• 열처리공학회지
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• 제7권1호
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• pp.44-52
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• 1994

In order to investigate the effect of tempring treatment on the mechanical properties of ausformed martensite in Fe-30%Ni-0.35%C alloy, the hardness, yield strength and elongation were examined by tensile test. 1. The strength of deformed austenite in Fe-30%Ni-0.35%C alloy was increased due to the work hardening induced from the dislocation density increased during deformation. The strength of ausformed martensite was increased because of defects inherited from deformed austenite by martensitic transformation. 2. The ductility of ausformed martensite was shown a nearly constant values independent of deformation degrees because of the interaction of multiple factors such as increased retained austenite, formation of void and decrement of twin in ausformed martensite. 3. The strength of ausformed martensite by tempering treatment was shown a little decrement up to $340^{\circ}C$, especially showed remarkable softening resistance in higher deformation degrees. 4. Virgin martensite and ausformed martensite were shown a maximum yield strength by clustering in tempering at $100^{\circ}C$ and above $100^{\circ}C$, yield strength was very small decreased due to the decrement of solute carbon by the destruction of clustering. 5. The decomposition of retained austenite was not shown up to $450^{\circ}C$ in ausformed martensite with tempering treatment, and the matrix was rapidly softening because of the decomposition of martensite and the formation of reversed austenite with tempering above $400^{\circ}C$.

• 열처리공학회지
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• 제7권2호
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• pp.88-95
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• 1994

In order to compare mechanical properties of ausformed martensite with those of marformed martemsite in Fe-30%Ni-0.1%C alloy and to investigate their strengthening mechanisms, ausformed martensite and marformed martensite were prepared by ausforming treatment and marforming treatment respectively. The microstructures were observed and the quantities of retained austenite, hardness, yield strength, ultimate tensile strength and elongation were examined. The strength of ausformed martensite was mainly increased because of the lattice defects inherited from austenite. The ductility of ausformed martensite was constant at the rate of 7-8% by ductile matrix formation of the retained austenite in spite of the increase in strength. The strength of marformed martensite was increased by the increment in dislocation density, the crossing of transformation twin with deformation twin and the mutual crossing of deformation twin. The ductility of mar formed martensite was slightly lower than that of ausformed martensite, but the strength of mar formed martensite was prominently higher.

• 열처리공학회지
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• 제6권1호
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• pp.26-36
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• 1993

In this study, the ausformed martensite and marformed martensite obtained from austenite with various deformation degrees in Fe-31% Ni-0.2%C alloy were transformed to revesed austenite at $510^{\circ}C$ by cyclic reverse martensite transformation. The effect of prior deformation, the rapid heating rate of reversion and number of cyclic transformation on the microstructure, mechanical properties of reversed austenite were investigated. The reverse austenite transformation is accomplised by the mechanism of shear type transformation. The structure of reversed austenite formed from ausformed martensite and marformed martensite with high deformation degrees is a fine structure of nearly equiaed grain containg a high density of dislocation tangles and was largely affected by the prior deformation applied before reversal transformation. The strength of reversed austenite is more increased with of cyclic transformation especially it is strength at the first cyclic transformation. The yield stress of revesed austenite of ausformed martensite is lower than that of marformed martensite.

• 열처리공학회지
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• 제12권4호
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• pp.313-319
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• 1999

The reverse transformation behavior was investigated by DSC analysis in thermomechanically processed Fe-30%Ni-0.35%C alloy. Upon increasing the heating rate from $5^{\circ}C/min$ to $80^{\circ}C/min$, the As point of the ausformed martensite was not changed and the As point of the marformed martensite decreased at reverse transformation. The Af points showed to be constant with increasing the heating rate both in the ausformed martensite and in the marformed martensite. With increasing the deformation degree, the As points of the ausformed martensite and the marformed martensite increased and the Af points appeared to be constant, structures. The enthalpy changes increased with increasing the heating rate, but decreased with increasing the deformation degree in both structures.

