• Title/Summary/Keyword: Average Surface Roughness

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Analysis of PVDF Coating Properties with Addition of Hydrophobically Modified Fumed Silica

  • Lee, Nam Kyu;Kim, Young Hoon;Im, Tae Gyu;Lee, Dong Uk;Shon, MinYoung;Moon, Myung Jun
    • Corrosion Science and Technology
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    • v.18 no.6
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    • pp.232-242
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    • 2019
  • In this study, hydrophobically modified fumed silica was added to the PVDF coating to improve corrosion protection performance. Two types of silane modifiers, trimethylchlorosilane (TMCS) and hexamethyldisilazane (HMDZ), were used for hydrophobic modification of the fumed silica. The composition of modified fumed silica was analyzed by Fourier transform infrared, X-ray photoelectron spectroscopy, and elemental analysis. The dispersion of modified fumed silica in the PVDF coating was observed by the transmission electron microscopy, and the hydrophobicity of PVDF coating was analyzed by the water contact angle. Surface properties were examined by the field emission scanning electron microscopy and scanning probe microscopy. Potentiodynamic polarization was conducted to confirm corrosion protection performance of PVDF coating in terms of hydrophobically-modified fumed silica contents. As a result, the average surface roughness and the water contact angle of the PVDF coating increased with modifier contents. The results of the potentiodynamic polarization test showed an increase of the Ecorr values with increase of the hydrophobicity of PVDF coating. Thus, it clearly indicates that the corrosion protection performance of PVDF coating improved with the addition of the hydrophobic-modified fumed silica that prevents the penetration of moisture into the PVDF coating.

Properties of IZTO Thin Films on Glass with Different Thickness of SiO2 Buffer Layer

  • Park, Jong-Chan;Kang, Seong-Jun;Yoon, Yung-Sup
    • Journal of the Korean Ceramic Society
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    • v.52 no.4
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    • pp.290-293
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    • 2015
  • The properties of the IZTO thin films on the glass were studied with a variation of the $SiO_2$ buffer layer thickness. $SiO_2$ buffer layers were deposited by plasma-enhanced chemical vapor deposition (PECVD) on the glass, and the In-Zn-Tin-Oxide (IZTO) thin films were deposited on the buffer layer by RF magnetron sputtering. All the IZTO thin films with the $SiO_2$ buffer layer are shown to be amorphous. Optimum $SiO_2$ buffer layer thickness was obtained through analyzing the structural, morphological, electrical, and optical properties of the IZTO thin films. As a result, the IZTO surface roughness is 0.273 nm with a sheet resistance of $25.32{\Omega}/sq$ and the average transmittance is 82.51% in the visible region, at a $SiO_2$ buffer layer thickness of 40 nm. The result indicates that the uniformity of surface and the properties of the IZTO thin film on the glass were improved by employing the $SiO_2$ buffer layer and the IZTO thin film can be applied well to the transparent conductive oxide for display devices.

A clindrical post dipping method to fabricate PDMS microlens array (CPD 방식을 통한 PDMS lens의 제작)

  • Lee, Kyoung-Gun;Jang, Yun-Ho;Yoo, Byung-Wook;Jin, Joo-Young;Ha, Joon-Geun;Park, Jae-Hyoung;Kim, Yong-Kweon
    • Proceedings of the KIEE Conference
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    • 2009.07a
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    • pp.1495_1496
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    • 2009
  • A cylindrical post dipping (CPD) method to fabricate the PDMS microlens arrays is presented in this paper. The proposed CPD method is based on the surface tension effect. 2 mm gap and gapless lenses with 2 mm diameter are fabricated and characterized geometically. Both profiles of the fabricated microlens are well-fitted with ideal lens profile. The surface roughness average of the fabricated lens is measured to be 1.953 nm. The focal length of 2mm gap lenses and the gapless lenses is calculated to be 17.00 mm with 0.65 mm standard deviation and 29.88 mm with 2.58 mm standard deviation, respectively. The proposed CPD method can be applied to wafer level lens fabrication due to its simplicity and versatility.

