• Title/Summary/Keyword: Average Grain

Search Result 1,149, Processing Time 0.028 seconds

MAGNETIC PROPERTIES OF NANOCRYSTALLINE (Fe,Co)-B-Al-M (M=Nb/Mo/Ta) ALLOYS

  • Kang, D.B.;Cho, W.S.;Kim, T.K.;Cho, Y.S.
    • Journal of the Korean Magnetics Society
    • /
    • v.5 no.5
    • /
    • pp.483-486
    • /
    • 1995
  • Soft magnetic properties of Fe-based (Fe,Co)-B-Al-M (M=Nb, Mo or Ta) nanocrystalline alloy have been investigated. The alloy obtained directly form the rapid solidification process. Microstructure of the alloy is a mixtu re of ultrafine bcc Fe(Co) nanocrystallines and a small amount of retained amorphous phase. Heat treatment of as-prepared alloys improves soft magnetic properties in high frequency range. ${(Fe_{.85}Co_{.15})}_{70}B_{18}Al_{10}Ta_{6}$ alloy alloy annealed at $500^{\circ}C$ for 1 h shows the most improved soth magnetic properties among the alloy examined. Average grain size of the nanocystalline is about 10 nm.

  • PDF

Electrical properties of (Na0.5K0.5)NbO3-BiTiO3 ceramics with the variation of sintering temperature

  • Lee, Tae-Ho;Lee, Sung-Gap
    • Journal of Ceramic Processing Research
    • /
    • v.13 no.spc2
    • /
    • pp.174-176
    • /
    • 2012
  • Piezoelectric 0.93(Na0.5K0.5)NbO3-0.07BiTiO3 (NKN-BTO) ceramics were fabricated by the mixed-oxide method and their structural and dielectric properties was investigated with the variation of sintering temperature. All specimens were crystallized in the perovskite single phase without any formation of a second phase such as pyrochlore. The average grain size of the NKN-BTO specimen sintered at 1130 ℃ is 0.32 ㎛. The specimen sintered at 1100 ℃ showed the highest relative density of 98%. Electromechanical coupling factor, relative dielectric constant and dielectric loss of the NKN-BTO specimens sintered at 1110 ℃ were 0.31, 1222 and 0.02, respectively. Curie temperature of the specimen sintered at 1110 ℃ was 445 ℃.

QUANTITATIVE ANALYSIS OF CRYOMILLED NANOCRYSTALLINE Ti-6Al-4V ALLOY POWDER BY X-RAY DIFFRACTION

  • M. OH;H.K. YU;J.-H. LEE;M.C. OH;S.-H. JUNG;B. AHN
    • Archives of Metallurgy and Materials
    • /
    • v.63 no.3
    • /
    • pp.1439-1442
    • /
    • 2018
  • A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).

Effect of pulse frequency and duty cycle on microstructure, residual stress and mechanical properties of ZrN coatings deposited by mid-frequency magnetron sputtering (펄스 주파수 및 듀티 사이클이 중간 주파수 마그네트론 스퍼터법으로 증착된 ZrN 코팅막의 미세구조, 잔류응력 및 기계적 특성에 미치는 영향)

  • Sung-Yong Chun
    • Journal of Surface Science and Engineering
    • /
    • v.57 no.4
    • /
    • pp.348-354
    • /
    • 2024
  • Nanocrystalline zirconium nitride (ZrN) coatings were deposited by mid-frequency direct current sputtering (mfMS) with varying pulsed plasma parameters such as pulse frequency and duty cycle to understand the effect of pulsed plasma on the microstructure, residual stress and mechanical properties. The results show that, with the increasing pulse frequency and decreasing duty cycle, the coating morphology changed from a porous columnar to a dense structure, with finer grains. Mid-frequency magnetron sputtered ZrN coatings with pulse frequency of 30 kHz showed the highest both nanoindentation hardness of 16.3 GPa, and elastic modulus of 214.4 GPa. In addition, Effect of pulse frequency on a residual stress and average crystal grain sizes was also investigated.

Selection of Rice Cultivars Adaptable to Top Rice Cultivation Region in Southern Part of Korea (남부지방 탑라이스 재배지역에 알맞은 벼 품종 선발)

  • An, Deok-Jong;Won, Jong-Gun;Kim, Se-Jong;Choi, Chung-Don;Lee, Sang-Chul
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.53 no.spc
    • /
    • pp.53-57
    • /
    • 2008
  • The experiment was carried out to select the rice cultivar adaptable to Top Rice cultivation region from 2006 to 2007 in Useong and Kyeongju, Korea. Four cultivars, recommended for high rice grain quality, were cultivated in the different region in this study. The average yield of head rice was higher in Samguangbyeo than the other three cultivars. The protein content was inversely associated with palatability (Toyo value). The protein content of Samguangbyeo was 6.2%, which was the lowest among the tested cultivars. L values in color of rice and cooked rice were not significantly different. The hardness of Samguangbyeo was lower than that of the other cultivars in texture properties of boiled rice on 4 cultivars. In conclusion,considering the rice yield and grain qualities, Samguangbyeo was selected as promising rice cultivar for Top Rice cultivation region.

