• 제목/요약/키워드: Analytical Tool

검색결과 657건 처리시간 0.024초

진동 원편광 이색성 분광기를 사용한 키랄 에폭사이드의 광학순도 분석 (Determination of Enantiopurity of Chiral Epoxides by Vibrational Circular Dichroism Spectroscopy)

  • 이주현;이충영;김건중
    • 공업화학
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    • 제23권6호
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    • pp.577-582
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    • 2012
  • 진동 원편광 이색성(VCD; Vibrational Circular Dichroism) 분석기기를 사용한 키랄 유도체의 광학순도 분석을 수행하였다. 이 분석법을 통하여 광학이성체의 절대배위와 2% 이내의 오차 범위 내에서 %EE 값을 용이하게 측정할 수 있었다. 또한 VCD분석을 연속순환방식으로 시간 변화와 함께 수행하여 키랄화합물의 %EE 값을 측정하였다. ECH와 글리시돌 두 키랄 성분이 섞인 2성분 계에서 특별한 분리조작 없이 각 성분에 대한 농도 및 %EE 변화를 동시에 모니터링하는 것이 가능하였다. 본 연구에서 응용한 VCD 분석법은 반응 중의 반응 속도 등을 연속적으로 측정하는데 유용한 기법이며, 서로 다른 키랄 화합물이 혼합되어 있는 경우에 각각의 광학순도를 시간 변화와 함께 비파괴법으로 측정하기에 편리한 방법임을 확인하였다.

아동의 독서실태조사 (An Analytical Study on Reading Behavior of School Children)

  • 김병주
    • 한국문헌정보학회지
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    • 제8권
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    • pp.157-182
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    • 1981
  • The purpose of present study is to investigate children's attitude toward reading, reading method, reading environment, reading volume, and then to compare the results obtained by sex, area and grade. The tool used in this survey was a questionaire designed specially by the investigator. The questionaire was distributed to 1339 children selected at the descretion of the investigator with due consideration of sex, area(large city, medium city and rural community) and grade (from 2nd grade of primary school to 2nd year of middle school). The results of this study are summerized as follows : 1) Regional difference was observed in respect of the followiug : Awareness on reading, motivation for reading, reading method, activity after reading, number of books collected, reading guidance, how to obtain books to read, monthly reading volume, and reading tendency. 2) Also difference by grade was observed in respcet of the following ; Activity after reading, reading guidance, monthly reading volume and reading tendency. The following conclusions have been made based on the results of the survey: 1) The children's attitude toward reading and reading method may be considered favorable while reading environment is not satisfactory yet. Especially, reading environment of school children in medium cities and rural communities is worse than that of large cities. 2) No difference by sex was observed in respect of attitudes toward reading, reading method, reading environment and reading volume while difference by sex was observed in respect of reading tendency. The followings are recommended based on the results of survey: 1) To establish and carry out a comprehensive program for the improvement of reading environment of the school children in medium cities and rural communities. 2) To improve and substantiate school library facilities and design a proper guidance program to have children utilize school library to the maximum extent. 3) To contemplate on the consolidated measures for reading behavior survey.

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복잡계 패러다임의 특성과 전망 (Nature and Prospect of Complexity Paradigm)

