• Title/Summary/Keyword: Alumina oxide

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A study on the pore size control of nano template by anodic aluminum oxidation (양극산화를 이용한 나노템플레이트 기공 크기 제어에 관한 연구)

  • Lee, Su-Ho;Seo, Mun-Su;Yoo, Hyun-Min;Lee, Jae-Hyeong;Joung, Yeun-Ho;Lim, Dong-Gun;Hwang, Hyeon-Seok
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.1495-1496
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    • 2011
  • Anodic aluminum oxide (AAO) nanotemplates for nano electronic device applications have been attracting increasing interest because of ease of fabrication, low cost process, and possible fabrication in large area. The size and density of the nanostructured materials can be controlled by changing the pore diameter and the pole density of AAO nanotemplate. In this paper, AAO nanotemplate was fabricated by second anodization method. In addition, effects of electrolyte and anodization voltate on the microstructure of porous alumina films were investigated. Vertically well aligned pores had the average pore sizes of 15-70 nm and the length of approximately 40 ${\mu}m$.

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Comparison of cutting performance of an AWJ with several types of abrasives (Water jet 절단에서의 연마재 종류별 성능 비교 시험)

  • Choon Sunwoo;;Ryu Chang ha;Kwng soo Kwon
    • Tunnel and Underground Space
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    • v.6 no.2
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    • pp.175-183
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    • 1996
  • Linear cutting tests on granite were conducted to evaluated the cutting performance of abrasive water jet(AWJ) using several types of abrasives. The abrasives used in the tests were grarnet, alumimum oxide, and silicon carbide. And one type of granite which is comercially known as "KeuchangSuk" was used as workpiece throughout the tests. The results from the tests were described in terms of cutting depth and abrasive productivity. Authors tried to confirm the effects of the operational parameters of abrasive mass flow rate, water pressure, and traverse speed of nozzle on cutting depth and presented almost all the data obtained in the tests. Abrasive productivity can be defined as the area of kerf wall cut by unit weight of abrasive and is an important factor to evaluated the cutting ability of abrasive and assess the cost effectiveness of an AWJ system. In the tests the maximum abrasive productivities of garnet, alumina, and silicon carbide were about 0.21, 0.24, and 0.20 $\textrm{cm}^2$ respectively under similar operational conditions.onditions.

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Synthesis of Cu/Al2O3 Nanostructured Composite Powders for Electrode Application by Thermochemical Process (열화학적 방법에 의한 전극용 나노 Cu/Al2O3 복합분말 합성)

  • 이동원;배정현;김병기
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.337-343
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    • 2003
  • Nanostructured Cu-$Al_2O_3$ composite powders were synthesized by thermochemical process. The synthesis procedures are 1) preparation of precursor powder by spray drying of solution made from water-soluble copper and aluminum nitrates, 2) air heat treatments to evaporate volatile components in the precursor powder and synthesis of nano-structured CuO + $Al_2O_3$, and 3) CuO reduction by hydrogen into pure Cu. The suggested procedures stimulated the formation of the gamma-$Al_2O_3$, and different alumina formation behaviors appeared with various heat treating temperatures. The mean particle size of the final Cu/$Al_2O_3$ composite powders produced was 20 nm, and the electrical conductivity and hardness in the hot-extruded bulk were competitive with Cu/$Al_2O_3$ composite by the conventional internal oxidation process.

Anodic Oxide Membrane Formation of Hexagonal Pore Arrarys on Aluminium (다공성 알루미나 박막의 나노 스케일 구조 제어)

  • Jung, Kyung-Han;Shin, Hoon-Kyu;Kwon, Young-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.830-833
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    • 2002
  • 최근 나노 구조 (nano structure)를 만들기 위한 시도 중 하나로서 스스로 조직화(self organization)하여 나노 구조를 형성하는 물질을 나노 소자 제작을 위한 형틀 (template)로 이용하려는 시도가 활발히 진행되고 있다. 이러한 물질로서 주목을 받고있는 것 중 하나가 전해질 용액에서 알루미늄을 양극산화(anodization) 시켰을 때 형성되는 다공성 알루미나 박막이다. 본 연구에서는 고 순도 알루미늄을 기계적으로 연마(mechanical polishing)하고 공기 분위기에서 어닐링 (annealing)하여 알루미늄을 재결정화(recrystallization) 시키고 인가 전압이 40 V인 정 전압하에서 0.3 M의 수산(oxalic acid)을 전해질로 사용하면서 양극산화를 수행하여 평균 직경이 65 nm인 고도로 배열된 육방밀집구조의 나노 다공성 박막을 제작하였다. 또한 같은 방향의 육방밀집 배열은 크기가 수 ${\mu}m$인 영역(grain)을 형성하고 있었으며, 평균적인 pore의 밀도는 $1.1{\times}10^{10}/cm^2$였다.

