• Title/Summary/Keyword: Analytical Techniques

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A Study on the Analytical Errors of Non-proficient Laboratories Participated in Quality Control Program (작업환경측정기관의 정도관리를 통한 분석능력이 미흡한 기관들의 분석오차 유발요인에 관한 고찰)

  • Park, D.W.;Shin, Y.C.;Park, S.H.;Lee, N.R.;Oh, S.M.;Yoon, C.S.;Paik, N.W.
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.4 no.1
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    • pp.96-102
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    • 1994
  • Factors affecting non-proficient analytical ability were compared and evaluated by rating of laboratories and round. Analyst Indices between proficient and non-proficient participants were different. Coefficients of determination($R^2$) for standard of toluene, xylene and trichloroethylene of the 4th round between some proficient and non-proficient participants were significantly different(p<0.05). But, there was no difference in the 5th round. Average desorption efficiency of non-proficient participants was 88%-98%, which was lower than 96%-100% of some randomly selected proficient participants. Also non-proficient participants have a large variance of desorption efficiency, 11.79-19.69%. In the 5th round, desorption efficiency of metyl iso-butyl ketone(MIBK) reported by all participants was lower than 90% tested by NIOSH and especially low compared to other analytes. Participants evaluated to be non-proficient in the metal part have 85%-100.84% of average recovery, which was larger variance than 98% of some proficient participants. Although it is difficult to find quantitatively factors causing non-proficiency in analytical ability, pretreatement techniques and experience of analyst seems to be more important factors to produce accurate analytical result.

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Techniques for Estimating Temper Bead Welding Process by using Temperature Curves of Analytical Solution (해석 해의 온도곡선을 이용한 템퍼비이드 용접공정 평가기술)

  • Lee, Ho-Jin;Lee, Bong-Sang;Park, Kwang-Soo;Byeon, Jin-Gwi;Jung, In-Chul
    • Journal of Welding and Joining
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    • v.28 no.5
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    • pp.51-57
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    • 2010
  • Brittle microstructure created in a heat affected zone (HAZ) during the welding of low alloy steel can be eliminated by post-weld heat treatment (PWHT). If the PWHT is not possible during a repair welding, the controlled bead depositions of multi-pass welding should be applied to obtain tempering effect on the HAZ without PWHT. In order to anticipate and control the tempering effect during the temper bead welding, the definition of temperature curve obtained from the analytical solution was suggested in this research. Because the analytical solution for heat flow is expressed as a mathematical equation of weld parameters, it may be effective in anticipating the effect of each weld parameter on the tempering in HAZ during the successive bead depositions. The reheating effect by the successive bead layer on the brittle coarse grained HAZ formed by earlier bead deposition was estimated by comparing the overlapped distance between the temperature curves in the HAZ. Three layered weld specimens of SA508 base metal with A52 filler were prepared by controlling heat input ratio between layers. The tempering effect anticipated by using the overlapped distance between the temperature curves was verified by measuring the micro-hardness distribution in the HAZ of prepared specimens. The temperature curve obtained from analytical solution was expected as a good tool to find optimal temper bead welding conditions.

Investigation of continuous and discontinuous contact cases in the contact mechanics of graded materials using analytical method and FEM

  • Yaylaci, Murat;Adiyaman, Gokhan;Oner, Erdal;Birinci, Ahmet
    • Computers and Concrete
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    • v.27 no.3
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    • pp.199-210
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    • 2021
  • The aim of this paper was to examine the continuous and discontinuous contact problems between the functionally graded (FG) layer pressed with a uniformly distributed load and homogeneous half plane using an analytical method and FEM. The FG layer is made of non-homogeneous material with an isotropic stress-strain law with exponentially varying properties. It is assumed that the contact at the FG layer-half plane interface is frictionless, and only the normal tractions can be transmitted along the contacted regions. The body force of the FG layer is considered in the study. The FG layer was positioned on the homogeneous half plane without any bonds. Thus, if the external load was smaller than a certain critical value, the contact between the FG layer and half plane would be continuous. However, when the external load exceeded the critical value, there was a separation between the FG layer and half plane on the finite region, as discontinuous contact. Therefore, there have been some steps taken in this study. Firstly, an analytical solution for continuous and discontinuous contact cases of the problem has been realized using the theory of elasticity and Fourier integral transform techniques. Then, the problem modeled and two-dimensional analysis was carried out by using ANSYS package program based on FEM. Numerical results for initial separation distance and contact stress distributions between the FG layer and homogeneous half plane for continuous contact case; the start and end points of separation and contact stress distributions between the FG layer and homogeneous half plane for discontinuous contact case were provided for various dimensionless quantities including material inhomogeneity, distributed load width, the shear module ratio and load factor for both methods. The results obtained using FEM were compared with the results found using analytical formulation. It was found that the results obtained from analytical formulation were in perfect agreement with the FEM study.

