• Title/Summary/Keyword: Attrition mill

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The Effects of Ball Size on Attritor Efficiency in the Processing of RBAO Ceramics (RBAO 세라믹스 공정에서 어트리터 효율에 미치는 볼 크기의 영향)

  • 김일수;강민수;박정현
    • Journal of the Korean Ceramic Society
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    • v.35 no.4
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    • pp.406-412
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    • 1998
  • The reaction bonded alumina ceramics was prepared through the addition of each SiC and ZrO2 powder to the mixture of Al metal powder and Al2O3 The mono sized (3mm) and biodal sized (3mm+5mm) balls were used in attrition milling of Al and starting powders. The milling efficiency of both cases was compared by the analysis of particle size and X-ray diffraction. After the forming and sintering of each powder batchs the weight gains dimensional changes and densities were determined. The specimens were investigated by X-ray diffraction analysis and scanning electron microscope. Bimodal sized balls had better milling effect than single ball size in the milling of Al powder. However in the milling which ceramic powders mono sized the green body during the reaction sintering at 1$600^{\circ}C$ for 5 hour was about 10% The densities attained the values of 92-98% theoretical. The SiC added specimen that was milled with 3mm ball media had 96% theoretical density and dense microstructure.

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Coarsening of Dispersoid and Matrix Phase in Mechanically Alloyed ODS NiAl (기계적 합금화된 ODS NiAl에서 분산상 및 기지상의 조대화 거동)

  • 어순철
    • Journal of Powder Materials
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    • v.4 no.1
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    • pp.48-54
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    • 1997
  • NiAl powders containing oxide dispersoids have been produced by mechanical alloying process in a controlled atmosphere using high energy attrition mill. The powders have been consolidated by hot extrusion and hot pressing followed by isothermal annealing to induce microstructure coarsening to improve high temperature properties. Grain growth and dispersoid coarsening kinetics have been investigated as functions of annealing time and temperature. Coarsening of dispersion strengthen NiAl and dispersoid has been discussed. Some clues of secondary recrystallization have been investigated. Mechanical property measurements have been also made and correlated with the microstructures.

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A study on Flotation of Crystalline Graphite by Microbubble Column (Microbubble Column에 의한 인상흑연(鱗狀黑鉛)의 부선(浮選)에 관한 연구(硏究))

  • Han, Oh-Hyung;Kang, Hyun-Ho
    • Resources Recycling
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    • v.15 no.2 s.70
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    • pp.37-44
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    • 2006
  • The total amount of graphite reserves in Korea is about 260 thousand tons. Graphite larks international competitiveness it is mined in only few mines, but recently the demand of portable electronic has increased. Therefore a research for manufacturing domestic high purity graphite is necessary because all of high purity graphite used electrode of 2nd batter depends on expensive importation. A preprocessing level for producing high purity graphite, flotation was conducted using microbubble column machine. In this research $D_{50}=10.314{\mu}m$ sample was used which was produced after grinding 29.50% F.C. primary crushing sample($D_{50}=69.393{\mu}m$) for 20 minutes through attrition mill. As a result using this sample, product above 95% F.C. with recovery over 90% was obtained with only after first stage process through the microbubble column.

Micronization of Ceramic Pigments for Digital Ink-Jet Printing Process (디지털 프린팅 공정을 위한 세라믹 안료의 미립화 거동 분석)

  • Lee, Ji-Hyeon;Hwang, Hae-Jin;Kwon, Jong-Woo;Kim, Jin-Ho;Hwang, Kwang-Taek;Han, Kyu-Sung
    • Korean Journal of Materials Research
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    • v.27 no.2
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    • pp.82-88
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    • 2017
  • Ink-jet printing techniques with ceramic ink, which contains ceramic pigments as colorant, are in increasingly use in the ceramic industry. Generally, ceramic pigments that are produced by conventional method show diameters of several micrometers; these micrometer sized particles in the ink-jet printing process can cause undesirable behavior such as print head nozzle clogging. To prevent this problem, a particle size reduction process is required. In this study, CMYK (cyan, magenta, yellow, black) pigments were synthesized via solid state method. Each pigment particle was milled to submicron size by an attrition mill. The effects of micronizing on the morphology, mechanical property, crystal structure and color property of the CMYK ceramic pigments were investigated by field emission scanning electron microscopy (FE-SEM), particle size analysis (PSA), X-ray diffraction (XRD) and CIE $L^{\ast}a^{\ast}b^{\ast}$.

