• Title/Summary/Keyword: Bond strengths

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Effect of the additional application of a resin layer on dentin bonding using single-step adhesives (중간층 레진 적용이 단일 접착과정 상아질 접착제의 접착에 미치는 영향)

  • Choi, Seung-Mo;Park, Sang-Hyuk;Choi, Kyung-Kyu;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.32 no.4
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    • pp.313-326
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    • 2007
  • The purpose of this study was to prove that an intermediate resin layer (IRL) oan increase the bond strength to dentin by reducing the permeability of single-step adhesives. Flat dentin surfaces were created on buccal and lingual side of freshly extracted third molar using a low-speed diamond saw under copious water flow. Approximately 2.0 mm thick axially sectioned dentin slice was abraded with wet #600 SiC paper. Three single-step self-etch adhesives; Adper Prompt L-Pop (3M ESPE, St Paul, MN, USA), One-Up Bond F (Tokuyama Corp, Tokyo, Japan) and Xeno III (Dentsply, Konstanz, Germany) were used in this study. Each adhesive groups were again subdivided into ten groups by; whether IRL was used or not; whether adhesives were cured with light before application or IRL or not; the mode of composite application. The results of this study were as follows; 1. Bond strength of single-step adhesives increased by an additional coating of intermediate resin layer, and this increasement was statistically signigicant when self-cured composite was used (p < 0.001). 2. When using IRL, there were no difference on bond strengths regardless the curing procedure of single-step adhesives. 3. There were no significant difference on bond strengths between usage of AB2 or SM as an IRL. 4. The thickness of Hybrid layer was correlated with the acidity of adhesive used, and the nanoleakage represented by silver deposits and grains was examined within hybrid and adhesive layer in most of single-step adhesives. 5. Neither thickness of hybrid layer nor nanoleakage were related to bond strength.

Comparison of push-out bond strength of post according to cement application methods (시멘트 도포 방법에 따른 포스트의 push-out 접착 강도 비교)

  • Kim, Seo-Ryeong;Yum, Ji-Wan;Park, Jeong-Kil;Hur, Bock;Kim, Hyeon-Cheol
    • Restorative Dentistry and Endodontics
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    • v.35 no.6
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    • pp.479-485
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    • 2010
  • Objectives: The aim of this study was to compare the push-out bond strengths of resin cement/fiber post systems to post space dentin using different application methods of resin cement. Materials and Methods: Thirty extracted human premolars were selected and randomly divided into 3 groups according to the technique used to place the cement into root canal: using lentulo-spiral instrument (group Lentulo), applying the cement onto the post surface (group Direct), and injecting the material using a specific elongation tip (group Elongation tip). After shaping and filling of the root canal, post space was drilled using Rely-X post drill. Rely-X fiber post was seated using Rely-X Unicem and resin cement was light polymerized. The root specimens were embedded in an acrylic resin and the specimens were sectioned perpendicularly to the long axis using a low-speed saw. Three slices per each root containing cross-sections of coronal, middle and apical part of the bonded fiber posts were obtained by sectioning. The push-out bond strength was measured using Universal Testing Machine. Specimens after bond failure were examined using operating microscope to evaluate the failure modes. Results: Push-out bond strengths were statistically influenced by the root regions. Group using the elongation tip showed significantly higher bond strength than other ways. Most failures occurred at the cement/dentin interface or in a mixed mode. Conclusions: The use of an elongation tip seems to reduce the number of imperfections within the selfadhesive cement interface compared to the techniques such as direct applying with the post and lentulospiral technique.