• 열처리공학회지
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• 제11권2호
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• pp.75-81
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• 1998

The effect of thermomechanical treatment on thermal expantion and melting point of Fe-30%Ni-0.35%C alloy was investigated. The dimention changes of the ausformed martensite and the marformed martensite were decreased with increasing deformation degree in the range of $25{\sim}350^{\circ}C$ prior to reverse transformation but became larger in the range of $500{\sim}800^{\circ}C$ after the reverse transformation. The dimension change and the thermal expansion coefficient were reduced in the order of the deformed austenite, the marformed martensite and the ausformed martensite in the range of $25{\sim}800^{\circ}C$. Therefore, the ausforming treatment is more effective than the marforming treatment in improving the heat-resistance. The melting points of the deformed austenite, the ausformed martensite and the marformed martensite were lowered as either the heating rate or the degree of deformation was increased.

• 한국재료학회지
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• 제10권6호
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• pp.392-397
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• 2000

Fe-30Ni-0.35C 합금과 몇가지 저융점 순금속의 상변태에 미치는 압력의 영향에 대하여 PDSC를 이용하여 조사하였다. Fe-30Ni-0.35C 합금의 오스폼트 마르텐사이트 및 마르폼드 마르텐사이트 오스테나이트로 역변태시 압력이 1 기압에서 60기압으로 증가하에 따라. $A_s$점이 약 $2~4^{\circ}C$ 저하하며, 이것은 상전이시의 체적변화가 음의 값이 되기 때문이다. 또한 $A_f$ 점은 압력이 증가함에 따라 변함없이 일정하거나 매우 미소한 상승을 나타내는데, 이것은 압력이 증가할수록 탄화물의 석출이 촉진되기 때문이다. Fe-30Ni-0.35C 합금의 오스폼드 마르텐사이트의 역변태시 엔탈피변화는 압력이 1 기압에서 60기압으로 상승함에 따라 10~14J/g 증가한다. 순금속 Se, Sn, Pb, Zn, Te 등의 용융점은 압력이 1기압에서 60기압으로 증가함에 따라 매우 완만하게 상승하며, 용융시의 엔탈피변화는 압력의 증가에 따라 거의 변화가 없거나 미소 증가를 나타낸다.

• 열처리공학회지
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• 제3권4호
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• pp.1-9
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• 1990

In this study, the ausformed martensite cooled to $-196^{\circ}C$ with various deformation degrees in Fe-30%Ni-0.24%C alloy was transformed to reversed austenite at $500^{\circ}C$ by cyclic reverse martensitic transformation. The effects of prior deformation and the number of cyclic reverse transformation on the microstructure and the mechanical properities of reversed anstensite were investigated. Experimental results showed that the strength of reversed austenite was higher than that of original austenite. This is due to higher dislocation density and grain refining. The reversed austenite formed from ausformed martensite was highly strengthened by prior deformation. This strengthening effect of reversed austenite is attributed to higher dislocation density than grain fefining. The yield strength of reversed austenite below 30% prior deformation, but above 30% prior deformation the strength of reversed austenite is lower than that of deformed austenite. This is due to partly disappearance of strain hardening effect at higher deformation degree by reverse transformation. The strength of reversed austenite is increased with the number of cyclic transformation. Especially, it is principally strengthened by the first cyclic transformation and shows higher increase in yield strength than that of ultimate tensile strength.

• 열처리공학회지
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• 제34권4호
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• pp.179-184
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• 2021

Two types of secondary hardening martensitic steels, 10Co-14Ni and 6Co-5Ni, were produced by vacuum induction melting to investigate the effect of ausforming process on mechanical properties. According to the results of present study, the alloy samples ausformed at low temperature indicated a rather low hardness level in overall aging time despite the refinement of martensite lath width. As the result can closely be related with the presence of primary carbides precipitated within the initial austenite matrix, we confirmed that, in ultrahigh strength secondary hardening martensitic alloy steels, the ausforming process can rather limit the degree of secondary hardening during the subsequent aging treatment.