Differential transform method and Adomian decomposition method for free vibration analysis of fluid conveying Timoshenko pipeline

  • Bozyigit, Baran;Yesilce, Yusuf;Catal, Seval
    • Structural Engineering and Mechanics
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    • v.62 no.1
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    • pp.65-77
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    • 2017
  • The free vibration analysis of fluid conveying Timoshenko pipeline with different boundary conditions using Differential Transform Method (DTM) and Adomian Decomposition Method (ADM) has not been investigated by any of the studies in open literature so far. Natural frequencies, modes and critical fluid velocity of the pipelines on different supports are analyzed based on Timoshenko model by using DTM and ADM in this study. At first, the governing differential equations of motion of fluid conveying Timoshenko pipeline in free vibration are derived. Parameter for the nondimensionalized multiplication factor for the fluid velocity is incorporated into the equations of motion in order to investigate its effects on the natural frequencies. For solution, the terms are found directly from the analytical solution of the differential equation that describes the deformations of the cross-section according to Timoshenko beam theory. After the analytical solution, the efficient and easy mathematical techniques called DTM and ADM are used to solve the governing differential equations of the motion, respectively. The calculated natural frequencies of fluid conveying Timoshenko pipelines with various combinations of boundary conditions using DTM and ADM are tabulated in several tables and figures and are compared with the results of Analytical Method (ANM) where a very good agreement is observed. Finally, the critical fluid velocities are calculated for different boundary conditions and the first five mode shapes are presented in graphs.

Dynamic Nonling Analysis Model for Reinforced Concrete Elements Considering Strain Rate Effects under Repeated Loads (변형율속도를 고려한 반복하중을 받는 철근 콘크리트 부재의 동적 비선형 해석모델)

  • 심종성;문일환
    • Magazine of the Korea Concrete Institute
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    • v.2 no.2
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    • pp.73-80
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    • 1990
  • The current analytical techniques for R/C elements under severe dynamic repeated loads, like earth¬quake or impact, have two major problems; one is that the effects of strain rate are not considered and the other one is the current analytical model was developed based on flexural behavior only. This study develops computer software that can idealize the flexural and shear behavior of R/C elements using several parameters and also can consider the effects of strain rate. The analytical results using the developed technique were compared with serveral experimental results and they were generally satisfied.

Investigation on the techniques of quality control for radiation counting systems (방사선 측정기의 품질관리 기법에 대한 고찰)

  • Song, Byoung-Chul;Kim, Young-Bok;Han, Sun-Ho;Oh, Se-Jin;Lee, Myung-Ho;Song, Kyu-Seok
    • Analytical Science and Technology
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    • v.24 no.6
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    • pp.414-420
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    • 2011
  • In this study, radiation measurement system has been investigated to set up for the radioisotopes analysis in the radioactive waste samples after selecting the radiation counters of alpha beta and gamma nuclides. The counting efficiencies for alpha, beta and gamma measurement systems were calibrated. To obtain stability of the radiation detectors, quality control program has been established. Also, minimum detectable activities (MDAs) depending on the type of samples were calculated for increasing the confidence level for analytical result.

