• Korean Journal of Materials Research
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• v.8 no.11
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• pp.1031-1037
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• 1998

To investigate the effect of cooling rate and annealing temperature on the corrosion of Zircaloy-4 and Zr-2. 5Nb alloys, autoclave corrosion tests were performed at $500^{\circ}C$ for the specimens prepared by various heat treatments. The specimens were heat-treated at $1050^{\circ}C$ for 30 minutes and cooled by ice-brine quenching, water quenching, oil quenching, air cooling, and furnace cooling. To investigate the effect of annealing temperature, the specimens were annealed at $\alpha$, ($\alpha$+$\beta$)-, and $\beta$-temperatures. It was observed from the $500^{\circ}C$ corrosion test that nodular corrosion occurred on the Zircaloy-4 alloy but did not occur on the Zr-2.5Nb alloy. The corrosion resistance of Zircaloy-4 increased with increasing the cooling rate. On the other hand, the corrosion resistance of Zr-2.5Nb decreased with increasing the cooling rate and the annealing temperature. It is suggested that corrosion resistance of Zircaloy-4 would be controlled by the distribution of Fe and Cr element in the matrix and precipitates, while that of Zr-2.5Nb alloy the niobium concentration and $\beta_{-Nb}$ phase.

• Composites Research
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• v.32 no.5
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• pp.199-205
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• 2019

The composite material has the advantage that the fibers can be arranged in a desired direction and can be manufactured in one piece. However, micro voids can be formed due to micro air, moisture or improper curing temperature or pressure, which may cause the deterioration in mechanical strength. In this paper, the composite panels with different thicknesses were made by varying the curing pressure in an autoclave vacuum bag process and their microporosities were evaluated. Microporosity was measured by image analysis method, acid digestion method, and combustion method and their correlation with ultrasonic attenuation coefficient was analyzed. From the test results, it was found that the acid digestion method had the highest accuracy and the lower the curing pressure, the higher the microporosity and the ultrasonic attenuation coefficient. In addition, the microporosity and the ultrasonic attenuation coefficient were increased as the thickness of the composite panel was increased at the same curing pressure.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2002.11a
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• pp.87-91
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• 2002

This paper investigates the corrosion inhibition and the reduction of hydration heat properties of Ground Granulated Blast-Furnace Slag (GGBFS) added concrete. Since the massive civil structure is vulnerable to the thermal crack by hydration. adiabatic temperature rising tests were performed for water-binder ratios from 43.2% to 47.3%, while replacing 15% to 50% of cement with GGBFS of equal weight. Then, the corrosion protection performance was evaluated using cylindrical specimens embedded with steel reinforcement according to the combination of 3 W/B ratios and 2 levels of chloride ion quantity. The corrosion area of the embedded steel ban was determined using the high pressure steam curing method specified in KS F 2561. The test results showed that the replacement of GGBFS was effective in reducing the hydration heat. The corrosion area of the embedded steel ban decreased as the replacement of GGBFS increased. However, the corrosion area of the steel bar was proportional to the autoclave cycle and the chloride ion quantity. Among the tested specimens, compressive strength, reduction of hydration heat, and corrosion inhibition performance were excellent when 50% of cement was replaced with GGBFS of equal weight.

• Composites Research
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• v.24 no.4
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• pp.48-54
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• 2011

The effect of moisture contents by salt water on the strength of composite single-lap bonded joints is investigated. The specimens were manufactured in an autoclave by secondary bonding and immersed in the 3.5% salt water of $71^{\circ}C$ for different durations to get various moisture contents; 0, 0.2, 0.5, 1.0, and 2.0%(saturation). A total of 80 joint specimens were tested for 5 different moisture contents and 2 temperature environments. Test results show that while the joint strengths after the saturation of moisture decrease compared to those of dry ones, the strengths of the pre-saturated joint up to 1.0% of moisture content increase in both room and elevated temperature conditions. It is also shown that the strengths of joints tested in elevated temperature are slightly higher than the strength in room temperature by 2-5% until the moisture content reaches 1 %. In contrast, the high temperature strength of the saturated joint is about 5% lower than the room temperature strength.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.10a
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• pp.1434-1439
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• 2004

CFRP composite materials have wide application in structure materials of airplane, ships, and aero space vehicles because of their high strength and stiffness. This paper is to study the effects of curvature and orientation angle on the penetration characteristics of CFRP laminate shell. They are staked with 8 Ply specimens [0$_2$/90$_2$]$_{s}$, [0/90$_2$/0]$_{s}$ and the stacked of outer plates degree with 12 Ply specimens [0$_3$/90$_3$]$_{s}$, [0$_2$/90$_2$/0]$_{s}$ and [90$_3$/0$_3$], [90$_2$/0$_2$/90]S. They are manufactured to varied curvature radius (R=100,150,200mm and $\infty$). They are cured by heating to the appropriate harding temperature(13$0^{\circ}C$) by mean of a heater at the vaccum bag of the autoclave. Test specimens were prepared with dimensions 100mm$\times$140mm. When the specimen is subjected to transverse impact by a steel ball, the velocity of the steel ball was measured both before and after impact by determining the time for it to pass two ballistic-screen sensor located a known distance apart. In general, kinetic energy after impact-kinetic energy before impact rised in all specimens. This study observed a fracture mode inside the specimen after a penetration test using a digital camera and it examined a fracture mode and a penetration mode to stack of outer orientation angle and curvature.rvature.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.5
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• pp.619-624
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• 2013

