ears of different HI individuals with identical pure-tone threshold presented different CLPs in one ear to the other. (3) Paired HI ears having the same averaged consonant score demonstrated completely different CLPs. We conclude that the standard clinical measurements are limited in their ability to predict the extent to which speech perception is degraded in HI ears, and thus they are a necessary, but not a sufficient measurement for HI speech perception. This suggests that the CV measurement would be a useful clinical tool.

중완(中脘)($CV_{12}$) 수념산(手拈散)약침이 Caerulein으로 유발된 흰쥐의 췌장염에 미치는 영향 (Effects of Sujeom Powder Pharmacopuncture Injected at Jung-wan($CV_{12}$) on the Caerulein-induced Acute Pancreatitis in the Rat)

  • 김인수;전상윤;정태산;강성순;조재준;이영수
    • Journal of Acupuncture Research
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    • 제29권6호
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    • pp.35-45
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    • 2012
  • Objectives : This study was designed to investigate Effects of Sujeom powder(SJP) pharmacopuncture Injected at Jung-wan($CV_{12}$) in rats with caerulein-induced acute pancreatitis(AP). Methods : We examined changes of organ weight, histology, immunohistochemistry and gene expression of cycolooxygenase 2(COX-2) in the pancreas. Twenty adult male Sprague-Dawley rats were divided into four groups as follow: normal(Nor), caerulein-induced(Con), caerulein+SJP pharmacopuncture 0.2mL injected at Jung-wan($CV_{12}$)(SA), and caerulein+SJP pharmacopuncture 0.8 mL injected at Jung-wan($CV_{12}$)(SB) groups. Pancreatic tissues of rats from all groups were removed for histological observation and light microscopic examination. Interleukin-6(IL-6) levels were determined spectrophotometrically. Results : The ratio of pancreas/body weights was significantly(p<0.05) increased in the Con, the SA and the SB compared with the Nor, but was slightly decreased in the SA and in the SB groups compared with the Con. Caerulein administration has significantly(p<0.05) increased in the levels of amylase, but the SA, the SB significantly(p<0.05) decreased in the levels of these enzyme. The levels of amylase were increased significantly with caerulein administration, but were inhibited significantly in the SA and in the SB groups. Interleukin-6(IL-6) levels were significantly(p<005) increased in all groups compared with the Nor, especially in the SB. were significantly increased. The levels of Tumor necrosis factor(TNF)-${\alpha}$ levels were significantly increased in all groups compared with the Nor. In the conclusion, the datum of IL-6 and TNF-${\alpha}$ are suggested that the inflamation was still existed actively at a point of measurement(24 hours later). The COX-2 positive materials are observed in the pancreas from the Con, but these positive materials are decreased in the SJP pharmacopuncture at Jung-wan($CV_{12}$) treatment group. Conclusion : SJP pharmacopuncture injected at Jung-wan($CV_{12}$) is potentially capable of limiting pancreatic damage during AP by restoring the fine structure of acinar cells and tissues. Therefore we can say that SJP pharmacopuncture Injected at Jung-wan($CV_{12}$) may have beneficial effects in the treatment of caerulein-induded AP. Further studies about the adequate amount of the SJP pharmacopuncture and about more effective route of administration is still required.

과산화수소를 이용한 Pt계 촉매의 인산 이온 피독 특성 정량 평가 방법 (The Measurement Method Using Hydrogen Peroxide for Quantification of Phosphate Ion Poisoning of Pt Based Catalyst)

  • 양승원;박정진;정용진;권용재
    • Korean Chemical Engineering Research
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    • 제57권3호
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    • pp.438-443
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    • 2019
  • 본 연구에서는 HT-PEMFC 공기극용 Pt계열 연료극 촉매의 인산이온 피독 특성에 대한 새로운 평가 방법을 제시하였다. 이를 위하여, 기존의 전기화학적 인산이온 피독 측정법인 CV와 ORR RDE 측정법이 갖고 있는 문제점을 저감하기 위하여, 과산화수소를 Pt 촉매와의 반응물로 이용하여 고농도 인산 이온 분위기에서의 내피독성 측정값 오차를 감소시켰다. 그 결과 인산이온 농도 0.1 M 이하의 저농도와 0.5 M 이상의 고농도에서 인산농도 대비 전류밀도의 변화가 직선적으로 나타나, 실제 HT-PEMFC의 구동 환경과 유사한 고농도의 인산이온 분위기에서의 Pt계 인산이온 피독 정량화에 대하여 기존의 측정방법에 비해 우수함을 확인하였다.