The Effect of a CAM Treatment on the Sinterability of UO2 Powder (연속형 아트리션 밀링 처리가 UO2 분말의 소결성에 미치는 영향)

  • Moon, Je-Sun;Na, S.H.;Kang, K.H.;Park, C.S.;Song, K.C.
    • Journal of Powder Materials
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    • v.14 no.1 s.60
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    • pp.8-12
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    • 2007
  • The effect of a CAM (Continuous Attrition Mill) treatment on the sinterability of ex-ADU $UO_2$ powder was investigated. As the cycles of a CAM increased, the apparent density, specific surface area and O/U of the milled powder increased, but there particle sizes decreased. However the sintered density of the $UO_2$ pellet decreased as the cycles of the CAM increased. It is considered that the decrease of the sintered density is due to the formation of $U_3O_8$, which was produced by a CAM mechanism.

The Characteristic Changes of Electromagnetic Wave Absorption in Fe-based Nanocrystalline P/M Sheet by the Additions of BaTiO3 Powder and Dispersant (BaTiO3 분말과 분산제 첨가에 따른 Fe계 나노결정 P/M시트의 전자파흡수 특성변화)

  • Kim, Mi-Rae;Cho, Hyeon-Jeong;Park, Won-Wook
    • Journal of Powder Materials
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    • v.15 no.1
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    • pp.53-57
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    • 2008
  • The amorphous $Fe_{73}Si_{16}B_7Nb_3Cu_1$(at%) alloy strip was pulverized using a jet mill and an attrition mill to get flake-shaped powder. The flake powder was mixed with dielectric $BaTiO_3$ powder and its dispersant to increase the permittivity. The powders covered with dielectric powders and its dispersant were mixed with a binder and a solvent and then tape-cast to form sheets. The absorbing properties of the sheets were measured to investigate the roles of the dielectric powder and its dispersant. The results showed that the addition of $BaTiO_3$ powders and its dispersant improved the absorbing properties of the sheets noticeably. The powder sheet mixed with 5 wt% of $BaTiO_3$ powder and 1 wt% of dispersant showed the best electromagnetic wave absorption rate because of the increase of the permittivity and the electrical resistance.

Secondary Recrystallization Behavior in Mechanically Alloyed ODS NiAI (기계적 합금화한 ODS NiAI의 이차 재결정화 거동)

  • Eo, Sun-Cheol
    • Korean Journal of Materials Research
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    • v.6 no.12
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    • pp.1248-1256
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    • 1996
  • Ni 및 AI단원소 분말을 혼합하여 attrition mill을 사용하여 분위기 속에서 기계적 합금화 NiAI 기 산화물 분산강화 금속간화합물을 제조하였다. 제조된 분말은 여러 가지 다른 미세조직을 얻기 위하여 각기 다른 공정으로 열간성형을 하였으며, 연이어 이차 재결정 조직을 얻기 위한 가공열처리(thermomechanical treatment)를 실시하였다. 이차 재결정이 일어날 수 있는 선수조건으로서의초기 미세조직과 가공열처리와의 상관관계를 조사하였다. 정상 결정립 성장의억제와 접합조직의 존재가 이차 재결정을 일으키기 위한 필요조건으로 판명되었다. 이 재료에 있어서, 잔류 변형에너지를 공급할 수 있고 결정립을 미세화 할 수 있는 특정 공정하에서 항온 열처리 후 이차 재결정이 생성됨을 알 수 있었다.