A bendable electronic module is developed. In this module, thin silicon electronic chips are embedded in a polymer-based encapsulating adhesive between flexible copper-clad polyimide layers. During the qualification test of a harshly thermal-hygroscopic complex loading condition, delaminations occur inside the module layers. A finite element model is developed for the module. To investigate the effect of hygroscopic stress on delamination, the results of the thermal and thermal-hygroscopic loads are compared. The analysis results reveal that the hygroscopic effect more strongly affects delamination than does the thermal effect. The potential failure mechanisms of the module are investigated based on the stress analysis.

• Journal of the Korean Recycled Construction Resources Institute
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• v.2 no.2
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• pp.137-144
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• 2014

The PHC pile utilizing the air-cooled blast-furnace slag as coarse aggregate was studied. This research was progressed with the range from the indoor mixing design evaluation into the actual goods production. The physical properties of the PHC pile are determined to satisfy through the appropriate mixing design adjustments. However, it should eliminate the aggregates including CaO and MgO in SG when it utilize in an AC (autoclave) type manufacturing process. It satisfied the bending moment, shear strength, and compressive strength of KS F 4306 except the surface states of the pile.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.10
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• pp.1514-1519
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• 2001

This paper is concerned with design, manufacturing and performance test of LIPCA ( Lightweight Piezo- composite Curved Actuator) using a top carbon fiber composite layer with near -zero CTE(coefficient of thermal expansion), a middle PZT ceramic wafer and a bottom glass/epoxy layer with high CTE. The main point of this design is to replace the heavy metal layers of THUNDER by thigh tweight fiber reinforced plastic layers without losing capabilities to generate high force and large displacement. It is possible to save weight up to about 30% if we replace the metallic backing material by the light fiber composite layer. We can also have design flexibility by selecting the fiber direction and the size of prepreg layers. In addition to the lightweight advantage and design flexibility, the proposed device can be manufactured without adhesive layers when we use epoxy resin prepreg system. Glass/epoxy prepregs, a ceramic wafer with electrode surfaces, and a graphite/epoxy prepreg were simply stacked and cured at an elevated temperature (177 $^{circ}C$ after following an autoclave bagging process. It was found that the manufactured composite laminate device had a sufficient curvature after detached from a flat mold. The analysis method of the cure curvature of LIPCA using the classical lamination theory is presented. The predicted curvatures are fairly in agreement with the experimental ones. In order to investigate the merits of LIPCA, a performance test of both LIPCA and THUNDE$^{TM}$ were conducted under the same boundary conditions. From the experimental actuation tests, it was observed that the developed actuator could generate larger actuation displacement than THUNDERT$^{TM}$.

• Composites Research
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• v.23 no.6
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• pp.61-66
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• 2010

In this paper, the variation of mechanical properties of T800 carbon/epoxy composites according to the forming pressure, which was referred to previous studies on a filament winding process, were investigated. The specimens of all the tests were fabricated by an autoclave de-gassing molding process controlling forming pressure (absolute pressures of 0.1MPa, 0.3MPa, 0.7MPa including vacuum) and water jet cutting after fabricating composite laminates. Various tensile tests were performed for in-plane properties and interlaminar properties were also measured by using Iosipescu test jig. Fiber volume fraction was measured to correlate the property variation and the forming pressure. This properties are expected to be utilized in the design of Type III pressure vessel for hydrogen vehicles which uses the same carbon fiber (T800 carbon fiber) for the filament winding process.

• Composites Research
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• v.36 no.2
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• pp.132-139
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• 2023

A linerless composite propellant tank was designed and manufactured by using the carbon fiber-reinforced composite materials which have superior strength-to-weight ratio in order to reduce weight of the tank. In this research, we designed a sub-scale composite propellant tank with a diameter of 800 mm to withstand an MEOP of 1.7 MPa. We manufactured the boss of the tank by using the same composite materials to reduce the thermal expansion difference between the boss and the secondary-bonded composite layers of the barrel in the cryogenic environment. We used the collapsible mandrel to manufacture the tank without any liner. The mandrel was made from epoxy-based composite tooling prepregs to reduce weight of the mandrel. We manufactured the test tanks by laying up the carbon fiber fabric prepregs manually on the mandrel and then applying the autoclave cure process. We performed a proof test, a helium tightness test, a repeated pressurization test, and a burst test in room temperature. The test results demonstrate that the proposed design and manufacture process satisfies all strength requirements as well as an anti-leakage requirement.