• Title/Summary/Keyword: Applied Mechanics of Materials

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Electromechanical Properties of Conductive MWCNT Film Deposited on Flexible Substrate Affected by Concentration of Dispersing Agent (분산제 농도에 따른 MWCNT 전도성 유연필름의 전기-기계적 특성)

  • HwangBo, Yun;Kang, Yong-Pil;Kim, Jae-Hyun;Kim, Duck-Jong;Lee, Hak-Joo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.36 no.5
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    • pp.517-521
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    • 2012
  • Carbon nanotubes (CNTs) have been regarded as a promising material for the fabrication of flexible conductors such as transparent electrodes, flexible heaters, and transparent speakers. In this study, a multiwalled carbon nanotube (MWCNT) film was deposited on a polyethylene terephthalate (PET) substrate using a spraying technique. MWCNTs were dispersed in water using sodium dodecyl sulfate (SDS). To evaluate the effect of the weight ratio between SDS and MWCNTs on the electromechanical properties of the film, direct tensile tests and optical strain measurement were conducted. It was found that the CNT film hardly affected the mechanical behavior of CNT/PET composite films, while the electrical behavior of the CNT film was strongly affected by the SDS concentration in the CNT film. The electrical resistance of CNT/PET films gradually increased with the strain applied to the PET substrate, even up to a large strain that ruptured the substrate.

Development of High-Temperature Solders: Contribution of Transmission Electron Microscopy

  • Bae, Jee-Hwan;Shin, Keesam;Lee, Joon-Hwan;Kim, Mi-Yang;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.45 no.2
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    • pp.89-94
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    • 2015
  • This article briefly reviews the results of recently reported research on high-temperature Pb-free solder alloys and the research trend for characterization of the interfacial reaction layer. To improve the product reliability of high-temperature Pb-free solder alloys, thorough research is necessary not only to enhance the alloy properties but also to characterize and understand the interfacial reaction occurring during and after the bonding process. Transmission electron microscopy analysis is expected to play an important role in the development of high-temperature solders by providing accurate and reliable data with a high spatial resolution and facilitating understanding of the interfacial reaction at the solder joint.

Toughnening of Dielectric Material by Thermoplastic Polymer

  • Lee, Jung-Woo;Cho, Jae-Choon;Ra, Seung-Hyun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.207-208
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    • 2007
  • Recently, high performance microelectronic devices are designed in multi-layer structure in order to make dense wiring of metal conductors in compact size. Imprint lithography have received significant attention due to an alternative technology for photolithography on such devices. In this work, we synthesized dielectric composite materials based on epoxy resin, and investigated their thermal stabilities and dynamic mechanical properties for thermal imprint lithography. In order to enhance the mechanical properties and toughness of dielectric material, various modified polyetherimide(PEI) was applied in the resin system. Curing behaviours, thermal stabilities, and dynamic mechanical properties of the dielectric materials cured with various conditions were studied using dynamic differential scanning calorimetry (DSC), thermo gravimetric analysis (TGA), and Universal Test Method (INSTRON).

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Effect of initial coating crack on the mechanical performance of surface-coated zircaloy cladding

  • Xu, Ze;Liu, Yulan;Wang, Biao
    • Nuclear Engineering and Technology
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    • v.53 no.4
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    • pp.1250-1258
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    • 2021
  • In this paper, the mechanical performance of cracked surface-coated Zircaloy cladding, which has different coating materials, coating thicknesses and initial crack lengths, has been investigated. By analyzing the stress field near the crack tip, the safety zone range of initial crack length has been decided. In order to determine whether the crack can propagate along the radial (r) or axial (z) directions, the energy release rate has been calculated. By comparing the energy release rate with fracture toughness of materials, we can divide the initial crack lengths into three zones: safety zone, discussion zone and danger zone. The results show that Cr is suitable coating material for the cladding with a thin coating while Fe-Cr-Al have a better fracture mechanical performance in the cladding with thick coating. The Si-coated and SiC-coated claddings are suitable for reactors with low power fuel elements. Conclusions in this paper can provide reference and guidance for the cladding design of nuclear fuel elements.

Guidelines for Joint Depth Determination and Timing of Contraction Joint Sawcutting for JCP Analyzed with Fracture Mechanics

  • Yang, Sung-Chul;Hong, Seung-Ho
    • International Journal of Concrete Structures and Materials
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    • v.18 no.3E
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    • pp.145-150
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    • 2006
  • An experiment with the objective of providing guidelines for joint depth determination and timing of contraction joint sawcutting to avert uncontrolled cement concrete pavement cracking has been conducted. Theoretical analysis and laboratory tests were performed to help in understanding and analyzing the field observation. Using two-dimensional elastic fracture mechanics, the influence of several parameters on crack propagation was delineated by a parametric study, involving initial notch ratio, joint spacing, Young's modulus and thermal expansion coefficient of concrete, temperature gradient, and modulus of subgrade reaction. Bimaterials made of rock plus cement mortar and rock plus polymer mortar were applied to the concrete in a field test section, and they were subjected to fracture tests. These tests have shown that fracture mechanics is a powerful tool not only in judging the quality of the jointed cement concrete pavement but also in providing a criterion for crack propagation and delamination. Based on fracture mechanics, a method is proposed to determine the joint depth, sawcut timing, and spacing of the jointed cement concrete pavement. This method has successfully been applied to a test section in Seohaean expressway. This study also summarizes the research results obtained from a field test for jointed plain concrete pavement, which was also carried out on the Seohaean expressway.

