• Title/Summary/Keyword: Analytical measurement range

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Measurement of Dispersion Relation of Plasma Wave (플라즈마 파동의 분산관계 측정에 관한 연구)

  • Jeong, Jung-Hyeon;Lee, Jong-Gyu
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.33 no.3
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    • pp.248-258
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    • 1997
  • The analytical solutions of the Fraunhofer Diffraction(FD) theory and the principle for measurement of the dispersion relation of plasma wave is presented. Especially, the method for measurement of low-frequency wave is discussed. The wavenumbers of the density fluctuations are obtained from the curve fitting between the expremental FD profile and theoretical one for each frequency component. In measurement of the wavenumber of the low -frequency region, the information of the wavenumber is easily obtained from the ratio of the intensity at = 0 to the intensity at =0.5. The millimeter wave FD apparatus was designed to measure low-frequency density fluctuations. The determined wavenumbers are in the range of =0.1~ 1.0cm. Thus, the millimeter wave FD method was shown to be useful for the measurement of low-frequency density fluctuations, which are impossible to be measured by using a convention. Thomson scattering. The obtained dispersion relations will be useful information for plasma waves.

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Comparison of Li-heparinized Versus Na-fluorinated Plasma for Routine Blood Glucose Determination Using Hexokinase Procedure (Hexokinase 방법을 이용한 Heparin 혈장과 NaF 혈장 시료의 혈당 분석치 비교)

  • Moon, In-Kyung
    • Korean Journal of Clinical Laboratory Science
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    • v.39 no.1
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    • pp.25-30
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    • 2007
  • In this study, the two sampling methods for blood glucose measurement were evaluated in order to reduce pre-analytical error. For this purpose, glucose levels of Li-heparinized plasma (LHP) and Na-fluorinated plasma (NFP) in blood collected from healthy volunteers were determined by using routine hexokinase procedures. The percentage range of pre-analytical error was quantitated by comparing LHP glucose values with NFP glucose values according to delaying analytical time (0, 60, and 120 min). LHP glucose values were decreased by 6.6% in 60 min., 17.7% in 120 min, whereas NFP glucose values decreased by 1.1% in 60 min, 2.0% in 120 min. Therefore it may be recommended that the NFP sampling method should be used for routine blood glucose determination in diabetes mellitus diagnosis.

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Evaluation of Methodology for the Measurement of VOCs in the Air by Adsorbent Sampling and Thermal Desorption with GC Analysis (흡착포집 및 열탈착/GC 분석에 의한 공기 중 휘발성 유기화합물의 측정방법론 평가)

  • 백성옥;황승만;박상곤;전선주;김병주;허귀석
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.2
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    • pp.121-138
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    • 1999
  • This study was carried out to evaluate the performance of a sampling and analytical methodology for the measurement of selected volatile organic compounds (VOCs) in the ambient air. VOCs were determined by the adsorbent tube sampling and automatic thermal desorption coupled with GC/FID and GC/MSD analysis. Target analytes were aromatic VOCs, including BTEX, 1,3,5-and 1,2,4,-trimethylbenzenes(TMBs), and naphthalene. The methodology was investigatedwith a wide range of performance criteria such as repeatability, linearity, lower detection limits, collection efficiency, thermal conditioning, breakthrough volume and calibration methods using internal and external standards. standards. Stability of samples collected on adsorbent tubes during storage was also investigated. In addition, the sampling and analytical method developed during this study was applied to real samples duplicately collected in various indoor and outdoor environments. Precisions for the duplicate samples and distributed volume samples appeared to be well comparable with the performance criteria recommended by USEPA TO-17. The audit accuracy was estimated by inter-lab comparison of both duplicate samples and standard materials between the two independent labs. The overall precision and accuracy of the method were estimated to be within 30% for major aromatic VOCs such as BTEX. This study demonstrated that the adsorbent sampling and thermal desorption method can be reliably applied for the measurement of BTEX in ppb levels frequently occurred in common indoor and ambient environments.

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Mechanism Design of the Micro Weighing Device by Using Null Balance Method (영위법을 이용한 미소중량 측정 장치의 기구설계)

  • Choi, In-Mook;Woo, Sam-Yong;Kim, Boo-Shik;Kim, Soo-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.27 no.1
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    • pp.183-193
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    • 2003
  • Micro-weighing device by using null balance method is being essential part in fields of high-technology industries such as precision semiconductor industry, precision chemistry, biotechnology and genetics etc. Also, requirements for high resolution and for large measurement range increase more and more. The performance of the micro-weighing device can be determined by the mechanism design and analysis. The analytical design method has been proposed for the performance improvement such as resolution, measurement range and fast response. The 2-stage displacement amplification is designed to overcome the limit of conventional force transmitting lever. The parallel spring is designed for the measurement result independent of the input force position variation. Also, the natural frequency of mechanism is analyzed for the fast response. After each analysis, optimal design has been carried out. To verify the analysis and design result, characteristics experiments had been carried out after construction. Finally, the system had been controlled.

