• Title/Summary/Keyword: Annealing Test

Search Result 279, Processing Time 0.033 seconds

Effect of Aging Heat Treatment on the Mechanical Properties in Inconel 718 Alloy (Inconel 718 합금의 시효열처리가 기계적 성질에 미치는 영향)

  • Kang, Hee Jae;Kim, Jung Min;Jee, Sung Hwan;Sung, Jie Hyun;Kim, Young Hee;Sung, Jang Hyun;Jeon, Eon Chan
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.30 no.3
    • /
    • pp.271-277
    • /
    • 2013
  • Inconel 718 super alloy was aging heat treated at the temperature range from $675^{\circ}C$ to $785^{\circ}C$ for 5~40 hours after solution annealing at $1025^{\circ}C$ for 1 hour. The aging treated specimens were investigated microstructure, mechanical properties and thermal expansion/contraction. Precipitates appeared for a long time aging treatment were niobium carbide and also ${\gamma}^{\prime}$ phase. For the aging treatment time of 10 hours, the changes in strength and hardness with increasing aging treatment temperature showed the maximum value at the temperature of $725^{\circ}C$. This maximum value is to be related with the precipitation of ${\gamma}^{\prime}$ and ${\gamma}^{{\prime}{\prime}}$ phases. The decrease in strength, elongation and hardness during long time aging at $725^{\circ}C$ were thought to be induced from the coarsening of the grain size and the transformation of ${\gamma}^{{\prime}{\prime}}$ phase to ${\gamma}^{\prime}$ phase. For the specimens treated for 10 hours, impact energy showed constant value of ~105 J with increasing the aging temperature, however this value continuously decreased with elapsing time at the aging temperature of $725^{\circ}C$. It was found that the decrease in impact value was induced from the coarsening of grain size and the carbide coarsening. The coefficient of thermal expansion of aging treated Inconel 718 alloy increased with raising test temperature, and the coefficient was appeared $11.57{\sim}12.09{\mu}m/m{\cdot}^{\circ}C$ and $14.28{\sim}14.39{\mu}m/m{\cdot}^{\circ}C$, respectively, after heating to $150^{\circ}C$ and $450^{\circ}C$.

Study on Corrosion Characteristic of New Nb-containing Zr based Alloys for Fuel cladding (Nb 첨가 핵연료피복관용 Zr 신합금의 부식특성 연구)

  • Choe, Byeong-Gwon;Ha, Seung-Won;Jeong, Yong-Hwan
    • Korean Journal of Materials Research
    • /
    • v.11 no.5
    • /
    • pp.405-412
    • /
    • 2001
  • Corrosion tests were carried out in $360^{\circ}C$ water and $360^{\circ}C$ 70ppm LiOH solution to investigate the corrosion behavior of new zirconium alloys (Zr-0.4Nb-0.8Sn-xFeCrMn, Zr-0.2Nb-1.1Sn-xFeCrMn, Zr-1.0Nb-xFeCu). Microstructures of tested alloys were analyzed by optical microscope and TEM. The cross-sectional surface and crystalline structure of the oxide layer were analyzed by SEM and XRD. From the results of corrosion test, all the alloys showed higher corrosion rates in $360^{\circ}C$ 70ppm LiOH aqueous solution thats in $360^{\circ}C$ water. Especially, high Nb-containing alloy exhibited the acceleration of corrosion rate in LiOH solution. The low Nb- and Sn-added alloys showed better corrosion resistance than the Sn- free high Nb alloy. from the effect of final annealing on the corrosion, it was observed that the partially recrystallized alloys showed better corrosion resistance than fully recrystallized alloys. This would be related to the size and distribution of the second phase particles.

  • PDF

Experimental Investigation of the Residual Stress on Fatigue Crack Growth of Welded Steel Members (용접(鎔接) 강부재(鋼部材)의 피로균열성장(疲勞龜裂成長)에 대한 잔류응력특성(殘留應力特性)에 관한 연구(硏究))

  • Chang, Dong Il;Kim, Doo Hwan
    • KSCE Journal of Civil and Environmental Engineering Research
    • /
    • v.7 no.2
    • /
    • pp.99-106
    • /
    • 1987
  • Annealing were performed to investigate the behaviors of the residual stress remaining on the member of a steel structure. According to the fatigue test, the welding part has higher fatigue crack growth rate than the base metal part because the hardening of welding part reduce fracture toughness. However, the heat treatment decrease the hardness and increase the resistance to failure. Thus, the fatigue crack growth rate is improved and it reaches the minimum at $650^{\circ}C$. Elber' s equation includes the effect of the crack-close so that this equation provides a lower the fatigue crack growth rate than Paris-Erdogan' s equation, the Elber's curves show no significant difference to indentify the effect of the residual stress. The Pop loading along the crack length increases as the hardness goes higher. The heat treatment not only decrease the hardness, and the fatigue crack growth rate, but increase the absorption energy and fracture toughness on the member of a steel structure. As the result, the heat treatment produces the resistant ability to cracking which can reduce the degree of danger to failure.

