• Title/Summary/Keyword: Analytical results

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Calibration Methods for the Gas Chromatographic Analysis of ppt-level Hydrogen Sulfide (H2) in Air (환경 대기 중 ppt 수준의 황화수소 분석을 위한 GC 방식의 검량 기법에 대한 연구)

  • 김기현;오상인;최여진;최규훈;주도원
    • Journal of Korean Society for Atmospheric Environment
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    • v.19 no.6
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    • pp.679-687
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    • 2003
  • In this study, we investigated the analytical techniques to quantify the ambient concentration of hydrogen sulfide (H$_2$S) in air at ppt concentration level. For this purpose, an on-line GC analytical system equipped with both pulsed-flame photometric detector (PFPD) and thermal desorption unit (TDU) was investigated by collecting ambient air samples. The results of our study generally indicated that calibration conditions of GC system is highly sensitive to affect the accuracy of the analytical technique. Most importantly. we found that the use of different matrices in the the preparation stage of working standards was sensitive to control the overall performance of this technique. The calibration of our analytical system was tested by the two types of working standard (prepared by mixing either with high purity $N_2$ or with the ambient air). According to this test, the latter represented more efficiently the detecting conditions of actual air samples. The peak occurrence patterns of both air samples and standards (prepared by mixing with ambient air) were altered in a similar manner as the function of the loaded volume; however, it was not the case for the $N_2$-mixed standards. Results of our study suggest that detection of H$_2$S is highly different from other sulfides and that its quantification requires minimiaing interfering effects of non -pure substance (like water vapor) and (either sorptive or destructive) loss effects.

Heat Transfer Analysis of Cylindrical Asphalt Specimen using DEM (DEM을 이용한 아스팔트 혼합물의 열전도 예측)

  • Yun, Taeyoung
    • International Journal of Highway Engineering
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    • v.19 no.4
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    • pp.37-44
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    • 2017
  • PURPOSES : Conductive and convective heat transfer simulations for an asphalt mixture were made by using discrete element method (DEM) and similarity principle. METHODS : In this research, virtual specimens composed of discrete element method particles were generated according to four different predetermined particle size distribution curves. Temperature variations of the four different particles for a given condition were estimated and were compared with measurements and analytical solutions. RESULTS : The virtual specimen with mixed particles and with the smallest particle show very good agreement with laboratory test results and analytical solutions. As particle size decreases, better heat transfer simulation can be performed due to smaller void ratio and more contact points and areas. In addition, by utilizing the similarity principle of thermal properties and corresponding time unit, analytical time can be drastically reduced. CONCLUSIONS : It is concluded that the DEM asphalt mixture specimens with similarity principle could be used to predict the temperature variation for a given condition. It is observed that the void ratio has critical effect on prediction of temperature variation. Comparing the prediction for a 4 mm particle specimen with a mixed particle specimen, it is also concluded that predicting the mixed particle specimen temperature is much more efficient considering the number of particles that are directly associated with computational time in DEM analysis.

Improved Method for Calculating Armature-Reaction Field of Surface-Mounted Permanent Magnet Machines Accounting for Opening Slots

  • Zhou, Yu;Li, Huaishu;Wang, Qingyu;Xue, Zhiqiang;Cao, Qing;Zhou, Shi
    • Journal of Electrical Engineering and Technology
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    • v.10 no.4
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    • pp.1674-1681
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    • 2015
  • This paper presented an improved analytical method for calculating armature-reaction field in the surface-mounted permanent magnet machines accounting for opening slots. The analytical model is divided into two types of subdomains. The current of the armature is centralized in the center of the slots. The field solution of each subdomain is obtained by applying the interface and boundary conditions of the model. Two 30-pole/36-slot prototype machines with different slot-opening width are used for validation. The FE (finite element) results confirm the validity of the analytical results with the proposed model. The investigation shows that the wider the slot-opening width is, the smaller the peak value of radial and circumferential components of flux density, and the analytical armature-reaction field produced by centralized current in the slots is similar with the armature-reaction field produced by distributed current in the slots in the FE.