  • 김문조
    • 과학기술학연구
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    • 제3권2호
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    • pp.1-27
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    • 2003
  • 이 논문은 최근 자연과학 분야에서는 물론이요 사회과학과 더불어 인문예술 영역에 이르는 방대한 학문 영역에서 영향력을 행사하고 있는 복잡계 패러다임의 특성과 전망을 고찰하고자 한 것이다. 흔히 '전체론적 세계관'이라든가 '심층생태학적 관점' 등으로 대변되는 복잡성 패러다임은 개방체계적 사고의 연장선상에 위치한 것으로서, 일차적으로는 개방성, 성장성, 가형성, 否(부)의 엔트로피, 적극적 환류, 자기규제성, 자기목적성, 등종착성과 같은 개방체계적 속성을 함유한다. 그러나 지난 20여 년간 학제적 경계를 초월해 활발히 진전된 복잡계론은 종전의 개방체계론적 논의 수준을 넘어서는 새로운 착상이나 증거를 지속적으로 축적해 온 바, 여기서는 (1) 복잡계 이론이 형성되고 발전되어온 전개과정을 간략히 개관하고, (2) 비평형성, 비선형성, 소산구조 자기조직성, 프랙탈 기하학, 자동생산성 및 공진화와 같은 복잡계의 주요 특성들을 논의하며, (3) 니클라스 루만의 체계이론을 사례로 복잡계 패러다임의 사회과학적 적용을 검토한 후, (4) 복잡계 패러다임의 함의와 전망을 진단해 보고자 한다.

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A Low Cost IBM PC/AT Based Image Processing System for Satellite Image Analysis: A New Analytical Tool for the Resource Managers

  • Yang, Young-Kyu;Cho, Seong-Ik;Lee, Hyun-Woo;Miller, Lee-D.
    • 대한원격탐사학회지
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    • 제4권1호
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    • pp.31-40
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    • 1988
  • Low-cost microcomputer systems can be assembled which possess computing power, color display, memory, and storage capacity approximately equal to graphic workstactions. A low-cost, flexible, and user-friendly IBM/PC/XT/AT based image processing system has been developed and named as KMIPS(KAIST (Korea Advanced Institute of Science & Technology) Map and Image Processing Station). It can be easily utilized by the resource managers who are not computer specialists. This system can: * directly access Landsat MSS and TM, SPOT, NOAA AVHRR, MOS-1 satellite imagery and other imagery from different sources via magnetic tape drive connected with IBM/PC; * extract image up to 1024 line by 1024 column and display it up to 480 line by 672 column with 512 colors simultaneously available; * digitize photographs using a frame grabber subsystem(512 by 512 picture elements); * perform a variety of image analyses, GIS and terrain analyses, and display functions; and * generate map and hard copies to the various scales. All raster data input to the microcomputer system is geographically referenced to the topographic map series in any rater cell size selected by the user. This map oriented, georeferenced approach of this system enables user to create a very accurately registered(.+-.1 picture element), multivariable, multitemporal data sets which can be subsequently subsequently subjected to various analyses and display functions.

카드뮴 분석용 홍합(Mytilus coruscus) 표준물질의 균질성 및 안정성 시험평가 (Evaluation of Homogeneity and Stability of Korean Mussel (Mytilus coruscus) Standards for Cadmium Analysis)

  • 이하은;이장호;정다위;이수용;박기완;심규영
    • 한국환경과학회지
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    • 제28권11호
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    • pp.1041-1045
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    • 2019
  • In this study, the KS A ISO Guide 35 was applied to develop analytical standards for heavy metal cadmium using the Korean mussel (Mytilus coruscus) and to evaluate the homogeneity and stability of the sample. Some of the crucial characteristics that reference materials must consist include homogeneity and stability of both intra- and inter-bottles. We tested homogeneity using ANOVA analysis and short-term stability using regression analysis. The variations of cadmium concentrations did not significantly differ between intra- and inter-bottles (F=0.41, p=0.90). For short-term stability verification, cadmium analysis results were not statistically significant as a result of the regression analysis (significance F=0.51, p=0.53). This suggests that we can not dismiss the null hypothesis that there is no significant variation in concentrations of cadmium over time. These results indicated that the cryogenic-milling process has statistically proven the short-term stability for materials from mussels in the chemical analysis of cadmium. Therefore, we propose that the Korean mussel's reference material developed for the proficiency test could be used as a tool to evaluate reliability and consistency in laboratories.

