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Strain Ageing in Zircaloy-4

  • Rheem, Karp-Soon;Park, Won-Koo
    • Nuclear Engineering and Technology
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    • v.8 no.1
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    • pp.19-27
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    • 1976
  • The strain ageing behaviour of Zircaloy-4 has been studied in the temperature range 175$^{\circ}C$ to 575$^{\circ}C$ for both quenched and annealed specimens. The strain ageing in quenched Zircaloy-4 was found in the temperature range 175$^{\circ}C$ to 50$0^{\circ}C$ and its Peak occured at 3$25^{\circ}C$ while the strain ageing in annealed specimens occured in the temperature range 175-575$^{\circ}C$, showing two peaks, one at 323$^{\circ}C$ and a higher one at 45$0^{\circ}C$. The peak at 3$25^{\circ}C$ in both quenched and annealed specimens is considered to be due to the segregation of interstitial oxygen atoms to cell walls during ageing. The peak at 45$0^{\circ}C$ in annealed specimens is considered to he due to the interaction of dislocations with Fe atoms. It has been found that strain ageing stress at ~30$0^{\circ}C$ in zirconium alloys is proportional to the square root of oxygen content.

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Determination of Peripheral Catechol O-methyltransferase (COMT) Activity in vivo using $[2-^{14}C]-3',4'-Dihydroxyacetophenone$

  • Kim, Eun-Joo;Ahn, Jong-Woong;Lee, Hye-Suk;Christ, Wolfram
    • Archives of Pharmacal Research
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    • v.14 no.4
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    • pp.290-294
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    • 1991
  • For the determination of peripheral COMT activity, we synthesized $[2-^{14}C]-3',4'-dihydroxyacetophenone([^{14}C]-DHAP)$, a model substrate closely related to catecholamines, which cannot be attacked by monoamine oxidase. After i.v.-injection of $[^{14}C]-DHAP$ in living animals, only 3',4'-dihydroxy-acetophenone (3',4'-DHAP) and 3'-methoxy-4'-hydroxyacetophenone (3'-MHAP) were detected in blood by thin layer radio chromatography. It could be speculated that 3',4'-DHAP was primarily O-methylated by COMT, followed by subsequent conjugations. The concentration of 3',4'-DHAP, a substrate for COMT, in blood at 5 min after injection of $[^{14}C]-DHAP$, were similar in all animals. The rate of 3'-MHAP formation can be therefore used as an indicator for peripheral COMT activity. The velocity of methylation in 15 min after i.v.-administration of $[^{14}C]-DHAP$ was $0.28\;{\mu}g/ml{\cdot}min$. From these results, 3',4'-DHAP was shown to be used as an appropriate substrate to determine the COMT activity in vivo.

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Bond Strength of Steel honeycomb Structure (철강 하니콤구조의 접합강도)

  • Song, Keun;Hong, Young Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.4
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    • pp.197-204
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    • 2003
  • Honeycomb structure has been fabricated by brazing method using 0.1 wt%C and 1.0wt%C carbon steel core and STS304 stainless steel face sheet. Core shear strength ratio in W and L directions was 1:1.03 in 7 mm cell size, whereas 1:1.45 in 4 mm cell size. Flexural strength on face sheet was 166.4 MPa (0.1 wt%C, W direction), 171.1 MPa (0.1 wt%C, L direction), and 120.2 MPa (1.0 wt%C, W direction) in 7 mm cell size. And in 4mm cell size specimen, it was 169.2 MPa (0.1 wt%C, W direction), 224.2 MPa (0.1 wt%C, L direction). This means that flexural strength of 0.1 wt%C core material was higher than that of 1.0wt%C core material, which was contrary to expectation. SEM and EDS analysis represented that grain boundary diffusion had occurred in0.1 wt%C core, but no grain boundary diffusion in 1.0 wt%C core. And corrugated surface of 0.1 wt%C core was flat, whereas that of 1.0 wt%C core was not flat. As a result, contact area between two 1.0 wt%C cores was much less than that of 0.1 wt% cores, It is thought to be main reason for lower flexural strength of 1.0 wt%C core.