A STUDY ON THE METAL SURFACE TREATMENT OF RESIN BONDED RETAINERS (산부식가공의치(酸腐植架工義齒)의 금속피착면(金屬被着面)에 관(關)한 연구(硏究))

  • Park, Charn-Woon
    • The Journal of Korean Academy of Prosthodontics
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    • v.29 no.2
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    • pp.17-22
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    • 1991
  • The purpose of this study was to evaluate the tensile bond strengths of treated alloy surfaces for resin bonded retainers. For the experiment metal surfaces of 5 alloys were teated with sandblasting, Silicoating Rocatec, and cemented with Visio-Gem. All specimens divided into two groups. The group I specimens were treated with 24-hour immersion in $37^{\circ}C$ distilled water, and group II specimens were teated with 1500 thermo-cycles from $5^{\circ}C\;to\;55^{\circ}C$. The obtained results were as follows: 1. Bond strength values showed significantly different between sandblasting group and other groups after a 24-hour immersion in $37^{\circ}C$ distilled water(P<0.05). 2. All samples were fractured during thermo-cycles for sandblasting group, and bond strength values for Silicoating and Rocatec groups showed significantly different after 1500 thermo-cycles from $5^{\circ}C\;to\;55^{\circ}C$.

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The influence of moisture control on bond strength of self-etching primer

  • Jin, Myoung-Uk;Park, Jeong-Won;Kim, Sung-Kyo
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.587.2-587
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    • 2001
  • The purpose of this study is to evaluate influence of moisture control on bond strength of self-etching primer by measuring enamel and dentin shear bond strengths. 96 extracted human molars were divided into 8 groups. Group 1 (Enamel 30min Dry), Group 2 (E. 5s air dry), Group 3 (E. 1s air dry), Group 4 (E. blot dry), Group 5 (Dentin 30min Dry), Group 6 (D. 5s air dry), Group 7 (D. 1s air dry), Group 8 (D. blot dry) were divided.(omitted)

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Two-dimensional Supramolecular Structures Mediated by Halogen Bonds: Comparing Cl and Br

  • Noh, Seung-Kyun;Chang, Min-Hui;Jeon, Jeong-Heum;Jang, Won-Jun;Yoon, Jong-Keon;Kahng, Se-Jong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.129-129
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    • 2012
  • Covalently bonded halogen ligands possess unusual charge distributions, attracting both electrophilic and nucleophilic molecular ligands to form halogen bonds. In many biochemical systems, halogen bonds coexist with hydrogen bonds, being complementary to them due to their similar bond strength and dissimilardirectionality. In this study, we directly visualize the individual molecular configuration of chlorinated 1,5-dichloroanthraquinone and brominated 1,5-dibromoanthraquinone molecules on Au(111) using scanning tunneling microscopy. The precise arrangements of observed molecular structures were explained in the context of halogen and hydrogen bonds. We discuss the distances and the strengths of the observed halogen and hydrogen bonds, which are consistent with previous bulk data.

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Effect of rewetting agent on dentinal microtensile bond strength

  • Kang, Hee-Young;Cho, Young-Gon
    • Proceedings of the KACD Conference
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    • 2003.11a
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    • pp.568-568
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    • 2003
  • I. Objectives This study investigated the effect of rewetting agent on dentinal microtensile bond strengths(${\mu}TBS$), using one bottle adhesives. II. Materials and Methods Non caries human molars were sectioned to exposed the superficial dentin surfaces, etched 15 seconds using 32% phosphoric acid and 10 seconds rinsed. Samples were randomly divided into two groups according to adhesives (Single Bond, One-Step) used. Each group were subdivided into five groups by different dentin surface treatment:15 second dry(D), blot dry(BD) or 15 second dry and rewetted with distrilled water(DW), Gluma Desensitizer(GD) and Aqua-Prep(AP) during 30 second, respectively.(omitted)

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An Experimental Study on the Effects of Early-Age Vibrations on the Properties of Concrete (진동이 양생중인 콘크리트에 미치는 영향에 관한 연구)

  • 오병환;송혜금;조재열
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.04b
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    • pp.531-537
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    • 1998
  • Recently, the pile driving or blasting works are increasingly done in many areas to perform large scale construction projects. The vibrations from these blasting works may affect the properties of concrete, especially young concrete. The purpose of present study is to explore the effects of vibration at early ages on the properties of concrete. To this end, comprehensive experimental study is conducted in the present study. The major test variables are peak particle velocity or vibration velocity and the age at vibration. The compressive strengths and bond strengths are measured for all the specimens at 28days after casting. The duration of vibration is fixed to 30 minutes for all cases. The results indicate that the strength increases for vibration velocity less than about 0.25cm/sec and decreases for vibration velocity larger than 0.5cm/sec. The effect of age at vibration is not pronounced and shows almost similar behavior for the age at vibration of 0 to 12 hours range. The present study provides some important guidelines to control the construction or vehicle vibrations for the concrete at very early ages.