Piecewise exact solution for analysis of base-isolated structures under earthquakes

  • Tsai, C.S.;Chiang, Tsu-Cheng;Chen, Bo-Jen;Chen, Kuei-Chi
    • Structural Engineering and Mechanics
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    • 제19권4호
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    • pp.381-399
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    • 2005
  • Base isolation technologies have been proven to be very efficient in protecting structures from seismic hazards during experimental and theoretical studies. In recent years, there have been more and more engineering applications using base isolators to upgrade the seismic resistibility of structures. Optimum design of the base isolator can lessen the undesirable seismic hazard with the most efficiency. Hence, tracing the nonlinear behavior of the base isolator with good accuracy is important in the engineering profession. In order to predict the nonlinear behavior of base isolated structures precisely, hundreds even thousands of degrees-of-freedom and iterative algorithm are required for nonlinear time history analysis. In view of this, a simple and feasible exact formulation without any iteration has been proposed in this study to calculate the seismic responses of structures with base isolators. Comparison between the experimental results from shaking table tests conducted at National Center for Research on Earthquake Engineering in Taiwan and the analytical results show that the proposed method can accurately simulate the seismic behavior of base isolated structures with elastomeric bearings. Furthermore, it is also shown that the proposed method can predict the nonlinear behavior of the VCFPS isolated structure with accuracy as compared to that from the nonlinear finite element program. Therefore, the proposed concept can be used as a simple and practical tool for engineering professions for designing the elastomeric bearing as well as sliding bearing.

그린IT 이니셔티브들 전략적 영향들을 평가하기위한 지속가능한 BSC-IT 기반 프레임워크 (A Sustainable BSC-IT based Framework for Assessing the Strategic Impacts of Green IT Initiatives)

  • ;박정선
    • 대한안전경영과학회지
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    • 제14권4호
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    • pp.205-210
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    • 2012
  • We don't have time to waste, time is running, and the global warming is an issue that concerns to all of us. Information technology, which on a global level is responsible for 2% of emission of greenhouse gases. However, the remaining 98% is seen as an opportunity for IT to help our planet, our companies and our society. The purpose of this paper is to analyze green information technology (IT) initiatives and their strategic impact. And to have done this, we develope and create a very useful balanced-scorecard framework to explain, understand, and identify the direct and indirect contribution of green IT initiatives. The green IT evaluation framework, called here a sustainable green IT balanced scorecard, integrates the four BSC-IT perspectives with the Zuboff's automate/informate goals of information systems and the contribution of the sustainability (economic, social and environment). This study also seeks to answer the following questions: 1) what are the driving forces for implementing green IT initiatives? 2) How can an analytical framework be built to systematically analyze the benefits and strategic contribution of green IT initiatives? And 3) how green IT initiatives impact the strategic goals of a firm and how they can contribute to the triple bottom line? The framework demonstrates to be useful as a management tool to hopefully integrate environmental and social management with the general management of a company. Besides, the strategy map and measures for each cell of the framework are provided.

Development of a Novel Multiple Cross-Linking Spiral Amplification for Rapid and Sensitive Detection of HPV16 DNA

  • Zhang, Donghong;Liu, Dongliang;Liu, Bing;Ma, Xiulan
    • Journal of Microbiology and Biotechnology
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    • 제31권4호
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    • pp.610-620
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    • 2021
  • There has been increasing interest in the head and neck squamous cell carcinoma (HNSCC) that is caused by high-risk human papillomavirus (HR-HPV) and has posed a significant challenge to Otolaryngologists. A rapid, sensitive, and reliable method is required for the detection of HR-HPV in clinical specimens to prevent and treat HPV-induced diseases. In this study, a multiple cross-linking spiral amplification (MCLSA) assay was developed for the visual detection of HPV-16. In the MCLSA assay, samples were incubated under optimized conditions at 62℃ for 45 min, and after mixing with the SYBR Green I (SGI) dye, the positive amplicons showed bright green fluorescence while the negative amplicons exhibited no obvious change. The specificity test revealed that the developed MCLSA technique had high specificity and could effectively distinguish all five HPV-16 strains from other pathogenic microorganisms. In terms of analytical sensitivity, the limit of detection (LoD) of MCLSA assay was approximately 5.4 × 101 copies/tube, which was 10-fold more sensitive than loop-mediated isothermal amplification (LAMP) and RT-PCR. The detection results of laryngeal cancer specimens collected from 46 patients with suspected HPV infection in the Liaoning region demonstrated that the positive detection rates of MCLSA and hybridized capture 2 kit were 32.61% (15/46). The true positive rate of the MCLSA assay was higher than that of RT-PCR (100% vs. 93.33%) and LAMP (100% vs. 86.67%). Therefore, the MCLSA assay developed in the present study could be a potentially useful tool for the point-of-care (PoC) diagnosis of HR-HPV, especially in resource-limited countries.