  • PDF

A Study of Thermo-Mechanical Analysis for the Design of High Pressure Piping System for Natural Gas Fuel Vessel (천연가스 연료선박의 고압 이중 배관 설계를 위한 열-구조 해석에 관한 연구)

  • Park, Seong-Bo;Sim, Myung-Ji;Kim, Myung-Soo;Kim, Jeong-Hyeon;Lee, Jae-Myung
    • Journal of Advanced Marine Engineering and Technology
    • /
    • v.39 no.4
    • /
    • pp.425-431
    • /
    • 2015
  • LNG (liquefied natural gas) is considered the best alternative eco-fuel, and many studies on the LNG fuel system have been performed to use LNG as the fuel for ships. For the LNG fuel supply system, natural gas transfers from the vaporizer to the engine in the gaseous state with a temperature of $50^{\circ}C$ and a pressure of 35MPa. Therefore, a structural safety evaluation of the double-walled pipelines considering thermal load is essential. In this article, an uniaxial tensile test for super duplex stainless steel, material for double-walled pipe, according to the annealing time was carried out to analyze the thermal effect. In addition, thermo-structural analysis of the high temperature-high pressure double-walled pipe with fixed supports that are now used widely was carried out to evaluate the structural safety. To minimize stress concentration of the connection point between the support and inner pipe, the shapes of the new type support that can slip through inner pipe were proposed, and the supports which has best structural performance was selected using the results from the thermo-structural analyses of new supports and an analysis of the whole double-walled pipeline was performed to ensure structural safety. These results can be used as a database for the design of double-walled pipelines and sliding support.

A Study on Development of Once-Over Harvest Pepper Harvester(I) - A Fundamental Factor Test for Pepper Detachment - (일시수확형 고추수확기 개발에 관한 연구 (I) - 고추 탈과 기초요인시험 -)