Effects of Hybrid and Maturity on Maize Stover Ruminal Degradability in Cattle Fed Different Diets

  • Arias, S.;Di Marco, O.N.;Aello, M.S.
    • Asian-Australasian Journal of Animal Sciences
    • /
    • v.16 no.11
    • /
    • pp.1619-1624
    • /
    • 2003
  • The effect of maize hybrid (Suco and Dekalb 765, DK 765), maturity stage (milk, $R_3$ and 1/2 milk line, $R_5$) and animal diet (Diet 1: 70% lucerne hay+30% maize silage; Diet 2: 50% maize silage+20% sunflower meal+30% maize grain) on ruminal stover dry matter (DM) degradability was studied. Additionally, morphological and chemical plant composition was evaluated. Fodder samples ground at 2 mm were incubated in three Holstein steers (400 kg body weight) using the in situ technique. Ruminal degradation kinetics was studied and the effective degradability (ED) was estimated for an assumed kp of 5%/h. The in situ data was analyzed in a complete randomized block design with the animals as blocks. Significant interactions between hybrid${\times}$diet and maturity${\times}$diet on kinetic digestion parameters were detected. In Diet 1, hybrids did not differ in degradable fraction, kd or ED, although a minor difference (p<0.05) in the soluble fraction was found (25.5 and 23.2% for Suco and DK 765, respectively). In Diet 2, the DK 765 had greater degradable fraction (p<0.001) but smaller (p<0.01) kd than Suco, without differences in the soluble fraction or in ED. Anticipating the harvest increased ED of stover from 37.5% in $R_5$ to 44.6% in $R_3$ (average values across hybrids and diets) due to the increase (p<0.001) in the soluble fraction ($R_5$: 22.6%, $R_3$: 28.8%). It is concluded that hybrids had similar stover in situ DM degradability and that soluble fraction represent the main proportion of degradable substrates. Advancing the date of harvesting may not improve the in situ DM degradability of whole maize plant silage since the increase in stover quality is counteracted by the depression in the grain-to-stover ratio. The diet of the animal consuming silage might not improve stover utilization either.

A Study on the Optimum Reheating Profess of A356 Alloy in Semi-Solid Forming (반용융 성형에서 A356합금의 최적 재가열 과정에 대한 연구)

  • Yoon, Jae-Min;Park, Joon-Hong;Kim, Young-Ho;Choi, Jae-Chan
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.19 no.2
    • /
    • pp.114-125
    • /
    • 2002
  • As semi-solid forging (SSF) is compared with conventional easting such as gravity die-easting and squeeze casting, the product without inner defects can be obtained from semi-solid forming and globular microstructure as well. Generally speaking. SSF consists of reheating, forging, ejecting precesses. In the reheating process, the materials are heated up to the temperature between the solidus and liquidus line at which the materials exists in the form of liquid-solid mixture. The process variables such as reheating time, reheating temperature, reheating holding time, and induction heating power have much effect on the quality of the reheated billets. It is difficult to consider all the variables at the same time when predicting the quality. In this paper, Taguchi method, regression analysis and neural network were applied to analyze the relationship between processing conditions and solid fraction. A356 alloy was used for the present study, and the learning data were extracted by the reheating experiments. Results by neural network were on good agreement with those by experiment. Polynominal regression analysis was formulated by using the test data from neural network. Optimum processing condition was calculated to minimize the grain size, solid fraction standard deviation, otherwise, to maximize the specimen temperature average. In this time, discussion is liven about reheating process of row material and results are presented with regard to accurate process variables for proper solid fraction, specimen temperature and grain size.