Buckling of axial compressed cylindrical shells with stepwise variable thickness

  • Fan, H.G.;Chen, Z.P.;Feng, W.Z.;Zhou, F.;Shen, X.L.;Cao, G.W.
    • Structural Engineering and Mechanics
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    • v.54 no.1
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    • pp.87-103
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    • 2015
  • This paper focuses on an analytical research on the critical buckling load of cylindrical shells with stepwise variable wall thickness under axial compression. An arctan function is established to describe the thickness variation along the axial direction of this kind of cylindrical shells accurately. By using the methods of separation of variables, small parameter perturbation and Fourier series expansion, analytical formulas of the critical buckling load of cylindrical shells with arbitrary axisymmetric thickness variation under axial compression are derived. The analysis is based on the thin shell theory. Analytic results show that the critical buckling load of the uniform shell with constant thickness obtained from this paper is identical with the classical solution. Two important cases of thickness variation pattern are also investigated with these analytical formulas and the results coincide well with those obtained from other authors. The cylindrical shells with stepwise variable wall thickness, which are widely used in actual engineering, are studied by this method and the analytical formulas of critical buckling load under axial compression are obtained. Furthermore, an example is presented to illustrate the effects of each strake's length and thickness on the critical buckling load.

Analysis and design of demountable embedded steel column base connections

  • Li, Dongxu;Uy, Brian;Patel, Vipul;Aslani, Farhad
    • Steel and Composite Structures
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    • v.23 no.3
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    • pp.303-315
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    • 2017
  • This paper describes the finite element model for predicting the fundamental performance of embedded steel column base connections under monotonic and cyclic loading. Geometric and material nonlinearities were included in the proposed finite element model. Bauschinger and pinching effects were considered in the simulation of embedded column base connections under cyclic loading. The degradation of steel yield strength and accumulation of plastic damage can be well simulated. The accuracy of the finite element model is examined by comparing the predicted results with independent experimental dataset. It is demonstrated that the finite element model accurately predicts the behaviour and failure models of the embedded steel column base connections. The finite element model is extended to carry out evaluations and parametric studies. The investigated parameters include column embedded length, concrete strength, axial load and base plate thickness. Moreover, analytical models for predicting the initial stiffness and bending moment strength of the embedded column base connection were developed. The comparison between results from analytical models and those from experiments and finite element analysis proved the developed analytical model was accurate and conservative for design purposes.

Seismic vulnerability assessment of confined masonry buildings based on ESDOF

  • Ranjbaran, Fariman;Kiyani, Amir Reza
    • Earthquakes and Structures
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    • v.12 no.5
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    • pp.489-499
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    • 2017
  • The effects of past earthquakes have demonstrated the seismic vulnerability of confined masonry structures (CMSs) to earthquakes. The results of experimental analysis indicate that damage to these structures depends on lateral displacement applied to the walls. Seismic evaluation lacks an analytical approach because of the complexity of the behavior of this type of structure; an empirical approach is often used for this purpose. Seismic assessment and risk analysis of CMSs, especially in area have a large number of such buildings is difficult and could be riddled with error. The present study used analytical and numerical models to develop a simplified nonlinear displacement-based approach for seismic assessment of a CMS. The methodology is based on the concept of ESDOF and displacement demand and is compared with displacement capacity at the characteristic period of vibration according to performance level. Displacement demand was identified using the nonlinear displacement spectrum for a specified limit state. This approach is based on a macro model and nonlinear incremental dynamic analysis of a 3D prototype structure taking into account uncertainty of the mechanical properties and results in a simple, precise method for seismic assessment of a CMS. To validate the approach, a case study was considered in the form of an analytical fragility curve which was then compared with the precise method.

Analytical Modeling for Two-story Two-span Reinforced Concrete Frames with Relaxed Section Details

  • Kim, Taewan;Chu, Yurim;Park, Hong-Gun
    • Architectural research
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    • v.20 no.2
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    • pp.53-64
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    • 2018
  • A nonlinear analytical model has been proposed for two-span two-story reinforced concrete frames with relaxed section details. The analytical model is composed of beam, column, and beam-column joint elements. The goal of this study is to develop a simple and light nonlinear model for two-dimensional reinforced concrete frames since research in earthquake engineering is usually involved in a large number of nonlinear dynamic analyses. Therefore, all the nonlinear behaviors are modeled to be concentrated on flexural plastic hinges at the end of beams and columns, and the center of beam-column joints. The envelope curve and hysteretic rule of the nonlinear model for each element are determined based on experimental results, not theoretical approach. The simple and light proposed model can simulate the experimental results well enough for nonlinear analyses in earthquake engineering. Consequently, the proposed model will make it easy to developing a nonlinear model of the entire frame and help to save time to operate nonlinear analyses.

