• 분석과학
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• 제13권5호
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• pp.666-674
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• 2000

본 연구는 기체크로마토그래피-질량분석법을 이용한 생물시료 중 polybrominated biphenyls(PBBs)의 분석법을 설명하였다. 생물 시료 중 PBB류는 40mL 아세톤과 80mL의 헥산 혼합용매에서 초음파추출기 20분간 교반하여 추출하였다. 추출액 중 존재하는 지질성분은 농축 황산용액으로 분해한 후 PBB류는 Florisil 컬럼으로 정제하였다. PBB류를 정량분석하기 위하여 정제액은 GC/MS-selected ion monitoring 방법에 의해 분석하였다. 본 실험 조건하에서 전반적인 PBB류의 추출율은 77-111%로 나타났다.

• 분석과학
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• 제8권4호
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• pp.575-582
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• 1995

A new analytical procedure using a serial dual electrode detector was developed for the analysis of amino acids and proteins. Bromine was generated at the upstream electrode and detected by the downstream electrode. The presence of amino acids and proteins was shown to lower the downstream current but with no apparent effect on the upstream current. This indirect mode of detection can be applied to the determination of amino acids and proteins which are electrochemically inactive or too large to be accessible to the electrode surface for electron exchange. The method is shown capable to determine various amino acids (cystine, tyrosine, lysine, tryptophan, glycine, methionine and arginine) and proteins (cytochrome c, hemoglobin, HAS, a-Amylase, Conalbumin I, Catalase and Myglobin) with linear working range for amino acids between $10^{-6}$ to $10^{-3}M$ and total proteins between $10^{-7}$ to $10^{-3}M$. The method has been applied for the analysis of amino acids and total protein in food using Flow Injection Analysis with results obtained comparable to those using the traditional analytical procedure. Use of pulse generation technique was shown to produce a more stable flow injection analysis peaks for repetitive determination than the use of conventional constant current method which showed increase of the background current after determination over 200 minutes. The pulse method was found to give stable baseline even after 400 minutes. Thus, the method is shown able to provide a suitable analytical procedure for automatic analysis of amino acids and proteins in food by flow injection analysis.

• Korean Journal of Geomatics
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• 제1권1호
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• pp.1-5
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• 2001

This paper presents an investigation into the operational comparison of SPOT triangulation to build GCP library by analytical plotter and DPW (digital photogrammetric workstation). GCP database derived from current SPOT images can be used to other image sensors of satellite, if any reasons, such as lack of topographic maps or GCPs. But, general formulation of a photogrammetric process for GCP measurement has to take care of the scene interpretation problem. There are two classical methods depending on whether an analytical plotter or DPW is being used. Regardless of the method used, the measurement of GCPs is the weakest point in the automation of photogrammetric orientation procedures. To make an operational comparison, five models of SPOT panchromatic images (level 1A) and negative films (level 1AP) were used. Ten images and film products were used for the five GRS areas. Photogrammetric measurements were carried out in a manual mode on P2 analytical plotter and LH Systems DPW770. We presented an approach for exterior orientation of SPOT images, which was based on the use of approximately eighty national geodetic control points as GCPs which located on the summit of the mountain. Using sixteen well-spaced geodetic control points per model, all segments consistently showed RMS error just below the pixel at the check points in analytical instrument. In the case of DPW, half of the ground controls could not found or distinguished exactly when we displayed the image on the computer monitor. Experiment results showed that the RMS errors with DPW test was fluctuated case by case. And the magnitudes of the errors were reached more than three pixels due to the lack of image interpretation capability. It showed that the geodetic control points is not suitable as the ground control points in DPW for modeling the SPOT image.

• Structural Engineering and Mechanics
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• 제42권2호
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• pp.131-152
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• 2012

In-plane free vibrations of circular beams with stepped cross-sections are investigated by using the exact analytical solution. The axial extension, transverse shear deformation and rotatory inertia effects are taken into account. The stepped arch is divided into a number of arches with constant cross-sections. The exact solution of the governing equations is obtained by the initial value method. Several examples of arches with different step ratios, different locations of the steps, boundary conditions, opening angles and slenderness ratios for the first few modes are presented to illustrate the validity and accuracy of the method. The effects of the geometric parameters on the natural frequencies are investigated in details. Several examples in the literature are solved and the results are given in tables. The agreement of the results is good for all examples considered. The mode transition phenomenon is also observed for the stepped arches. Some examples are solved also numerically by using the commercial finite element program ANSYS.