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Synchrotron X-ray Reflectivity Studies on Nanoporous Low Dielectric Constant Organosilicate Thin Films

  • Oh, Weon-Tae;Park, Yeong-Do;Hwang, Yong-Taek;Ree, Moon-Hor
    • Bulletin of the Korean Chemical Society
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    • v.28 no.12
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    • pp.2481-2485
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    • 2007
  • Spatially resolved, quantitative, non-destructive analysis using synchrotron x-ray reflectivity (XR) with subnano-scale resolution was successfully performed on the nanoporous organosilicate thin films for low dielectric applications. The structural information of porous thin films, which were prepared with polymethylsilsesquioxane and thermally labile 4-armed, star-shaped poly(ε-caprolactone) (PCL) composites, were characterized in terms of the laterally averaged electron density profile along with a film thickness as well as a total thickness. The thermal process used in this work caused to efficiently undergo sacrificial thermal degradation, generating closed nanopores in the film. The resultant nanoporous films became homogeneous, well-defined structure with a thin skin layer and low surface roughness. The average electron density of the calcined film reduced with increase of the initial porogen loading, and finally leaded to corresponding porosity ranged from 0 to 22.8% over the porogen loading range of 0-30 wt%. In addition to XR analysis, the surface and the inner structures of films are investigated and discussed with atomic force and scanning electron microscopy images.

An Estimation of Extreme Wind Speed of Typhoon Affecting the Damage of Public and Industrial Facilities (공공 및 산업시설 피해에 영향을 미치는 태풍의 최대풍속 도출)

  • Jung, Woo-Sik
    • Journal of Environmental Science International
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    • v.24 no.9
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    • pp.1199-1210
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    • 2015
  • There were 35 typhoons affecting Korean Peninsula from 1999 to 2009(The average annual number of typhoon is 3.18). Among these typhoons, the number of typhoon passing through the Yellow sea, the Southern sea and the East sea were 14, 6 and 15 respectively. Wind speed on the height of 10 m can be finally estimated using the surface roughness after we calculate wind speed on the height of 300 m from the data on the surface of 700 hPa. From the wind speeds on the height of 10 m, we can understand the regional distributions of strong wind speed are very different according to the typhoon tracks. Wind speed range showing the highest frequency is 10~20 m/s(45.69%), below 10 m/s(30.72%) and 20~30 m/s(17.31%) in high order. From the analysis of the wind speed on the hight of 80 m, we can know the number of occurrence of wind speed between 50 and 60 m/s that can affect wind power generation are 104(0.57%) and those of between 60 and 70 m/s that can be considered as extreme wind speed are even 8(0.04%).

A Study on the Fabrication Method of Mold for 2 inch LCD-BLU by 50μm Microlens : Effect of Different Aspect Ratio (50μm급 마이크로렌즈 적용 2인치 휴대폰 LCD-BLU 금형 개발 : 광학패턴의 세장비 영향)

  • Kim, J.S.;Ko, Y.B.;Min, I.K.;Yu, J.W.;Heo, Y.M.;Yoon, K.H.;Hwang, C.J.
    • Transactions of Materials Processing
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    • v.16 no.1 s.91
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    • pp.48-53
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    • 2007
  • LCD-BLU(Liquid Crystal Display - Back Light Unit) consists of several optical sheets: LGP(Light Guiding Plate), light source and mold frame. The LGP of LCD-BLU is usually manufactured by etching process and forming numerous dots with $50{\mu}m$ in diameter on the surface. But the surface roughness of LGP with etched dots is very high, so there is much loss of light. In order to overcome the limit of current etched dot patterned LGP, optical pattern design with microlens of $50{\mu}m$ diameter was applied in the present study. The microlens pattern fabricated by modified LiGA with thermal reflow process was applied to the optical design of LGP and optical simulation was carried out to know tendency of microlens patterned LGP simultaneously. The attention was paid to the effects of different aspect ratio(i.e. $0.2\sim0.5$) of optical pattern conditions to the brightness distribution of BLU with microlens patterned LGP. Finally, high aspect ratio microlens patterned LGP showed superior results to the one made by low aspect ratio in average luminance.