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A Study of Production, Hot Consolidation, Secondary Recrystallization and Mechnical Property Assesment of Mechanically Alloyed $NiAl-Fe-AiN-Al_2O_3$ (기계적 합금화에 의한 $NiAl-Fe-AIN-Al_2O_3$ 합금분말의 제조, 열간 성형, 이차재결정화 및 기계적 성질 평가에 관한 연구)

  • 이순철
    • Journal of Powder Materials
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    • v.6 no.1
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    • pp.111-118
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    • 1999
  • Ni(Fe)Al powders containing a homogeneous distribution of the in-situ formed AIN and $Al_2O_3$ dispersoids have been produced by mechanical alloying process in a controlled atmosphere using high energy attrition mill. The powders have been successfully consolidated by hot extrusion process. The phase information investigated by TEM and XRD analysis reveals that Fe can be soluble up to 20% to the NiAl phase ($\beta$) at room temperature after MA process. Subsequent thermomechanical treatment under specific condition has been tried to induce secondary recrystallization (SRx) to improve high temperature properties, however, the clear evidence of SRx was not obtained in this material. Mechanical properties in term of strength at room temperature as well as at high temperatures have been improved by the addition pf AIN, and the room temperature ductility has been shown to be improved after heat treatment, presumably due to the precipitation of second phase of $\alpha$ in this material.

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Measurement and Analysis of Conduction Noise through Microstrip Line Attached with Composite Sheets of Iron Particles and Rubber Matrix (마이크로스트립 전송선로를 이용한 순철 압분체-고무 복합재의 전도노이즈 흡수특성 측정 및 해석)

  • Kim, Sun-Tae;Oh, Byung-Ki;Kim, Sung-Soo;Cho, Han-Sin;Lee, Jae-Hee
    • Journal of the Korean Magnetics Society
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    • v.14 no.5
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    • pp.174-179
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    • 2004
  • Attenuation of conduction noise through microstrip line attached with the high lossy iron flakes-rubber composites has been investigated in GHz frequencies. Microstrip line was designed with characteristic impedance of 50 $\Omega$ and a length corresponding to the center frequency of 3 GHz. Iron flakes were fabricated by mechanical forging of spherical iron powders using an attrition mill. The fabricated microstrip line shows a ideal propagation characteristics of S$\sub$11/ < -60 dB and S$\sub$21/ = 0 dB. Attaching a noise absorbing sheet on the microstrip line, S$\sub$11/ increases to about -10 dB and S$\sub$21/ decreases to -20~-60 dB depending on the length of absorbing sheet. The calculated power loss is as high as 80% in the frequency range 2~8 GHz. It is suggested that the most critical material parameter is magnetic loss for the enhancement of noise attenuation.

Analysis of Properties of Flake Sendust EM Wave Absorber according to Granularity (입도에 따른 Flake Sendust 전파 흡수체의 특성 분석)

  • Park, Soo-Hoon;Kim, Dong-Il;Choi, Dong-Han;Kim, Seong-Yeon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.19 no.9
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    • pp.1051-1057
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    • 2008
  • In this paper, we analyzed the characteristics of the EM wave absorber which was fabricated by using flake sendust (soft metal magnetic powder). The flake sendust was made of 3 different granularity by attrition mill. First, we have fabricated 3 kind of EM wave absorbers using the flake sendust and CPE(Chlorinated Polyethylene) and measured the S-parameters of the EM wave absorber. The complex relative permittivity and permeability were calculated from the measured data and the variations according to a change of granularity were researched. As a result, it was confirmed that the EM wave absorber using flake sendust with the $140{\mu}m$ average granularity has outstanding absorption ability in high frequency range(C band) for the reduction of eddy current loss(increase of permeability) and the increase of space charge polarization(increase of permittivity).