• Mass Spectrometry Letters
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• v.9 no.3
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• pp.81-85
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• 2018

In this study, the chemical composition of bacterial melanin isolated from the Streptomyces glaucescens strain was elucidated by ultra-high-resolution Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometry. Ultra-high-resolution mass profiles of the microbial melanin product were acquired using a 15 Tesla FT-ICR mass spectrometer in positive and negative ion modes via electrospray ionization to obtain more complete descriptions of the molecular compositions of melanin-derived organic constituents. A mass resolving power of 500,000 (at m/z 400) was achieved for all spectra while collecting 400 scans per sample with a 4 M transient. The results of this analysis revealed that the melanin pigment isolated from S. glaucescens predominantly exhibits CHON and CHO species, which belong to the proteins class of compounds, with the mean C/O and C/N ratios of 4.3 and 13.1, thus suggesting that the melanin could be eumelanin. This analytical approach could be utilized to investigate the molecular compositions of a variety of natural or synthetic melanins. The compositional features of melanins are important for understanding their formation mechanisms and physico-chemical properties.

• Journal of Korean Society for Atmospheric Environment
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• v.17 no.E1
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• pp.17-24
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• 2001

For the purpose of collecting fog droplets as a function of size a new sampling method was developed in this study. Formation of 100$\pm$10㎛ thickness of polymeric water absorbent film (PWAF) on a nuclepore filter could be successfully realized. Also applicability of particle induced X-ray emission (PIXE) method to the chemical analysis of size-segregated fog droplets collected on PWAF was examined experimentally with synthetic fog droplets generated from a nebulizer. Absorption capacity of S-PAAS polymeric water absorbent shows marked decreases in the range less than 1 wt% and slight decrease between 1 and 3.5 wt% of every salt concentration. Dependency of absorption capacity on pH shows the maximum at pH 7. No apparent peak which can influence the quantitative analysis of elements dissolved and suspended in fog droplets was found at PIXE spectrum of PWAF blank. PWAF kept the original shape without rupture under the PIXE analytical conditions of beam intensity for 10 to 60 nA and irradiation time of 4∼5 min. It should be said that the proposed new technique in the work is helpful to get more detailed information of fog droplets, to clarify the fog formation processes, and to develop a model of acid deposition process.

• Journal of Industrial Technology
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• v.3
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• pp.69-74
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• 1983

For the determination of a reservoir capacity Rippl's mass-curve method has long been used with the past river flow data assuming the same flow records will be repeated in the future. This study aims to find out a better method for determining the reservoir capacity by employing the analytical theory based on the stochastic process. For the present study the synthetic generation methods of Thomas-Fiering type was used to synthetically generate 50 years of monthly river inflows to three single-purpose reservoirs and three multi-purpose reservoirs. The generated sequences of monthly flows were analyzed based on the range concept. With the optimum operation rule of the reservoirs as the one which maximizes the water-use downstream the waterrelease from the reservoir was determined and with due consideration to the mean inflows and the range of monthly flows the required reservoirs capacity was stochastically determined. It was possible to repersent the so-determined reservoir capacity in terms of the mean monthly inflows and the number of subseries in the determination of ranges. It is suggested that the result obtained in this study would be applied to approximately estimate, in the stage of preliminary design, the required capacity of a reservoir in question with the limited information such as the mean monthly inflow and the period of reservoir operation.

• Korean Journal of Mineralogy and Petrology
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• v.33 no.1
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• pp.65-71
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• 2020

Glass reference materials have been essentially used for precise geochemistry analytical techniques. In order to make up for the drawback of synthetic glass reference materials, which have the high uncertainty caused by the difference in composition of natural rocks, we introduce a glass geostandard using natural glass. The NK-B1G sample, which comes from the Baekdusan obsidian, is a natural glassy rock that contains only few crystals such as microlites or inclusions. We examined the feasibility of the sample as a reference material for microanalysis like EPMA or LA-ICPMS.

• Proceedings of the KIEE Conference
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• 2005.11a
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• pp.96-99
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• 2005

In this study, we build system and techniques of evaluating the interruption performance of the GCB with experimental method. We constructed a simplified synthetic test circuit of which ability is up to 245kV, 50kA BTF test. And We composed a model test circuit breaker with puffer assisted self blasting type GCB. With this circuit breaker, we carried out the experiment of no load and SLF90. During the tests, we measured the several factors such as stroke, pressure, arc temperature, the voltage and current near the current zero and dI/dt, dV/dt. Arc conductivity before 200ns before current zero which is one of the indexes of the thermal recovery of a GCB was measured. With these kinds of measurement, we could estimate the performance of a GCB fundamentally. Futhermore these results were used to adjust the arc modeling with CFD(computational fluid dynamics) and we could increase the plausibility of the analytical method.