The Development of an Electroconductive SiC-ZrB2 Ceramic Heater through Spark Plasma Sintering

  • Ju, Jin-Young;Kim, Cheol-Ho;Kim, Jae-Jin;Lee, Jung-Hoon;Lee, Hee-Seung;Shin, Yong-Deok
    • Journal of Electrical Engineering and Technology
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    • v.4 no.4
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    • pp.538-545
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    • 2009
  • The SiC-$ZrB_2$ composites were fabricated by combining 30, 35, 40 and 45vol.% of Zirconium Diboride (hereafter, $ZrB_2$) powders with Silicon Carbide (hereafter, SiC) matrix. The SiC-$ZrB_2$ composites, the sintered compacts, were produced through Spark Plasma Sintering (hereafter, SPS), and its physical, electrical, and mechanical properties were examined. Also, the thermal image analysis of the SiC-$ZrB_2$ composites was examined. Reactions between $\beta$-SiC and $ZrB_2$ were not observed via X-Ray Diffractometer (hereafter, XRD) analysis. The relative density of the SiC+30vol.%$ZrB_2$, SiC+35vol.%$ZrB_2$, SiC+40vol.%$ZrB_2$, and SiC+45vol.%$ZrB_2$ composites were 88.64%, 76.80%, 79.09% and 88.12%, respectively. The XRD phase analysis of the sintered compacts demonstrated high phase of SiC and $ZrB_2$ but low phase of $ZrO_2$. Among the SiC-$ZrB_2$ composites, the SiC+35vol.%$ZrB_2$ composite had the lowest flexural strength, 148.49MPa, and the SiC+40vol.%$ZrB_2$ composite had the highest flexural strength, 204.85MPa, at room temperature. The electrical resistivities of the SiC+30vol.%$ZrB_2$, SiC+35vol.%$ZrB_2$, SiC+40vol.%$ZrB_2$ and SiC+45vol.%$ZrB_2$ composites were $6.74\times10^{-4}$, $4.56\times10^{-3}$, $1.92\times10^{-3}$, and $4.95\times10^{-3}\Omega{\cdot}cm$ at room temperature, respectively. The electrical resistivities of the SiC+30vol.%$ZrB_2$, SiC+35vol.%$ZrB_2$ SiC+40vol.%$ZrB_2$ and SiC+45[vol.%]$ZrB_2$ composites had Positive Temperature Coefficient Resistance (hereafter, PTCR) in the temperature range from $25^{\circ}C$ to $500^{\circ}C$. The V-I characteristics of the SiC+40vol.%$ZrB_2$ composite had a linear shape. Therefore, it is considered that the SiC+40vol.%$ZrB_2$ composite containing the most outstanding mechanical properties, high resistance temperature coefficient and PTCR characteristics among the sintered compacts can be used as an energy friendly ceramic heater or electrode material through SPS.

Optimum Culture Conditions of Four Species of Microalgae as Live Food from China (중국산 식물먹이생물 4종의 최적 배양환경)

  • 박정은;허성범
    • Journal of Aquaculture
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    • v.13 no.2
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    • pp.107-117
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    • 2000
  • Optima for temperature, salinity and light intensity for Nitzschia closterium, Chlorella salina, I내초교냔 galbana and Tetraselmis subcordiformis, which are widely used in bivalve hatcheries of Shandong Province in China, were estimated. The temperature optimum was 23 $^{\circ}C$ for N. closterium and I. galbana and 25 and 27$^{\circ}C$ for C. salina and T. subcordiformis, respectively. That for salinity was 23${\textperthousand}$ for N. closterium and T, subcordiformis, but was 33${\textperthousand}$ for C. salina and I. galbana. In general, all the four microalgae grew faster under 6,000 lux than under 4,000 lux. Growth of N. closterium was faster at $25^{\circ}C$ and dropped abruptly >$25^{\circ}C$, and that of C. salina and T. subcordiformis progressively increased upto $25^{\circ}C$ but dropped beyond 27$^{\circ}C$. T. subcordiformis was the most eurythermal among the 4 species. For mass culture of microalgae in Korea, N. closterium and C. salina are suitable during spring and autumn but C. salina and I. galbana during summer. T. subcordiformis is suitable for culture throughout the year.