• 대한산업공학회지
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• 제29권2호
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• pp.150-156
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• 2003

The IEEE 802.11 MAC (Media Access Control) Protocol supports two modes of operation, a random access mode for nonreal-time data applications processed by Distributed Coordinated Function (DCF), and a polling mode for real-time applications served by Point Coordinated Function (PCF). It is known that the standard IEEE 802.11 is insufficient to serve real-time traffic. To provide Quality of Service (QoS) of real-time traffic, we propose the Downlink-first scheduling with Earliest Due Date (EDD) in Contention Free Period (CFP) with suitable admission control. The capacity and deadline violation probability of the proposed system is analyzed and compared to the standard pair system of downlink and uplink. Analytical and simulation results show that the proposed scheme is remarkably efficient in view of the deadline violation probability.

• Structural Engineering and Mechanics
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• 제75권3호
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• pp.377-387
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• 2020

Modern long-span floor system typically possesses low damping and low natural frequency, presenting a potential vibration sensitivity problem induced by human activities. Field test and numerical analysis methods are available to study this kind of problems, but would be inconvenient for design engineers. This paper proposes a simplified method to determine the acceleration amplitudes of long-span floor system subjected to walking or running load, which can be carried out manually. To theoretically analyze the acceleration response, the floor system is simplified as an anisotropic rectangular plate and the mode decomposition method is used. To facilitate the calculation of acceleration amplitude a_P, a coefficient α_wmn or α_Rmn is introduced, with the former depending on the geometry and support condition of floor system and the latter on the contact duration t_R and natural frequency. The proposed simplified method is easy for practical use and gives safe structural designs.

• Journal of Electrical Engineering and Technology
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• 제11권6호
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• pp.1571-1581
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• 2016

A novel method is proposed to construct the voltage stability boundary of power system considering different Reactive Power Control Mode (RPCM) of Doubly-Fed Induction Generator (DFIG) Wind Power Plant (WPP). It can be used for reflecting the static stability status of grid operation with wind power penetration. The analytical derivation work of boundary search method can expound the mechanism and parameters relationship of different WPP RPCMs. In order to improve the load margin and find a practical method to assess the voltage security of power system, the approximate method of constructing voltage stability boundary and the critical points search algorithms under different RPCMs of DFIG WPP are explored, which can provide direct and effective reference data for operators.

• International Journal of Aeronautical and Space Sciences
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• 제17권3호
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• pp.358-365
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• 2016

In this study, one-dimensional analysis under the assumption of an inviscid flow was conducted for the experiment initiated by the French-German Research Institute of Saint-Louis (ISL) in order to investigate the energy effect of aluminum combustion. Previous theoretical analysis based on the assumptions of isentropic compression and a constant specific heat derived by ISL claimed that the experiment was not affected by the heat of aluminum combustion. However, rigorous analysis in present investigation that considered the average properties behind the shock wave compression and temperature-dependent specific heat showed that the S225 experiment was partially affected by the aluminum combustion. The increase in heat due to aluminum combustion was estimated from the rigorous analysis.

• 한국지진공학회논문집
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• 제22권6호
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• pp.345-352
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• 2018

It is inevitable to use the distinct element method in the analysis of structural dynamics for stacked stone pagoda system. However, the experimental verification of analytical results produced by the discrete element method is not sufficient yet, and the theory of distinct element method is not universal in Korea. This study introduces how to model the stacked stone pagoda system using the distinct element method, and draws some considerations in the seismic analysis procedures. First, the rocking mode and sliding mode are locally mixed in the seismic responses. Second, the vertical stiffness and the horizontal stiffness on the friction surface have the greatest influence on the seismic behavior. Third, the complete seismic analysis of stacked stone pagoda system requires a set of the horizontal, vertical, and rotational velocity time histories of the ground. However, earthquake data monitored in Korea are limited to acceleration and velocity signals in some areas.

• Structural Engineering and Mechanics
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• 제67권5호
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• pp.517-525
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• 2018

In this study, we investigate the vibration of single-walled carbon nanotubes embedded in a polymeric matrix using nonlocal elasticity theories with account arbitrary boundary conditions effects. A Winkler type elastic foundation is employed to model the interaction of nanobeam and the surrounding elastic medium. Influence of all parameters such as nonlocal small-scale effects, Winkler modulus parameter, vibration mode and aspect ratio of nanobeam on the vibration frequency are analyzed and discussed. The mechanical properties of carbon nanotubes and polymer matrix are treated and an analytical solution is derived using the governing equations of the nonlocal Euler-Bernoulli beam models. Solutions have been compared with those obtained in the literature and The results obtained show that the non-dimensional natural frequency is significantly affected by the small-scale coefficient, the vibrational mode number and the elastic medium.