Semi-analytical vibration analysis of functionally graded size-dependent nanobeams with various boundary conditions

  • Ebrahimi, Farzad;Salari, Erfan
    • Smart Structures and Systems
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    • v.19 no.3
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    • pp.243-257
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    • 2017
  • In this paper, free vibration of functionally graded (FG) size-dependent nanobeams is studied within the framework of nonlocal Timoshenko beam model. It is assumed that material properties of the FG nanobeam, vary continuously through the thickness according to a power-law form. The small scale effect is taken into consideration based on nonlocal elasticity theory of Eringen. The non-classical governing differential equations of motion are derived through Hamilton's principle and they are solved utilizing both Navier-based analytical method and an efficient and semi-analytical technique called differential transformation method (DTM). Various types of boundary conditions such as simply-supported, clamped-clamped, clamped-simply and clamped-free are assumed for edge supports. The good agreement between the presented DTM and analytical results of this article and those available in the literature validated the presented approach. It is demonstrated that the DTM has high precision and computational efficiency in the vibration analysis of FG nanobeams. The obtained results show the significance of the material graduation, nonlocal effect, slenderness ratio and boundary conditions on the vibration characteristics of FG nanobeams.

The study of simplified technique compared with analytical solution method for calculating the energy consumption loads of four houses having various wall construction

  • Han, Kyu-Il
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.47 no.1
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    • pp.46-58
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    • 2011
  • A steady-state analysis and a simple dynamic model as simplified methods are developed, and results of energy consumption loads are compared with results obtained using computer to evaluate the analytical solution. Before obtaining simplified model a mathematical model is formulated for the effect of wall mass on the thermal performance of four different houses having various wall construction. This analytical study was motivated by the experimental work of Burch et al. An analytical solution of one-dimensional, linear, partial differential equation for wall temperature profiles and room air temperatures is obtained using the Laplace transform method. Typical Meteorological Year data are processed to yield hourly average monthly values. This study is conducted using weather data from four different locations in the United States: Albuquerque, New mexico; Miami, Florida; Santa Maria, California; and Washington D.C. for both winter and summer conditions. The steady state analysis that does not include the effect of thermal mass can provide an accurate estimate of energy consumption in most cases except for houses #2 and #4 in mild weather areas. This result shows that there is an effect of mass on the thermal performance of heavily constructed house in mild weather conditions. The simple dynamic model is applicable for high cycling rates and accurate values of inside wall temperature and ambient air temperature.

Shear and tensile behaviors of headed stud connectors in double skin composite shear wall

  • Yan, Jia-Bao;Wang, Zhe;Wang, Tao;Wang, Xiao-Ting
    • Steel and Composite Structures
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    • v.26 no.6
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    • pp.759-769
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    • 2018
  • This paper studies shear and tensile behaviors of headed stud connectors in double skin composite (DSC) structure. Firstly, 11 push-out tests and 11 tensile tests were performed to investigate the ultimate shear and tensile behaviors of headed stud in DSC shear wall, respectively. The main parameters investigated in this test program were height and layout of headed stud connectors. The test results reported the representative failure modes of headed studs in DSC structures subjected to shear and tension. The shear-slip and tension-elongation behaviors of headed studs in DSC structures were also reported. Influences of different parameters on these shear-slip and tension-elongation behaviors of headed studs were discussed and analyzed. Analytical models were also developed to predict the ultimate shear and tensile resistances of headed stud connectors in DSC shear walls. The developed analytical model incorporated the influence of the dense layout of headed studs in DSC shear walls. The validations of analytical predictions against 22 test results confirmed the accuracy of developed analytical models.