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Changes of Lactulose Content during Heat Treatment of Milk (우유의 열처리 및 저장 조건에 따른 Lactulose의 함량 변화)

  • 김철현;백승천;정운현
    • Food Science of Animal Resources
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    • v.22 no.1
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    • pp.50-54
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    • 2002
  • The aim of this work to determine the formation of lactulose during heat treatment process as a contribution to the estabilishment of limits of chemical indicators for different types of heat processed milk and analyze of lactulose for the reconstituted milk added samples. The HTST(75$\^{C}$/15s) and UHT(130$\^{C}$/2∼3s) treatment realized with a pilot plant and heat-treated samples were stroed at 4, 10, 30$\^{C}$ for 4 weeks. Changes in lactulose was evaluated at 7 days intervals. The other heat treatment was sealed in glass tube and heated at 75$\^{C}$ for 10 to 120s and heated at 130$\^{C}$ for 2 to 60s in a thermostatically controlled constant temperature bath of glycerol. The reconstituted milk was made with full fat dry milk that reconstituted with deionized water to 10% total solid, and was added to milk at 10, 20, 30% respectively. The samples processed with a HTST pilot plant showed that lactulose was contained at 1.47∼1.52mg/10()ml and 8.19 ∼8.32mg/100ml for UHT-treated samples. Changes in the lactulose content of heat-treated samples during storage at 4 and 10$\^{C}$ for 4 weeks caused a slight increase, however a noticeable increase was observed at 30$\^{C}$ for 4 week. The glass tube samples showed that high correlations between relative increase in content of lactulose and increasing processing times(75$\^{C}$ : r = 0.986, 130$\^{C}$ : r = 0.987, respectively). Added with reconstituted milk would cause a increase of the lactulose content linear with increasing addition amount(r = 0.982). This results observed for lactulose in commercial milk samples would applied to the detection of chemical changes during heat treatment and illegal use of reconstituted milk.

Change of Fermentation Characteristic of Kimchi by n-Capric Acid or n-Capric Acid Methyl Ester Addition and Storage Temperature (n-Capric Acid 또는 n-Capric Acid Methyl Ester 첨가와 저장온도에 따른 김치의 발효특성)

  • Kim, Byung-Yong;Ahn, Tae-Young;Kim, Myung-Hwan
    • Applied Biological Chemistry
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    • v.42 no.2
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    • pp.156-161
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    • 1999
  • This study was conducted to investigate the effects of n-capric acid(CA) or n-capric acid methyl ester (CE) addition during salting process, and fermentation temperature on chemical and microbial changes of Kimchi. The pHs of control, CA and CE were 3.78, 4.28 and 4.35 after 6 days of storage at $20^{\circ}C$ and were 3.85, 5.14 and 5.10 after 42 days of storage at $4^{\circ}C$, respectively. The effects of CA or CE addition at $4^{\circ}C$ were higher than those at $20^{\circ}C$. The maximum edible acidity, 0.75%, was reached within 3 days at $20^{\circ}C$, 15 days at $12^{\circ}C$, and the acidity of 42 days at $4^{\circ}C$ was 0.62% which was still lower value than the maximum edible acidity. Total bacteria, Leuconostoc, Lactobacillus and yeast counts of the control were higher value than those of the treatments throught the whole fermentation period. The addition of CE at $4^{\circ}C$ had much affected the reduction of yeast count. As microbial counts and reduction rates of control and treated Kimchi increased with increasing the storage temperature.

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The Effects of Cryoprotectants on Motility and Viability Kinetics of Liquid Boar Semen at $4^{\circ}C$ (액상 보존액 내 동결 보호제가 $4^{\circ}C$에 보관된 액상 돼지 정액의 운동성과 생존성에 미치는 효과)

  • Jeon, Yu-Byeol;Park, Kwang-Woo;Kwak, Seong-Sung;Jeong, Seung-A;Yoon, Jun-Chul;Hyun, Sang-Hwan
    • Journal of Embryo Transfer
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    • v.27 no.1
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    • pp.51-55
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    • 2012
  • The objective of this study was to investigate the motility and kinematics of boar sperm that while stored at 4C. The samples of fresh boar semen were place into an extender, Androhep, and stored at $4^{\circ}C$. In three of these samples, cryoprotectants were added. The sperm's motilities and kinematics were evaluated by using microscope (${\times}400$) and the viability status was evaluated by using with eosin staining method. The 5 sample groups are; Goup A:Androhep (extender), stored at $17^{\circ}C$. Group B:Androhep (extender), stored at $4^{\circ}C$. Group C:Androhep (extender), + 3% glycerol (cryoprotectant), stored at $4^{\circ}C$. Group D:Androhep (extender), + 3% DMSO (cryoprotectant), stored at $4^{\circ}C$. Group E:Androhep (extender), + 3% ethylene glycol (cryoprotectant), stored at $4^{\circ}C$. In group A, the sperm's motility was reduced. On day one the sperm's motility was ($85.7{\pm}2.3$) and day 5 the motility was ($43.9{\pm}3.3$). In group B, C and D the sperm's motility were reduced to 0 on day 5. In group E the sperm's percentage of motility decreased. On day one the sperm's motility was ($42.0{\pm}0.5$) and day 5 the motility was ($2.3{\pm}0.3$). When comparing cryoprotectant in samples of boar sperm there is a slight improvement in the results when the use of Androhep Lite (extender), + 3% ethylene glycol (cryoprotectant), stored at $4^{\circ}C$ are used. Based on these results, ethylene glycol can protect sperm from heat shock at $4^{\circ}C$, but not satisfactory level. However, it showed the possibilities of liquid semen preservation at $4^{\circ}C$ by using cryoprotectant.