Analyses of Additives Applied in a Polycarbonate (폴리카보네이트에 사용된 첨가제의 분석)

  • Kim, Seog-Jun
    • Analytical Science and Technology
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    • v.13 no.3
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    • pp.282-290
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    • 2000
  • In this study, polymer additives were extracted and separated by Soxhlet extraction method and the dissolution-precipitation method from a polycarbonate (optical grade) which completely absorbed UV light below 390 nm. Analytical techniques such as UV-Vis spectroscopy, FT-IR, and HPLC were applied to analyze additives in polycarbonate. Separated materials from the polycarbonate may be a complex mixture containing additives such as UV stabilizer, antioxidants (primary and secondary), monomers, and oligomers. Several compounds such as bisphenol A, Irganox 1010, and Cyasorb UV-5411 were identified by chromatograms and UV spectra obtained from RP HPLC analysis using Bondapak $C_{18}$ column, methanol mobile phase, and a photodiode array (PDA) detector. Also, the content of UV-5411 in the polycarbonate was about 0.12 wt% by a quantitative analysis through UV spectroscopy.

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Development of Hybrid Extinction $SF_6$ Interrupter using Analytical and Experimental Method ($SF_6$ 자력팽창 소호부 개발에 관한 실험 및 해석적 고찰)

  • Sohn, J.M.;Kang, J.S.;Lee, B.W.;Kim, Y.K.;Kim, D.K.
    • Proceedings of the KIEE Conference
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    • 2001.07b
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    • pp.696-698
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    • 2001
  • This paper considers the research of the hybrid interrupter which adopts both rotating arc and thermal expansion technology. The operating principle of this device depends on rapid arc rotation due to the magnetic field created by the fault current through a coil which is mounted on contacts and also relies on the principle of thermal expansion created by arc energy in extinguishing chamber and finally causes pressure rise in expansion volume. To develope this type of interrupter, we introduced analytical analysis including electromagnetic and arc fluid simulation and experimental analysis including construction of current source generation facility and arc behavior measurements. In this research, the principle of the interrupting techniques are given and analytical and experimental results of hybrid interrupter which is developed by new technology is introduced.

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Facture Behavior Analysis of Box Culvert Specimen Using Non-local Damage Model (비국소 손상모델을 이용한 전력구 모형 실험체의 파괴거동 해석)

  • Kwon, Yong-Gil;Woo, Sang-Kyun;Han, Sang-Hoon;Song, Young-Cheul
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.225-228
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    • 2008
  • In case of nonlinear analysis for reinforced concrete structure, the characteristics of the failure, which are depend on loading conditions, such as tension splitting, compression crushing and shear distortion should be considered. On the analytical evaluation for the failure behavior of these, the finite element techniques is the most widely used. After the maximum load, however, an analytical results by finite element technique are depending on the size of the element. In this study, integral nonlocal model which is one of those study for overcoming the element sensitivity and dependancy, used for the failure analysis of box culvert specimen. Comparing on the experimental and analytical results, validity and reliability of integral nonlocal model are investigate.

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Performance Analysis of Space-Time Codes in Realistic Propagation Environments: A Moment Generating Function-Based Approach

  • Lamahewa Tharaka A.;Simon Marvin K.;Kennedy Rodney A.;Abhayapala Thushara D.
    • Journal of Communications and Networks
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    • v.7 no.4
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    • pp.450-461
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    • 2005
  • In this paper, we derive analytical expressions for the exact pairwise error probability (PEP) of a space-time coded system operating over spatially correlated fast (constant over the duration of a symbol) and slow (constant over the length of a code word) fad­ing channels using a moment-generating function-based approach. We discuss two analytical techniques that can be used to evaluate the exact-PEPs (and therefore, approximate the average bit error probability (BEP)) in closed form. These analytical expressions are more realistic than previously published PEP expressions as they fully account for antenna spacing, antenna geometries (uniform linear array, uniform grid array, uniform circular array, etc.) and scattering models (uniform, Gaussian, Laplacian, Von-mises, etc.). Inclusion of spatial information in these expressions provides valuable insights into the physical factors determining the performance of a space-time code. Using these new PEP expressions, we investigate the effect of antenna spacing, antenna geometries and azimuth power distribution parameters (angle of arrival/departure and angular spread) on the performance of a four-state QPSK space-time trellis code proposed by Tarokh et al. for two transmit antennas.