  • Kim, Y. K.;Hong, J. T.;Choi, Y.;Jun, H. J.;Park, H. J.;Cho, Y. M.
    • Proceedings of the Korean Society for Agricultural Machinery Conference
    • /
    • 2002.02a
    • /
    • pp.54-59
    • /
    • 2002
  • 1. 일시수확형 고추의 기계수확 요인을 구명하기 위하여 4종류의 탈과장치를 제작하여 공시고추로 탈과시험을 실시한 결과 탈과장치는 방사대칭식(브러쉬형), 고추이송(공급)속도는 0.1m/s, 탈과장치 간격은 3cm, 탈과장치 회전수는 180rpm에서 정상탈과율 77.3%, 손상률 7.6% 미탈과율 3.0%로 가장 양호한 성적이 나타났다. 2. 방사대칭식(브러쉬형) 탈과장치를 이용하여 무지용 상향착과형 고추, 지주용 하향착과형 고추, 지주용 상향착과형 고추를 공시하여 고추별 탈과시험을 실시한 결과, 고추이송(공급)속도 0.1m/s, 원통사이간격 3cm, 탈과장치 회전수 180rpm에서 가장 양호한 성적이 나왔으며, 지주용 하향착과형 고추가 정상탈과률 82.7%, 손상률 7.4%, 미탈과율 2.7%로 무지주용 상향착과형 고추(52.3%, 14.3%, 12.5%)와 지주용 상향착과형 고추(77.3%, 7.6%. 3.0%)에 비해 기계수확에 적합한 것으로 나타났다. 3. 이상의 고추 기계수확 요인시험의 결과, 탈과장치는 방사대칭식(브러쉬형) 고추종류로는 하향착과형 고추가 기계수확에 바람직한 것으로 나타났으며, 수확 후 회수가 가능한 줄기부착고추를 포함한다면 고추기계수확률은 80% 이상, 꼭지가 떨어진 것이 대부분인 손상고추도 수확 후 즉시 기계건조하여 가공용으로 사용한다고 가정한다면 기계 수확률은 90% 이상 가능하지만, 이것의 수용 여부는 좀 더 폭넓은 의견수렴 및 조사가 필요하다고 사료된다. 4. 고추수확 기계화를 위해서는 실내요인 시험 결과를 토대로 포장에서 수확메커니즘 구명과 더불어 고추 과실이 크고 무지주용 하향착과형 일시수확형 고추 품종의 개발이 병행되어야 한다고 판단된다. 5) 마늘 선별작업 -마늘선별기는 작업성능이 높고 5등급으로 균일 선별되었으며 손상도 없었으나, 기계가 크고 무거워 이동이 곤란하고 가격이 비싸므로 선별등급을 3∼4단계로 줄이고 소형 농가보급형으로 개량제작이 요구됨. 나. 마늘재배 일관기계화에 의한 노동투하시간과 비용 -종자준비부터 통마늘선별까지의 일관기계화로 투입된 주요작업의 노력은 75∼76%가 절감되고, 재배규모 3ha기준시 비용은 44-53%절감되었음. the annealing texture. Observations by TEM and EBSD revealed the formation of very fine grains of ∼1.0$\mu\textrm{m}$ after CCSS.he dislocations form local defect arrangements at the grooves permitting the substantial reduction in defect density over the remainder of the interfacial area.한 최대의 감자 재배지역을 형성하였다. 제주도는 산지지형과 따뜻한 기온으로 2기작이 가능하고, 감자가공 공장설립과 교통발달에 따른 육지 시장과의 접근이 용이해졌기 때문에 남한에서 2번째로 큰 감자재배지역이 되었다.(요약 및 결론에서 발췌)그람양성균에서 효과적이었으며, 농도별 항균력시험 결과 농도가 증가할수록 비례하여 저해율도 증가함을 알 수 있었다. 첨가농도를 달리하여 미생물의 생육도를 측정한 결과, fraction II磎꼭\ulcorner경우 그람양성균에 대해 500 ppm 이상에서 뚜렷한 증식억제효과를 나타내었다.서 뚜렷한 증식억제효과를 나타내었다.

  • PDF

Quality Characteristics of Cookies with Resistant Starches (저항전분을 첨가하여 제조한 쿠키의 품질 특성)

  • Kim, Jae-Suk;Shin, Mal-Shick
    • Korean journal of food and cookery science
    • /
    • v.22 no.5 s.95
    • /
    • pp.659-665
    • /
    • 2006
  • The effects of resistant starches on the quality characteristics of cookies were investigated by the physicochemical, instrumental and sensory properties of RS-added flours and cookies. Retrograded RS3 by autoclaving-cooling cycle and cross-linked RS4 after annealing treatment were used. The protein content of RS-added flour decreased, but the ash content of RS4-added flour increased slightly with increasing RS content. The RS levels of wheat flour, RS3- and RS4-added flours were 7.0%, 9.6-13.4% and 11.5-17.9%, respectively. The swelling powers of RS-added flours at 80$^{\circ}C$ decreased, but the solubility of RS3-added flour increased by 2-3 fold compared to that of control flour. Initial pasting temperature increased, but peak, holding, and final viscosities decreased with increasing RS content. The retrogradation degree of RS-added flours was lowered, because of the decreased consistency and breakdown viscosity. The yellowness of RS3-added flour increased with increasing RS3 content which induced browning reaction during baking. On the sensory test, RS-added cookies were significantly different in shape, color and overall quality (p<0.05), and their texture also affected. Overall quality was higher in peanut cookies than in AACC standard cookies and RS addition (up to 30%, w/w), regardless of the RS type, improved the cookie quality.

A Study on Microstructure and Mechanical Properties of TiC/Steel Composites Fabricated by Powder Metallurgy Process (분말야금공정으로 제조된 TiC/steel 금속복합재료의 미세조직 및 기계적 물성 연구)

  • Lee, Jihye;Cho, Seungchan;Kwon, Hansang;Lee, Sang-Kwan;Lee, Sang-Bok;Kim, Daeha;Kim, Junghwan
    • Composites Research
    • /
    • v.34 no.5
    • /
    • pp.311-316
    • /
    • 2021
  • In this study, TiC/steel metal matrix composites were fabricated by powder metallurgy process using Fealloy powders with 3 wt.% Cr and 10 wt.% Cr, respectively, as matrix material. Subsequently, the composite samples were heat treated by the annealing and quenching-tempering(Q-T), respectively, to understand the effect of heat treatment on the mechanical properties of the composites. The correlation between microstructure and structural strength depending on the chromium content and the heat treatment conditions was studied through tensile, compressive, and transverse rupture test and microstructural analysis. In the case of TiC/steel composite containing 10 wt.% Cr, the tensile strength and transverse rupture strength at room temperature were significantly lowered by the influence of coarse chromium carbide formed at the TiC/steel interface. On the other hand, both TiC/steel composites containing 3 wt.% Cr and 10 wt.% Cr showed much higher compressive strength of about 4 GP after quenching-tempering compared to the annealed specimens regardless of the presence of the chromium carbide.