The Storage Temperature Effect on Vibrio parahaemolyticus in Fish Homogenates (생선회에 오염원 장염비브리오균에 미치는 저장온도의 영향)

  • KIM Young-Man;LEE Myoung-Suk;CHANG Dong-Suck
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.19 no.2
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    • pp.136-140
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    • 1986
  • The change of cell counts of Vibrio parahaemolyticus in fish muscle by the storage time and temperature was examined to get basic informations for precautionary steps against food poisoning of slices of raw fish (sashimi). There fore, we inoculated fish homogenate of oceanic bonito (Katsuwonus pelamis), yellow tail (Seriola quinqueradiata) with Kanagawa positive Vibrio parahaemolyticus and stored it at $30^{\circ}C,\;18^{\circ}C,\;4^{\circ}C\;and\;-20^{\circ}C$ for 24 hours. The number of the Vibrio parahaemolyticus upon fish homogenate stored at $30^{\circ}C\;and\;18^{\circ}C$ decreased for the first two hours and increased thereafter. When the fish homogenates inoculated with Vibrio parahaemolyticus at about $10^3$ per gram were stored at $18^{\circ}C\;and\;30^{\circ}C$ for 10 hours, the cell numbers increased about 10 times and 1,000 times initial cell numbers, respectively. The survival rate of Vibrio parahaemolyticus was about $20\%$, when the inoculated fish homogenates were stored at $-20^{\circ}C$ for 24 hours. Vibrio parahaemolyticus inoculated in fish homogenates was decreased by about $10\%$ of initial cell numbers by the storage at $4^{\circ}C$ for 4 hours and it was decreased by about $50\%$ after 24 hours storage of the samples at the same temperature. The decreasing rate of inoculated Vibrio parahaemolyticus in fresh fish muscle homogenate was higher than that in frozen fish muscle homogenate during the storage time at a refrigerator.

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Effect of Temperature on the Development of Sciarid fly, Bradysia sp. (Diptera: Sciaridae) (검정날개버섯파리류 1종 Bradysia sp. 의 생육에 미치는 온도의 영향)

  • 이흥수;김규진;이현욱
    • Korean journal of applied entomology
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    • v.37 no.2
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    • pp.171-178
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    • 1998
  • This study was conducted to investigate the effect of temperature on the development of amushroom-infesting sciarid fly, Bradysia sp. (Diptera: Sciaridae). Egg period was 12.1, 7.0, 4.4, 3.4, and3.2 days, larval period was 38.3, 26.5, 13.4, 13.2, 12.7 days and pupal period was 10.4, 7.1, 4.4, 3.3, 3.2days, and total development period from egg to adult emergence was 60.8,40.6, 22.2, 19.9, and 19.1 daysat 10, 15, 20,25, 28"C, respectively. Development threshold temperature (DT) and effective accumulativetemperatures (ET) were 3.8"C, 74.8DD in eggs, 1.2"C, 321.8DD in larva, and 3.1$^{\circ}$C, 76.5DD in pupa,respectively. The number of eggs laid per female was 107.9, 129.7, 131.8, 86.9, and 82.7 at respectivetemperatures. Preoviposition period was 6.6, 4.4, 2.2, 1.3, 1.8 days, oviposition period 1.5, 1.5, 1.1, 1.1,1.1 days, postoviposition period 2.0, 1.1, 0.9, 0.6, and 0.3 days at th'e temperature of 10, 15, 20, 25 and 28"C, respectively. The longevity of male and female at the temperature was 13.3, 7.8, 5.9,4.1, 3.4 days and10.4, 7.0, 4.2, 3.0, 3.3days, respectively. The optimum temperature for hatchability was estimated to the20$^{\circ}$C and adult emergence was highest at 20$^{\circ}$C. Pupation rate was 50.7, 68.4, 84.3, 86.5, 45.4% at 10, 15,20, 25, and 28"C, respectively. at 10, 15,20, 25, and 28"C, respectively.tively.

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