• Title/Summary/Keyword: CNT Dip-Coating

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Interfacial Control of Multi-functional CNT and ITO/PET Nanocomposites having Self-Sensing and Transparency (자체-감지능 및 광투과도를 지닌 CNT 및 ITO/PET 다기능성 나노복합소재의 계면 조절 연구)

  • Wang, Zuo-Jia;Kwon, Dong-Jun;Gu, Ga-Young;Park, Joung-Man
    • Composites Research
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    • v.24 no.1
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    • pp.45-50
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    • 2011
  • Transparent and conductive carbon nanotube on polyethylene terephthalate (PET) were prepared by dip-coating method for self-sensing multi-functional nanocomposites. The changes in the electrical and optical properties of CNT coating mainly depended on the number of dip-coating, concentration of CNT solution. Consequently, the surface resistance and transmittance of CNT coating were sensitively controlled by the processing parameters. Surface resistance of CNT coating was measured using four-point method, and surface resistance of coated CNT could be better calculated by using the dual configuration method. Optical transmittance of PET film with CNT coating was evaluated using UV spectrum. Surface properties of coated CNT investigated by wettability test via static and dynamic contact angle measurement were consistent with each other. As dip-coating number increased, surface resistance of coated CNT decreased seriously, whereas the transmittance exhibited little lower due to the thicker CNT networks layer. Interfacial microfailure properties were investigated for CNT and indium tin oxide (ITO) coatings on PET substrates by electrical resistance measurement under cyclic loading fatigue test. CNT with high aspect ratio exhibited no change in surface resistance up to 2000 cyclic loading, whereas ITO with brittle nature showed a linear increase of surface resistance up to 1000 cyclic loading and then exhibited the level-off due to reduced electrical contact points based on occurrence of many micro-cracks.

Manufacture of Recycled PET E-Textile by Plasma Surface Modification and CNT Dip-Coating (플라즈마 표면 개질과 CNT 함침공정을 통한 고전도성의 재생PET사 전자섬유)

  • Jun-hyeok Jang;Sang-un Kim;Joo-Yong Kim
    • Science of Emotion and Sensibility
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    • v.26 no.1
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    • pp.79-86
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    • 2023
  • This study aims to create a highly conductive E-textile made by recycling PET with a Dip-coating process. PET fiber with hydrophobic properties is characterized by the difficulty in imparting great conductivity when both Virgin and Recycled are made of electronic fibers through a Dip-coating process. To advance the effectiveness of the Dip-coating process, a sample made of recycled PET was surface modified for 50 w 5 minutes and 10 minutes employing a Covance-2mprfq model from FEMTO SCIENCE. After that, the sample was immersed in an SWCNT dispersion (.1 wt%, Carbon Co., Ltd.) for 5 minutes, and then dip coating was conducted to allow the solution to permeate well into the sample through a padder (DAELIM lab). After the procedure was completed, the resistance measurement was measured with a multimeter at both ends and then accurately remeasured with a wider electrode. As a result of this contemplation, it was affirmed that great conductivity might be given through an impregnation process through the plasma surface modification. When the surface modification was performed for 10 minutes, the resistance was reduced by up to 2.880 times. Dependent on the results of this research, E-fibers employed in the smart wearable sector can also be made of recycled materials, improving smart wearable products that can save oil resources and reduce carbon emissions.

Enhancement of Penetration by Using Mechenical Micro Needle in Textile Strain Sensor (텍스타일 스트레인 센서에 마이크로 니들을 이용한 전도성입자 침투력 향상)

  • Hayeong Yun;Wonjin Kim;Jooyong Kim
    • Science of Emotion and Sensibility
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    • v.25 no.4
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    • pp.45-52
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    • 2022
  • Recently, interest in and demand for sensors that recognize physical activity and their products are increasing. In particular, the development of wearable materials that are flexible, stretchable, and able to detect the user's biological signals is drawing attention. In this study, an experiment was conducted to improve the dip-coating efficiency of a single-walled carbon nanotube dispersion solution after fine holes were made in a hydrophobic material with a micro needle. In this study, dip-coating was performed with a material that was not penetrated, and comparative analysis was performed. The electrical conductivity of the sensor was measured when the sensor was stretched using a strain universal testing machine (Dacell Co. Ltd., Seoul, Korea) and a multimeter (Keysight Technologies, Santa Rosa, CA, USA) was used to measure resistance. It was found that the electrical conductivity of a sensor that was subjected to needling was at least 16 times better than that of a sensor that was not. In addition, the gauge factor was excellent, relative to the initial resistance of the sensor, so good performance as a sensor could be confirmed. Here, the dip-coating efficiency of hydrophobic materials, which have superior physical properties to hydrophilic materials but are not suitable due to their high surface tension, can be adopted to more effectively detect body movements and manufacture sensors with excellent durability and usability.