Estimation of Anti-proliferative Activity of Saccharin against Various Cancer Cell Lines and MSCs (다양한 암세포 주와 MSCs에 대한 Saccharin의 항증식성 평가)

  • Choi, Jeong Su;Park, Sang Yong;Yang, Man Gil;Lee, Dong Beom;Lee, Tae Bok;Heo, Ji Hye;Lee, Min Woo;Kim, Suhng Wook
    • Korean Journal of Clinical Laboratory Science
    • /
    • v.48 no.3
    • /
    • pp.169-175
    • /
    • 2016
  • Saccharin (o-benzoic sulfimide) is the first artificial and non-caloric sweetener that was first synthesized in 1879. In this study, we examined the biological activity of saccharin against various human cancer cell lines and human bone marrow-derived mesenchymal stem cells. A viability assay based on the conversion of 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (MTT) was performed to test for the cytotoxicity of saccharin about the four human cancer cell lines (H460, H157, A549 and SKOV3), one murine cancer cellline (Raw264.7), and MSCs. In order to find the differentially expressed gene in saccharin-treated MSCs against untreated MSCs, we performed annealing control primer (ACP)-based differential display reverse transcriptionp-olymerase chain reaction (DDRT-PCR). All tested cells were treated with saccharin at various concentrations (0.0, 4.8, 7.2, 9.6, 12.0, 14.4 mg/mL) for 48 hr. The number of metabolically active cancer cells decreased when treated with the saccharin at various concentrations for 48 hr as compared with the untreated cells. The decrease in cell survival was more evident with increasing concentrations of saccharin. Moreover, novel candidate genes, which were differentially expressed in MSCs in response to saccharin, were identified in 16 bands on 2% agarose gel. This revealed 16-7 up-regulated and 9 down-regulated-differentially expressed genes indicated by arrows. One of these candidate genes was a FK506-binding protein gene. The functional roles of FK506 binding proteins, with respect to the activities of stem cell proliferation, were not characterized. Further studies are required to get a better understanding of FK506-binding proteins in its roles in increasing stem cell proliferative activities from using saccharin.

Development of pSJE6c, an Expression Vector for Kimchi Lactic Acid Bacteria, and Heterologous Gene Expression Using the Vector (김치유산균용 발현벡터 pSJE6c 개발과 이를 이용한 외래 유전자 발현)

  • Lee, Kang-Wook;Park, Ji-Yeong;Lee, Ji-Yeon;Lee, Hwang-A;Baek, Chang-Un;Jo, Hyeon-Deok;Kim, Joo-Yeon;Kwon, Gun-Hee;Chun, Ji_Yeon;Kim, Jeong-Hwan
    • Microbiology and Biotechnology Letters
    • /
    • v.37 no.4
    • /
    • pp.389-398
    • /
    • 2009
  • Development of expression vectors is important for the basic and applied researches on kimchi LAB (lactic acid bacteria). An expression vector, pSJE6c was constructed by inserting P6C promoter sequence from Lactococcus lactis into pSJE, a shuttle vector for E. coli and Leuconostoc species. To test the efficiency of pSJE6c, aga ($\alpha$-galactosidase) and lacZ ($\beta$-galactosidase) genes were expressed in Lactobacillus brevis 2.14. Compared to the pSJE, expression levels of both genes were increased, indicating P6C promoter was better than indigenous promoters. Enzyme activities of L. brevis cells harboring pSJE6caga (pSJE6c with aga) or pSJE6Z (pSJE6c with lacZ) were 1.5-2 fold higher than those with pSJEaga (pSJE with aga) or pSJEZ (pSJE with lacZ). More RNA transcripts were detected in cells harboring pSJE6c based recombinant plasmid. The results indicated that heterologous gene expressions in kimchi LAB could be improved significantly by use of efficient expression vectors.