22kV 전력케이블의 열화 판정에 관한 연구 (A Study on the Remain Life with Aging in 22kV CV cable)

  • 이관우;목영수;김보경;박복기;박대희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2003년도 추계학술대회 논문집 전기물성,응용부문
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    • pp.19-21
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    • 2003
  • In this paper, we studied on life-decision of underground cable of live-lines state. As all equipments have been wear, underground cables decided design-life on the whole 30 years because underground cable have been occurred aging as time goes. CV cable has been become about 30 years after installation in the South Korea, is come to a important point of time with estimation about life. Study target cable is 22 kV CV cables in this point of view and installation cable is about 10 years before and behind. Measurement method used dc leakage method of live-lines state that applied voltage of 50V in neutral point and data is analyzing result that is measured during 5 years. In this result, insulation resistance could confirm that change according to season and cause is effect of humidity, seasons and load current. Also, according as data is gone aging, insulation resistance by Weibull distribution could confirm functionally its decrease. As a result, the aging speed of cable that water tree is gone could confirm fastness very. Numerical analysis result, cable that water tree is not gone could confirm that life of cable that has passed 10 years remains about $10{\sim}20$ years.

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간결한 예측 모형에 기반한 납축전지의 정전류-정전압 충전시간 특성화 (CC-CV Charging Time Characteristics of Lead-Acid Batteries Based on Compact Estimation Model)

  • 한정견;신동화
    • 대한임베디드공학회논문지
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    • 제11권5호
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    • pp.305-312
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    • 2016
  • Modern embedded systems are typically operated by the rechargeable batteries in our daily life. Since charge of batteries is considered as an time consuming task, there have been extensive efforts to manage the charge time from the perspective of materials, circuits, and systems. Estimation of battery charge time is one of the essential information to design the charge circuitry. A compact macro model for the constant-current and constant-voltage charge protocol was recently introduced, which gives us a quick estimation of charge time with similar shape to the famous Peukert's law for discharge time estimation. The CC-CV charging protocol is widely used for Lithium-based batteries and Lead-acid batteries. In this paper, we characterize the lead-acid battery by measurement to extract the model coefficients, which was not covered by the previous studies. By our proposed model, the key coefficient Kcc results in 1.18-1.31, which is little bit higher than that of Lithium batteries. The accuracy of our model is within the range of ${\pm}10%$ error, which is compatible with the other studies such as Peukert's law.

THE TRANSFER OF CHLORIDE ION ACROSS ANION EXCHANGE MEMBRANE

  • Yu, Zemu;Wang, Hanming;Wang, Erkang
    • 분석과학
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    • 제8권4호
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    • pp.597-601
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    • 1995
  • The transfer of chloride ion across an anion exchange membrane (AEM) was investigated by cyclic voltammetry (CV) and electrochemical impedance spectra. In CV experiment, when the size of the hole in membrane was much smaller than the distance between membrane holes, the Cl anion transfer showed steady state voltammetric behavior. Each hole in membrane can be regarded as a microelectrode and the membrane was equivalent to a microelectrode array in this condition. When the hole in membrane was large or the distance between membrane holes was small, the CV curve of the Cl anion transfer across membrane showed peak shape, which attributed to linear diffusion. In ac impedance measurement, the impedance spectrum of the membrane system was composed of two semicircles at low de bias, corresponding to the bulk characteristics of the membrane and the kinetic process of ion transfer, respectively. The bulk membrane resistance increases with increasing dc bias and only one semicircle was observed at higher dc bias. The parameters related to kinetic and membrane properties were discussed.

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