Field emission properties of carbon nanotubes grown by various methods (다양한 방법에 의해 성장된 탄소 나노튜브의 전계방출 특성)

  • Kim, Bu-Jong;Chang, Han-Beet;Kim, Jong-Pil;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.1408-1409
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    • 2011
  • Carbon nanotubes (CNTs) were grown on conical tip substrates by using various methods such as electrophoretic deposition, dip-coating, and spray. The scanning electron microscope measurement showed that the spray method ascertained the most uniform deposition of CNTs. The CNT-emitter that was fabricated by the spray method revealed the lowest turn on voltage of electron emission and the highest emission current. In addition, the spray-produced CNT emitter showed the most stable long-term emission characteristics.

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Development of an Angle Estimation System Using a Soft Textile Bending Angle Sensor (소프트 텍스타일 굽힘 각 센서를 이용한 각도 추정 시스템 개발 )

  • Seung-Ah Yang;Sang-Un Kim;Joo-Yong Kim
    • Science of Emotion and Sensibility
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    • v.27 no.1
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    • pp.59-68
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    • 2024
  • This study aimed to develop a soft fabric-based elbow-bending angle sensor that can replace conventional hard-type inertial sensors and a system for estimating bending angles using it. To enhance comfort during exercise, this study treated four fabrics (Bergamo, E-band, span cushion, and polyester) by single-walled carbon nanotube dip coating to create conductive textiles. Subsequently, one fabric was selected based on performance evaluations, and an elbow flexion angle sensor was fabricated. Gauge factor, hysteresis, and sensing range were employed as performance evaluation metrics. The data obtained using the fabricated sensor showed different trends in sensor values for the changes in the angle during bending and extending movements. Because of this divergence, the two movements were separated, and this constituted the one-step process. In the two-step process, multilayer perceptron (MLP) was employed to handle the complex nonlinear relationships and achieve high data accuracy. Based on the results of this study, we anticipate effective utilization in various smart wearable and healthcare domains. Consequently, a soft- fabric bending angle sensor was developed, and using MLP, nonlinear relationships can be addressed, enabling angle estimation. Based on the results of this study, we anticipate the effective utilization of the developed system in smart wearables and healthcare.

Carbon-nanotube-based Spacer Fabric Pressure Sensors for Biological Signal Monitoring and the Evaluation of Sensing Capabilities (생체신호 모니터링을 위한 CNT 기반 스페이서 직물 압력센서 구현 및 센싱 능력 평가)

  • Yun, Ha-yeong;Kim, Sang-Un;Kim, Joo-Yong
    • Science of Emotion and Sensibility
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    • v.24 no.2
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    • pp.65-74
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    • 2021
  • With recent innovations in the ICT industry, the demand for wearable sensing devices to recognize and respond to biological signals has increased. In this study, a three-dimensional (3D) spacer fabric was embedded in a single-wall carbon nanotube (SWCNT) dispersive solution through a simple penetration process to develop a monolayer piezoresistive pressure sensor. To induce electrical conductivity in the 3D spacer fabric, samples were immersed in the SWCNT dispersive solution and dried. To determine the electrical properties of the impregnated specimen, a universal testing machine and multimeter were used to measure the resistance of the pressure change. Moreover, to examine the changes in the electrical properties of the sensor, its performance was evaluated by varying the concentration, number of penetrations, and thickness of the specimen. Samples that penetrated twice in the SWCNT distributed solution of 0.1 wt% showed the best performance as sensors. The 7-mm thick sensors showed the highest GF, and the 13-mm thick sensors showed the widest operating range. This study confirms the effectiveness of the simple process of fabricating smart textile sensors comprising 3D spacer fabrics and the excellent performance of the sensors.