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Exploring Reliability of Oriented Strand Board's Tensile and Stiffness Strengths

  • Wang, Y.;Young, T.M.;Guess, F.M.;Leon, R.V.
    • International Journal of Reliability and Applications
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    • v.8 no.1
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    • pp.111-124
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    • 2007
  • In this paper, we apply insightful statistical reliability tools to manage and seek improvements in the strengths of Oriented Strand Board (OSB). As a part of the OSB manufacturing process, the product undergoes destructive testing at various intervals to determine compliance with customers' specifications. Workers perform these tests on sampled cross sections of the OSB panel to measure the tensile strength, also called internal bond (IB), in pounds per square inches until failure. Additional stiffness strength tests include parallel and perpendicular elasticity indices (EI), which are taken from cross sectional samples of the OSB panel in the parallel and perpendicular directions with respect to the orientation of the wood strands. We explore both graphically and statistically these "pressure-to-failures" of OSB. Also, we briefly comment on reducing sources of variability in the IB and EI of OSB.

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Forcing a Closer Fit in the Lower Tails of a Distribution for Better Estimating Extremely Small Percentiles of Strengths

  • Guess, Frank-M.;Leon, Ramon-V.;Chen, Weiwei;Young, Timothy-M.
    • International Journal of Reliability and Applications
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    • v.5 no.4
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    • pp.129-145
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    • 2004
  • We use a novel, forced censoring technique that closer fits the lower tails of strenth distributions to better estimate extremly smaller percentiles for measuring progress in continuous improvement initiatives. These percentiles are of greater interest for companies, government oversight organizations, and consumers concerned with safely and preventing accidents for many products in general, but specifically for medium density fiberboard (MDF). The international industrial standard for MDF for measuring highest quality is internal bond (IB, also called tensile strengh) and its smaller percentiles are crucial, especially the first percentile and lower ones. We induce censoring at a value just above the median to weight lower observations more. Using this approach, we have better fits in the lower tails of the distribution, where these samller percentiles are impacted most. Finally, bootstrap estimates of the small percentiles are used to demonstrate improved intervals by our forced censoring approach and the fitted model. There was evidence from the study to suggest that MDF has potentially different failure modes for early failures. Overall, our approach is parsimonious and is suitable for real time manufacturing settings. The approach works for either strengths distributions or lifetime distributions.

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Mechanical Properties of Cork Composite Boards Reinforced with Metal, Glass Fiber, and Carbon Fiber

  • Min-Seong, CHA;So-Jeong, YOON;Jin-Ho, KWON;Hee-Seop, BYEON;Han-Min, PARK
    • Journal of the Korean Wood Science and Technology
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    • v.50 no.6
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    • pp.427-435
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    • 2022
  • For effective applicability of reinforced cork, cork composites reinforced with metal, glass fiber, and carbon fiber were developed, and the effects of the reinforcing materials on the mechanical properties of cork composites were investigated. The bending moduli of elasticity (MOE) of cork composites were in the 32.7-35.9 MPa range, while the bending strength values were in the 1.62-1.73 MPa range. The strength performance decreased in the order cork-metal > cork-carbon fiber > cork-glass fiber. The bending MOEs were improved by 29%-41% compared with simple cork boards, while the bending strengths of reinforced cork were 35%-45% higher. The strength performance significantly improved following the incorporation of thin mesh materials into the middle layer of the studied cork composites. The bending strains of the cork composites were remarkably higher compared with oak wood, making them promising for applications that require bending processing, such as curved jointing. The internal bond strengths of the cork composites were 0.26-0.44 MPa, approximately 0.36-0.60 times lower compared with medium-density fiber boards.