Assessment of compressive strength of cement mortar with glass powder from the early strength

  • Wang, Chien-Chih;Ho, Chun-Ling;Wang, Her-Yung;Tang, Chi
    • Computers and Concrete
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    • 제24권2호
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    • pp.151-158
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    • 2019
  • The sustainable development principle of replacing natural resources with renewable material is an important research topic. In this study, waste LCD (liquid crystal display) glass powder was used to replace cement (0%, 10%, 20% and 30%) through a volumetric method using three water-binder ratios (0.47, 0.59, and 0.71) to make cement mortar. The compressive strength was tested at the ages of 7, 28, 56 and 91 days. The test results show that the compressive strength increases with age but decreases as the water-binder ratio increases. The compressive strength slightly decreases with an increase in the replacement of LCD glass powder at a curing age of 7 days. However, at a curing age of 91 days, the compressive strength is slightly greater than that for the control group (glass powder is 0%). When the water-binder ratios are 0.47, 0.59 and 0.71, the compressive strength of the various replacements increases by 1.38-1.61 times, 1.56-1.80 times and 1.45-2.20 times, respectively, during the aging process from day 7 to day 91. Furthermore, a prediction model of the compressive strength of a cement mortar with waste LCD glass powder was deduced in this study. According to the comparison between the prediction analysis values and test results, the MAPE (mean absolute percentage error) values of the compressive strength are between 2.79% and 5.29%, and less than 10%. Thus, the analytical model established in this study has a good forecasting accuracy. Therefore, the proposed model can be used as a reliable tool for assessing the design strength of cement mortar from early age test results.

Discrimination and bifurcation analysis of tumor immune interaction in fractional form

  • Taj, Muhammad;Khadimallah, Mohamed A.;Hussain, Muzamal;Rashid, Yahya;Ishaque, Waqas;Mahmoud, S.R.;Din, Qamar;Alwabli, Afaf S.;Tounsi, Abdelouahed
    • Advances in nano research
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    • 제10권4호
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    • pp.359-371
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    • 2021
  • A tumor immune interaction is a main topic of interest in the last couple of decades because majority of human population suffered by tumor, formed by the abnormal growth of cells and is continuously interacted with the immune system. Because of its wide range of applications, many researchers have modeled this tumor immune interaction in the form of ordinary, delay and fractional order differential equations as the majority of biological models have a long range temporal memory. So in the present work, tumor immune interaction in fractional form provides an excellent tool for the description of memory and hereditary properties of inter and intra cells. So the interaction between effector-cells, tumor cells and interleukin-2 (IL-2) are modeled by using the definition of Caputo fractional order derivative that provides the system with long-time memory and gives extra degree of freedom. Moreover, in order to achieve more efficient computational results of fractional-order system, a discretization process is performed to obtain its discrete counterpart. Furthermore, existence and local stability of fixed points are investigated for discrete model. Moreover, it is proved that two types of bifurcations such as Neimark-Sacker and flip bifurcations are studied. Finally, numerical examples are presented to support our analytical results.