The Effect of Polymer Thin Film for Sealing Buffer on the Characteristics of OLEO Device (OLED 소자의 특성에 미치는 밀봉 버퍼용 고분자박막의 영향)

  • Lee, Bong-Sub;Ju, Sung-Hoo;Yang, Jae-Woong
    • Journal of the Korean institute of surface engineering
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    • v.41 no.3
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    • pp.102-108
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    • 2008
  • In this paper, the LiF and polymer thin film as passivation layer have been evaporated on green OLED devices. HDPE, polyacenaphthylene, polytetrafluoroethylene, poly(2,6-dimethyl-1,4-pheneylene oxide), poly sulfone and poly(dimer-acid-co-alkyl poly-amine) have been used as polymer materials. The optical transmittance of evaporated polymer thin film was very good as an above 90% in visible range. The morphology of polymer thin film was measured by AFM. As a result of the measurement average roughness($R_a$) value of the polysulfone was very low as 2.2 nm. The green OLED devices with a structure of ITO/HIL/HTL/EML/Buffer/Al in series of various passivation films were fabricated and analyzed. It was observed that an OLED device with LiF as first passivation film has shown the good electrical and optical property, and all kind of polymer films did not influence on the I-V-L characteristics and the life time of OLED devices. Therefore, we found that polymer layer played a key role as a buffer layer between the inorganic passivation layers to relieve the stress of the inorganic layers.

Heat Transfer of a Two-Dimensional Jet Impinging on the Wall with Transverse Repeated Ribs of Square Cross-Section (四角리브를 갖는 傳熱面에 衝突하는 2次元 噴流의 熱傳達에 관한 硏究)

  • 김상필;서정윤
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.11 no.2
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    • pp.214-221
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    • 1987
  • The purpose of this study is augmentation of heat transfer without additional power in the case of rectangular air jet which impinges vertically on the heating surface. The experimental results are obtained heat transfer augmentation of a two-dimensional impinging jet using the surface roughness of transverse repeated-rib type. The integral average heat transfer coefficient of ribbed plate is about two times larger than that of flat plate. In order to supplement the information about the mechanism of heat transfer augmentation, the flow structure in the stagnation region is visually studied by using the smoke wire technique. The heat transfer augmentation is due to the effect of stretching of large scale vortex in the stagnation region.

Study on the growth of boron-doped diamond films in relation to pretreatment processes (전처리 공정에 따른 보론 첨가 다이아몬드 박막의 성장 거동)

  • Mi Young You;Song Hyeon Lee;Pung-Keun Song
    • Journal of the Korean institute of surface engineering
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    • v.57 no.1
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    • pp.1-7
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    • 2024
  • The study investigated the impact of substrate pretreatment on depositing high-quality B-doped diamond (BDD) thin films using the HFCVD method. Films were deposited on Si and Nb substrates after sanding and seeding. Despite identical sanding conditions, BDD films formed faster on Nb due to even diamond seed distribution. Post-deposition, film average roughness (Ra) remained similar to substrate Ra, but higher substrate Ra led to decreased crystallinity. Nb substrate with 0.83 ㎛ Ra exhibited faster crystal growth due to dense, evenly distributed diamond seeds. BDD film on Nb with 0.83 ㎛ Ra showed a wide, stable potential window (2.8 eV) in CV results and a prominent 1332 cm-1 diamond peak in Raman spectroscopy, indicating high quality. The findings underscore the critical role of substrate pretreatment in achieving high-quality BDD film fabrication, crucial for applications demanding robust p-type semiconductors with superior electrical properties.

Study on the Pad Wear Profile Based on the Conditioner Swing Using Deep Learning for CMP Pad Conditioning (CMP 패드 컨디셔닝에서 딥러닝을 활용한 컨디셔너 스윙에 따른 패드 마모 프로파일에 관한 연구)

  • Byeonghun Park;Haeseong Hwang;Hyunseop Lee
    • Tribology and Lubricants
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    • v.40 no.2
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    • pp.67-70
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    • 2024
  • Chemical mechanical planarization (CMP) is an essential process for ensuring high integration when manufacturing semiconductor devices. CMP mainly requires the use of polyurethane-based polishing pads as an ultraprecise process to achieve mechanical material removal and the required chemical reactions. A diamond disk performs pad conditioning to remove processing residues on the pad surface and maintain sufficient surface roughness during CMP. However, the diamond grits attached to the disk cause uneven wear of the pad, leading to the poor uniformity of material removal during CMP. This study investigates the pad wear rate profile according to the swing motion of the conditioner during swing-arm-type CMP conditioning using deep learning. During conditioning, the motion of the swing arm is independently controlled in eight zones of the same pad radius. The experiment includes six swingmotion conditions to obtain actual data on the pad wear rate profile, and deep learning learns the pad wear rate profile obtained in the experiment. The absolute average error rate between the experimental values and learning results is 0.01%. This finding confirms that the experimental results can be well represented by learning. Pad wear rate profile prediction using the learning results reveals good agreement between the predicted and experimental values.