Parity Space and Pattern Recognition Approach for Hardware Redundant System Signal Validation using Artificial Neural Networks (인공신경망을 이용하여 하드웨어 다중 센서 신호 검증을 위한 패리티 공간 및 패턴인식 방법)

  • 윤태섭
    • Journal of Institute of Control, Robotics and Systems
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    • v.4 no.6
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    • pp.765-771
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    • 1998
  • An artificial neural network(NN) technique is developed for hardware redundant sensor validation. Since the measurement space is a continuous space with many operating regions, it is difficult to train a NN to correctly detect failure in an accurate measurement system. A conventional backpropagation NN is modified to include an additional preprocessing layer that extracts classification features from scalar measurements. This feature extraction means transform the measurement space to parity space. The NN is independent of the state variable being measured, the instrument range, and the signal tolerance. This NN resembles the parity space approach to signal validation, except that analytical parity equations are unneeded and the NN pattern recognition capability is utilized for decision making.

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Optical Transmission Characteristics of the Breast Tissue In the Range of Near IR (근접적외선 영역에서 Breast Tissue 의 광투과 특성)

  • Cho, Jin-Ho;Ha, Yeong-Ho;Lee, Kuhn-Il
    • Journal of Biomedical Engineering Research
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    • v.7 no.2
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    • pp.159-168
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    • 1986
  • As a fundamental study of Near IR tomography system, transmission parameters of the mongolian breast tissue at 904 nm wavelengh were measured. A analytical model to determin the light intensity in the breast was developed and the measurement, and gheoretical calculations were obtained.

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Measurement of Laminar Flame Speeds of Dimethyl Ether-Air Mixtures at High Pressure (고압에서 DME-Air 혼합기의 화염속도 측정)

  • Lee, Su Gak;Lee, Ki Yong
    • 한국연소학회:학술대회논문집
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    • 2013.06a
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    • pp.103-105
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    • 2013
  • Spherically expanding flames are used to measure flame speeds, which are derived the corresponding laminar flame speeds at zero stretch. Dimethyl Ether-Air mixtures at high pressure are studied over an extensive range of equivalence ratios. The classical shadowgraph technique is used to detect the reaction zone. In analytical methodology the optimization process using least mean squares is performed to extract the laminar flame speeds. Laminar flame speeds are compared with results reported in the literature.

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A Study on the Dose Analysis of Pottery Shards by Thermoluminescence Dating Method (TL 연대측정법을 이용한 토기 시편의 선량 분석)

  • Shin, Hyun-Sang
    • Analytical Science and Technology
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    • v.12 no.6
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    • pp.558-564
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    • 1999
  • A method for measuring archaeological dose of Packjae pottery shards using thermoluminescence dosimetry(TLD) has been studied. TL measurement has been achieved using quartz crystals in the size range of 90 to $125{\mu}m$ diameter extracted from the pottery shards. The stable temperature region of the TL glow curve which is devoid of anomalous fading components was identified by the plateau test and found to exist from 265 to $300^{\circ}C$. The archaeological dose of the pottery shards was estimated to be 7.43 Gy using the dose calibration curves obtained from sequential irradiation of $^{137}Cs$ gamma source to the samples and TL measurement of natural samples.

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Potentiometric Determination of L-Malate Using Ion-Selective Electrode in Flow Injection Analysis Syste

  • Kwun, In-Sook;Lee, Hye-Sung;Kim, Meera
    • Preventive Nutrition and Food Science
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    • v.4 no.1
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    • pp.79-83
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    • 1999
  • A potentiometric biosensor employing a CO3-2 ion-selective electrode(ISE) and malic enzyme immobilization in al flow injection analysis (FIA) system was constructed. Analytical parameters were optimized for L-malate determination . The CO3-2 -ISE-FIA system was composed of a pump, an injector, a malic enzyme (EC1.1.1.40) reactor, a CO3-2 ion-selective electrode, a pH/mV meter and a recorder. Cofactor NADP was also injected with substrate for theenzyme reaction into the system. Optimized analytical parameters for L-malate determination in the CO3-2 ISE-FIA system were as follows ; flow rate, 14.5ml/hr ; sample injection volume, 100ul; enzyme loading in the reactor, 20 units ; length of the enzyme reactor , 7 cm ; tubing length form the enzyme reactor to the detector as a geometric factor in FIA, 15 cm . The response time for measuring the entire L-malate concentration range (10-2 ~10-5 mol/L ; 4 injections )was <15minutes . In this CO3-2 -ISE-FIA system, the potential differences due to th eformation of CO3-2 by the reaction of malic enzyme on L-malate were correlated to L-malate concentration in the range of 10-2 ~10-5mol/L ; the detection limit was 10-5 mol/L. This potentionmetric CO3-2 ISE--FIA system was found to be useful for L-malate measurement.

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Liver tissue sensor for the determination of dopamine (간조직 센서를 이용한 dopamine의 정량)

  • Hur, Moon-Hye;Kim, Ki-Myo;Kim, Young-Hak;Paek, Kwang-Jin;Choi, Hyun-Young;Ahn, Moon-Kyu
    • Analytical Science and Technology
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    • v.8 no.3
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    • pp.365-370
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    • 1995
  • A tissue biosensor for the measurement of dopamine has been constructed by immobilizing the slice of Sprague-Dawley rat liver on $NH_3$-sensing electrode. To overcome the defect of tissue sensors, the maximal velocity of response curve was measured and applied to the Lineweaver-Burk equation instead of the Nernst equation. And then compared the results with those obtained from Nernst equation. When we obtained calibration curves from Nernst equation, there were variances on the slope and the linear range. But from Lineweaver-Burk equation, the scale of variance was small. Response time was reduced from 7~12 minutes to 2~3 minutes.

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