INTUMESCENT INORGANIC AND ORGANIC COATINGS

  • Kodolov, V.I.;Mikhalkina, T.M.;Shuklin, S.G.;Bystrov, S.G.;Larionov, K.I.
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 1997.11a
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    • pp.130-137
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    • 1997
  • Intumescent inorganic and organic coatings which dintr one from the other by the type of gas formers and the mechanisms of foam formation have been obtained and investigated. Inorganic intumescent coatings are the compositions based on water glass and mineral additives with different dispersity. Mineral additives contain adsorbed and absorbed water and carbonates which are destructed with the carbon dioxide and water evolution during the flame action on coating. The decreasing of mineral additives particle sizes under the mechanical milling with the fraction precipitation promotes the foam coke formation with less defects. Here the main structure of comparing compositions does not change. In organic coatings based on epoxy-polymers the polyammonium phosphate additive is used. It is the cabonization catalyst and the foam agent. The polyammonium phosphate of various dispersity employed is uniformly distributed on the polymeric matrix. The decreasing of the particle sizes leads to the increasing of the fire resistant properties of the intumescent coa-ting. The fire resistant analysis of the coating during more than an hour: the coating back side the temperature on plastic or wooden materials does not exceed 423K, and on metal-573K.

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Crack Tip Creep Deformation Behavior in Transversely Isotropic Materials (횡방향으로 등방성인 재료에서 균열선단 크리프 변형 거동)

  • Ma, Young-Wha;Yoon, Kee-Bong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.12
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    • pp.1455-1463
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    • 2009
  • Theoretical mechanics analysis and finite element simulation were performed to investigate creep deformation behavior at the crack tip of transversely isotropic materials under small scale creep (SCC) conditions. Mechanical behavior of material was assumed as an elastic-$2^{nd}$ creep, which elastic modulus ( E ), Poisson's ratio ( ${\nu}$ ) and creep stress exponent ( n ) were isotropic and creep coefficient was only transversely isotropic. Based on the mechanics analysis for material behavior, a constitutive equation for transversely isotropic creep behavior was formulated and an equivalent creep coefficient was proposed under plain strain conditions. Creep deformation behavior at the crack tip was investigated through the finite element analysis. The results of the finite element analysis showed that creep deformation in transversely isotropic materials is dominant at the rear of the crack-tip. This result was more obvious when a load was applied to principal axis of anisotropy. Based on the results of the mechanics analysis and the finite element simulation, a corrected estimation scheme of the creep zone size was proposed in order to evaluate the creep deformation behavior at the crack tip of transversely isotropic creeping materials.

Temperature Calibration of a Specimen-heating Holder for Transmission Electron Microscopy

  • Kim, Tae-Hoon;Bae, Jee-Hwan;Lee, Jae-Wook;Shin, Keesam;Lee, Joon-Hwan;Kim, Mi-Yang;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.45 no.2
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    • pp.95-100
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    • 2015
  • The in-situ heating transmission electron microscopy experiment allows us to observe the time- and temperature-dependent dynamic processes in nanoscale materials by examining the same specimen. The temperature, which is a major experimental parameter, must be measured accurately during in-situ heating experiments. Therefore, calibrating the thermocouple readout of the heating holder prior to the experiment is essential. The calibration can be performed using reference materials whose phase-transformation (melting, oxidation, reduction, etc.) temperatures are well-established. In this study, the calibration experiment was performed with four reference materials, i.e., pure Sn, Al-95 wt%Zn eutectic alloy, NiO/carbon nanotube composite, and pure Al, and the calibration curve and formula were obtained. The thermocouple readout of the holder used in this study provided a reliable temperature value with a relative error of <4%.

Fabrication of Thin Film Dielectric by Hybrid Sol (Hybrid Sol을 이용한 박막 유전체 제작)

  • Kim, Yong-Suk;Yoo, Won-Hee;Chang, Byeung-Gyu;Oh, Yong-Soo
    • Korean Journal of Materials Research
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    • v.17 no.4
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    • pp.185-191
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    • 2007
  • The purpose of this study is to evaluate the thin fihn dielectric made of hybrid sol, which consist of barium titanate powder, polymeric sol and other polymers. This sol will be used dielectric applied to small, thin electric passive components such as MLCC(Multi Layer Ceramic Condenser), resister, inductor. This sol is composed of mixed fine barium titanate powder and polymeric sol including Ba, Ti-precursor, solvent, chelating agent, chemical reaction catalyst, the additive sols to improve fired densification and temperature reliability. First at all, we mixed hybrid sol to be dispersed and be stabilized by ball milling for 24hrs. By spin coating method, we makes thin film dielectric on the convectional green sheet for MLCC. After heat treatments, we analyzes the structure morphology, physical, electrical properties and X5R Temperature properties.

Use of homogenization theory to build a beam element with thermo-mechanical microscale properties

  • Schrefler, B.A.;Lefik, M.
    • Structural Engineering and Mechanics
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    • v.4 no.6
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    • pp.613-630
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    • 1996
  • The homogenization method is used to develop a beam element in space for thermo-mechanical analysis of unidirectional composites. Local stress and temperature field in the microscale are described using the function of homogenization. The global (macroscopic) behaviour of the structure is supposed to be that of a beam. Beam-type kinematical hypotheses (including independent shear rotations) are hence applied and superposed on the microdescription. A macroscopic stiffness matrix for such a beam element is then developed which contains the microscale properties of the single cell of periodicity. The presented model enables us to analyse without too much computational effort complicated composite structures such as e.g. toroidal coils of a fusion reactor. We need only a FE mesh sufficiently fine for a correct description of the local geometry of a single cell and a few of the newly developed elements for the description of the global behaviour. An unsmearing procedure gives the stress and temperature field in the different materials of a single cell.