• Journal of the Korean Ceramic Society
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• v.43 no.1 s.284
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• pp.4-9
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• 2006

To test the fracture toughness of alumina; a Surface-Crack-in-Flexure (SCF) method, a Single-Edge-Precracked-Beam (SEPB) method and a Single-Edge-V-Notched-Beam (SEVNB) method were used at crosshead rates ranging from 0.005 mm/min to 2 mm/ min and relative humidity ranging from $15\%\;to\;80\%$. The results show that the fracture toughness tested by the SCF method increases with either an increasing loading rate or decreasing relative humidity; in contrast, the toughness by the SEPB method and the SEVNB method does not depend on the loading rate or the relative humidity. Theoretical analysis of the way slow crack growth affects the apparent fracture toughness indicates that the three testing methods have different effects with respect to the loading rate and the relative humidity; moreover, these differences are attributable to differences in the size of the cracks or notches.

• Proceedings of the Korea Concrete Institute Conference
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• 2000.10a
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• pp.655-660
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• 2000

This study was performed to verify the properties of concrete used recycled aggregate(0, 30%, 50%). Also, to improve the brittle fracture, energy absorption and apparent ductility of concrete, we added polypropylene fibers(0, 0.1, 0.2, 0.5, 1.0% by volume of concrete). As the experimental results, adding 30% recycled aggregates and 0.5% polypropylene fibers to concrete mixes enhances the properties of both compressive strength and toughness.

• Proceedings of the Korea Concrete Institute Conference
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• 2000.04a
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• pp.78-81
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• 2000

The test specimen proposed in this study, named the bimaterial eccentric compression specimen, is a rectangular prism of two dissimilar materials with a notch at their interface. Normalized energy release rates and phase angles were calibrated with the finite element method. The normalized energy release rate increases with notch ratio but decreases with E2/E2, loading point, and phase angle, Bimaterial specimens consisting of mortar and ploymer as well as mortar and rock were prepared and tested to simulate fracture behavior ar the interface. Test results have confirmed that initial notch has significant effect on the apparent interfacial toughness.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2004.10a
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• pp.223-226
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• 2004

The objectives of this study are to evaluate mechanical properties of glass ceramic for dome port cover material o( the ramjet. Candidate material for dome port cover of the ramjet is selected the machinable glass ceramic(MACOR glass-filled ceramic, Corning Glass Works, code 9658). Static and dynamic fracture toughness tests were performed to evaluate the apparent fracture toughness of notched specimen.

• Applied Microscopy
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• v.26 no.4
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• pp.447-456
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• 1996

Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

• Korean Journal of Metals and Materials
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• v.46 no.8
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• pp.524-537
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• 2008

Zr-based amorphous alloy matrix composites reinforced with metallic continuous fibers were fabricated by liquid pressing process, and their fracture properties were investigated by directly observing microfracture process using an in situ loading stage installed inside a scanning electron microscope chamber. About 60 vol.% of metallic fibers were homogeneously distributed inside the amorphous matrix. Apparent fracture toughness of the stainless-steel- and tungsten-fiber-reinforced composites was lower than that of monolithic amorphous alloy, while that of the Ta-fiber-reinforced composite was higher. According to the microfracture observation, shear bands or cracks were initiated at the amorphous matrix, and the propagation of the initiated shear bands or cracks was effectively blocked by fibers, thereby resulting in stable crack growth which could be confirmed by the fracture resistance curve (R-curve) behavior. This increase in fracture resistance with increasing crack length improved fracture properties of the fiber-reinforced composites, and could be explained by mechanisms of formation of multiple shear bands or multiple cracks at the amorphous matrix and blocking of crack or shear band propagation and multiple necking at metallic fibers.

• Journal of Mechanical Science and Technology
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• v.18 no.3
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• pp.388-394
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• 2004

Composites of Si$_3$N$_4$-SiC containing up to 30 wt% of dispersed SiC particles were fabricated via hot-pressing with an oxynitride glass. To determine the effect of sintering time and SiC content on the mechanical properties and the cutting performance, the composites with fixed 8hr-sintering time and 20 wt% SiC content were fabricated and tested. Fracture toughness of the composites increased with increasing sintering time, while the hardness increased as the SiC content increased up to 20 wt%. The hardness of the composites was relatively independent of the grain size and the sintered density. For machining heat-treated AISI4140, the insert with 20 wt% SiC sintered for 8hr showed the longest tool life while the insert with 20 wt% SiC sintered for 12hr showed the longest tool life for machining gray cast iron. An effort was made to relate the mechanical properties, such as hardness, fracture toughness and wear resistance coefficient with the tool life. However, no apparent relationship was found between them. It may be stated that tool life is affected by not only the mechanical properties but also other properties such as surface roughness, density, grian size and the number of the inherent defects in the inserts.

• Journal of the Korean Ceramic Society
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• v.35 no.3
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• pp.231-238
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• 1998

Cr3C2 -dispersed TiC composites were prepared via HPCS(high pressure-self combustion sintering) pro-cess using mixtures of Ti, Cr and a carbon source for the purpose of increasing the facture toughness and sinterability of TiC. In this study the microstructure and properties of the composites were investigated in terms of relation to the carbon source the particle size of Ti and the amount of Cr. It was found that car-bon black was the most effective carbon source among the various carbon sources tested and the reaction was more effective as the particle size of Ti decreased. Among the sintered composites of Ti-C-Cr system the one with 30wt% Cr showed the best physical properties with 0.5% in apparent porosity 98.8% in re-lative density 18.2 GPa in hardness and 4.46 MPa.m1/2 in fracture toughness. In addition it was observed that the lattice constant of TiC decreased gradually with increasing the amount of Cr.

• Korean Journal of Materials Research
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• v.24 no.9
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• pp.474-480
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• 2014

Process conditions for the impregnation of polycarbosilane preceramic polymer into SiC-based composites were investigated. Two kinds of preceramic polymer (PCP) was impregnated into SiC-fiber fabrics with different solvents of n-hexane and divinylbenzene (DVB). Both microstructural observations and mechanical tests were conducted to evaluate the impregnation. The matrix phases were particulated in the case of hexane solvents. Apparent relative density of the matrix was about 78.8%. The density of matrix was increased to about 96.1-98.8% when the DVB was used; however, brittle fracture was observed during a bending test. The modulus of toughness was less than $0.74J/m^3$. The fabric impregnated with a mixed PCP-dissolved solution showed intermediate characteristics with relative high density of filling (apparent density of ~96.1%) as well as proper bending behavior. The modulus of toughness was increased to about $5.31J/m^3$. The composites developed by changing the precursor and solvent suggested the possibility of fabricating SiCf/SiC composites without a fiber to matrix interphase coating.

• Journal of Welding and Joining
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• v.8 no.4
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• pp.46-57
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• 1990

TMCP steel manufactured by controlled rolling followed by accelerated cooling process is known to have extra-ordinary mechanical properties such as tensile strength and toughness. However, there is much uncertainty about the fatigue fracture characteristics, especially, in the welded state of this steel. In case of this steel, the softening zone by welding is generated in heat affected zone in contrast with the case of conventional normalized high strength steel. This softening zone is considered to play significant roles in low cycle fatigue fracture of the welded part of this steel. In this paper, the low cycle fatigue behaviors of TMCP steel were inspected in as-received and welded state using the smooth specimen. The fatigue life-time was seperately investigated on the basis of failure of the specimen and crack initiation which is detected by differential strain method. Moreover, the low cycle fatigue characteristics of TMCP steel were quantitatively compared with those of the conventional normalized steel of same strength level.