• 한국문화재보존과학회:학술대회논문집
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• 2002.02a
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• pp.12-20
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• 2002

The analysis of danchung pigments at the Geunjeongjeon Hall in the Gyeongbokgung Palace were carried out by EXRF and MXRD. The analytical results showed that mineral pigments were employed for the inside of the Geunjeongjeon Hall. The main ingredients of green pigments were chalcanthite and celadonite. Red pigment was cinnnabar. It was also revealed that synthetic pigments were applied for the outside of the Hall. Yellow pigment was chrome yellow. The main ingredients of red pigments were red lead and hematite. Green pigments were emeral green and chrome green. Lazurite was employed for blue pigment and titanium dioxide for white one.

• Korean Journal of Materials Research
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• v.27 no.9
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• pp.459-465
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• 2017

Nano-sized Zinc selenide (ZnSe) powder was successfully synthesized using Zn and Se precursors in a hydrothermal process. Temperature for the synthesis was varied from $95^{\circ}C$ to $180^{\circ}C$ to evaluate its influence on the microstructural properties of the synthetic particles. ZnSe powder thus fabricated was characterized using various analytical tools such as SEM, XRD, TEM and UV-Vis methods. Two types of ZnSe particles, that is, the precipitated particle and the colloidal particles, were identified in the analysis. The precipitated particles were around 100 nm in average size, whereas the average size of the colloidal particles was around 20 nm. The precipitated particles made at $150^{\circ}C$ and $180^{\circ}C$ were found to be a single phase of ZnSe; however, an inhomogeneous phase was obtained at the lower synthesis temperature of $95^{\circ}C$, suggesting that the temperature for the synthesis should be over $100^{\circ}C$. The precipitated particles were inactive in the UV-Vis absorption investigation, whereas the colloidal particles showed that absorptions occurred at 380 nm in the UV-Vis spectrum.

• Journal of Families and Better Life
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• v.21 no.3
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• pp.109-121
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• 2003

The purpose of this study was to investigate the difficulty of doing job among housing manager. It might be Provide the basic opinion which could be used for professionalizing of housing manager. The survey had been made 156 housing manager in managerial situation of multi-family housing for sale(so called condominium). The analytical methods adopted in this study were frequency, percentage, 1-test, one-way ANOVA, post-hoc estimation(Scheffe test), correlation by the SPSS 10.1 for Windows program. The major findings of this study were as follows. First, it was revealed that many housing manager thought about Residents' Committee In the negative. Because housing manager considered that Residents' Committee interfered in housing manager's business, on the other hand they set a low value on Residents' Committee disposition and its knowledge about housing management. Second, it was founded that a lot of housing manager felt uneasy about his employment for the reason mentioned. Actually Residents' Committee exercised its influence over hiring as well as dismissing housing manager in any management alternatives. Third, it was necessary that synthetic plan might be prepared for housing manager to educate, to re-educate, to furnish information etc. about related in housing management for the specialization of housing management.

• Archives of Pharmacal Research
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• v.24 no.2
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• pp.100-104
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• 2001

Differential pulse polarographic(DPP) analytical procedure for the rifampicin antibiotic, which can be applied to monitor its synthetic process from the starting antibiotic of rifamycin B or rifamycin SV has been developed based on the electrochemical reduction of an azomethine group. Rifampicin exhibited a cathodic peak due to the azomethine group in the side chain of 3-[(4-methyl-1-piperazinyl)imino]methyl moiety and another cathodic peak due to the carbonyl group in rifamycin SV by DPP. The experimental peak potential shift of an azomethine reduction was -73 mV/pH in the pH range between 3.0 and 7.5, agreeing with involvement of 4 e-and 5 $H^5$ in its reduction. By the cyclic voltammetric(CV) studies, the azomethine and the carbonyl reductions in rifampicin were processed irreversibly on the mercury electrode. The plot of peak currents vs. concentrations of rifampicin ranging $1.0{\times}10^{-7} M~$1.0{\times}10^{-5} M yielded a straight line with a correlation coefficient of 0.9996. The detection limit was $1.0{\times}10^{-8} M with a modulation amplitude of 50 mV DPP has been successfully applied for the determination of rifampicin in the pharmaceutical preparations.

• Publications of The Korean Astronomical Society
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• v.30 no.2
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• pp.113-114
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• 2015

Recent high-resolution, high-sensitivity observations of protostellar jets have shown many to possess an underlying 'wiggle' structure. HH 211 is one such example where recent sub-mm observations revealed a clear reflection-symmetric wiggle. An explanation for this is that the HH211 jet source is moving as part of a protobinary system. Here we test this assumption by simulating HH211 through 3D hydrodynamic simulations using the pluto code with a molecular chemistry and cooling module, and initial conditions based on an analytical model derived from SMA observations. Molecular chemistry allows us to accurately plot synthetic molecular emission maps and position-velocity diagrams for direct comparison to observations, enabling us to test the observational assumptions and put constraints on the physical parameters of HH211. Our preliminary results show that the reflection-symmetric wiggle can be recreated through the assumption of a jet source being part of a binary system.