Synthesis and Properties of La1-xSrxMnO3 System as Air Electrode for Solid Oxide Fuel Cell (고체산화물 연료전지의 공기극으로서 La1-xSrxMnO3 계의 합성 및 특성)

  • Lee, You-Kee;Lee, Young-Ki
    • Korean Journal of Materials Research
    • /
    • v.22 no.9
    • /
    • pp.470-475
    • /
    • 2012
  • $La_{1-x}Sr_xMnO_3$(LSM,$0{\leq}x{\leq}0.5$) powders as the air electrode for solid oxide fuel cell were synthesized by a glycine-nitrate combustion process. The powders were then examined by X-ray diffraction(XRD) and scanning electron microscopy (SEM). The as-formed powders were composed of very fine ash particles linked together in chains. X-ray maps of the LSM powders milled for 1.5 h showed that the metallic elements are homogeneously distributed inside each grain and in the different grains. The powder XRD patterns of the LSM with x < 0.3 showed a rhombohedral phase; the phase changes to the cubic phase at higher compositions($x{\geq}0.3$) calcined in air at $1200^{\circ}C$ for 4 h. Also, the SEM micrographs showed that the average grain size decreases as Sr content increases. Composite air electrodes made of 50/50 vol% of the resulting LSM powders and yttria stabilized zirconia(YSZ) powders were prepared by colloidal deposition technique. The electrodes were studied by ac impedance spectroscopy in order to improve the performance of a solid oxide fuel cell(SOFC). Reproducible impedance spectra were confirmed using the improved cell, which consisted of LSM-YSZ/YSZ. The composite electrode of LSM and YSZ was found to yield a lower cathodic resistivity than that of the non-composite one. Also, the addition of YSZ to the $La_{1-x}Sr_xMnO_3$ ($0.1{\leq}x{\leq}0.2$) electrode led to a pronounced, large decrease in the cathodic resistivity of the LSM-YSZ composite electrodes.

Varietal Variation in Antioxidative Activity of Rice Grain by DPPH and TBA Methods

  • Chung, Ill-Min;Kim, Kwang-Ho;Ahn, Joung-Kuk;Lee, Jin-Ohk
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.45 no.4
    • /
    • pp.261-266
    • /
    • 2000
  • This study was to investigate antioxidative activity of rice grain using 1, 1-Diphenyl-2-picrylhydrazyl(DPPH) and thiobarbituric acid (TBA) method and germination ability for screening rice varieties with high antioxidative activities on korean native and foreign rice varieties harvested in 1998 and 1999. The average antioxidative activity of foreign rice varieties (DPPH 63.5% and TBA 55.2%) was significantly higher than that of native rice varieties (DPPH 47.2% and TBA 45.6%) on varieties harvested in 1999. The promptness index (PI) of native rice varieties was higher in stored rices for three months (mean PI=160.7) than that of stored rices for a year (mean PI=141.6). On the other hand, the PI of foreign rice varieties was higher in stored rices stored for a year (mean PI=176.7) than that of stored rices for three months (mean PI=157.5). Varieties with high redness of hulled rice (a-value) showed significant lipid peroxidation inhibitory activity to DPPH in a stored rices for a year (r=${0.5744}^**$) and stored rices for three months (r=${0.5630}^**$) . These results indicate that the pigments of hulled rice varieties may play important antioxidative roles and colored rice varieties with higher antioxidative potentials can be developed and also may provide information with rice breeder to breed rice variety with a high antioxidative activity for a rapid screening of a small amounts of a large number of samples using color value.

  • PDF

Optimum Transplanting Time for Extremely Early Rice Greenhouse Cultivation in the Southern Area (남부지역 시설하우스 벼 극조기재배의 안전작기 설정)

  • 최장수;안덕종;원종건;이승필;윤재탁;김길웅
    • Korean Journal of Agricultural and Forest Meteorology
    • /
    • v.5 no.3
    • /
    • pp.191-199
    • /
    • 2003
  • Optimum transplanting time for extremely early rice cultivation as an after-crop of fruit and vegetables under greenhouse conditions in the southern area was determined. Rice was transplanted on March 10, March 20, March 30, April 10 and April 20 far three years from 1998 to 2000. Meteorological computations for rice production were high for heading between early May and early July, but they were too low for heading between late July and early August. Especially the expected yield predicted with 35,000 spikelets, the average spikelets per $m^2$ for extremely early transplanting. Computation for heading between late July and early August was low by 106 kg/10a compared with that yield at heading during the same period in the field. As the transplanting date in extremely early rice cultivation was earlier) rice growth at early stages was more retarded by low temperature. Rice growth at heading stage recovered with high temperature, showing less difference for the transplanting date. Abnormal tillers occurred by 15.5∼22.2%. The contribution of 1,000 grain weight${\times}$ripened grain ratio to yield of the extremely early rice cultivation in the greenhouse was 50.6%, indicating 16% hi일or than the degree of panicle per $m^2$ on yield. The estimated optimum transplanting time on the basis of yield for the extremely early greenhouse rice cultivation ranged from March 19 to April 28, and the estimated critical transplanting date on the basis of accumulated effective temperature was March 12. Rice reduced the amount of NO$_3$-N by 97.1% and EC by 90.5% in greenhouse soil with continuous fruit/vegetables fer more than a 10-year period, and completely removed the root-knot nematodes.