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각종 치과용 합착 Cement의 색소침투에 관한 실험적 연구

  • Chin, Yong-Whan;Kim, Sang-Se;Lee, Eun-Ho;Kim, Sung-Il;Ahn, Sang-Kyu
    • The Journal of the Korean dental association
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    • v.12 no.8
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    • pp.613-617
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    • 1974
  • The authors have studied the marginal leakage of various dental cements; Fynal cement (Caulk), Zinc cement (S.S. White) Carbo cement (Shofu, Poly-carboxylate cement), EBA cement (Opotow alumina cement), Propac (G-C's zinc oxide euginol cement), and Super cement (Shofu oxyphosphate zinc cement), by means of penetration of 2% methylene blue solution between orden crown restorations and human teeth in 150 cases. The result revealed as follow 1. None of the cements tested were free from dye penetration. 2. There was a wide difference in dye penetration among the trade brands of dental cement when immersed in dye solution before setting of cements. 3. EBA cement and Carbo cement showed comparatively low grade of dye penetration at the restorative margins.

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Ballistic Resistance of an Armor Ceramic Structure against a Shaped Charge Jet As a Function of Penetration Depth

  • Hyunho Shin;Lee, Chang-Hyun;Wan Sung
    • The Korean Journal of Ceramics
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    • v.5 no.3
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    • pp.270-277
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    • 1999
  • The ballistic capability of an alumina-rich oxide armor ceramic against a shaped jet was characterized as a function of penetration depth in a layered target structure. The penetration resistance of the ceramic, based upon the determination of penetration velocity, was not equally realized throughout the depth of penetration. It was abnormally low at an early stage of penetration, followed by a sudden increase to reach ~16GPa thereafter. There was no apparent change in such a profile with respect to the lateral size of the specimen. Based upon 2-D flash x-ray radiography and 3-D Hull code simulation, the feasibility of forming a pressure-induced predamnaged zone in front of the jet tip was speculated to foster an increased penetration velocity in the initial stage penetration, resulting in the diminished penetration resistance. The disappearance of such a predamaged zone with penetration was interpreted to restore the resistance of the ceramic in the later penetration stage.

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An Experimental Study on the Tensile Strength of Dental Cements (치과용 Cement의 장력에 관한 실험적 연구)

  • Suh, Kyu-Won
    • The Journal of the Korean dental association
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    • v.11 no.1
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    • pp.41-44
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    • 1973
  • The experiment consisted of cementing full veneer crown of extracted teeth and a standardized cylindrical metal dies (6mm diameter, 6mm height, 1mm shoulder) and then measuring the tensile strength required to remove the cemented restoratoins by the Instron testing machine in the Korea Institude of Science and Technology. The Instron machine was operated at a rate of loading of 0.2cm per minute. From the experiments, the following results obtained. 1. The tension of zinc phosphate and alumina EBA cements were highest all of the cements. 2. The tension of Fynal and the addition of eugenol to zinc Phosphate cements were similar. The addition of eugenol to zinc phosphate cement was half stength and Fynal cement was on third strength than zinc phosphate cement. 3. The tension of zinc oxide-eugenol cement was lowest all of the cements.

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An Investigation on the Dielectric and Microwave Properties of Ag(Ta,Nb)O3 Thick Films on the Alumina Substrates (알루미나 기판에 스크린 프린팅된 Ag(Ta,Nb)O3 후막의 유전특성 및 초고주파 특성에 대한 연구)

  • Lee, Ku-Tak;Koh, Jung-Hyuk
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.11
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    • pp.925-928
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    • 2011
  • Perovskite niobates and tantalates have been placed on a short list of functional materials for future technologies. This article was investigated ferroelectric materials $Ag(Ta,Nb)O_3$ thick film. In this study, we have fabricated the $Ag(Ta,Nb)O_3$ thick film on the $Al_2O_3$ substrates by screen printing method. The $Ag(Ta,Nb)O_3$ thick film were fabricated by the mixed oxide method. The sintering temperature and time were 1,150$^{\circ}C$, 2 hr. The electrical properties of $Ag(Ta,Nb)O_3$ thick film were investigated at 30~100$^{\circ}C$.

Preparation of Titanium Carbide Fiber-Reinforced Alumina Ceramic Matrix Composites by Self-Propagating High-Temperature Synthesis

  • Yun, Jondo;Bang, Hwancheol
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.171-175
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    • 1998
  • $Al_2O_3$-TiC composites were prepared from aluminum, titanium oxide, and carbon fibers by self-propagating high-temperature synthesis(SHS). After the SHS reaction, the TiC phase in the sample was found either fibrous or non-fibrous shape. The fraction of the fibrous TiC phase varied with the amount of $Al_2O_3$ diluent addition. The optimum amount of diluent to make fibrous carbide was determined to be 30%. The fibers were hollow inside and made of multiple grains with a composition of titanium carbide. The hollow fiber formation mechanism was suggested and discussed. The synthesized powders were consolidated to dense composites by hot pressing at $1750^{\circ}C$ under 30 MPa.

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Preparation of Yttria Stabilized zirconia Films by the Electrochemical Vapor Deposition (전기화학증착에 의한 이트리아 안정화 지르코니아 박막의 제조)

  • 정지원;박동원;전치훈;최병진;김대룡
    • Journal of the Korean Ceramic Society
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    • v.31 no.5
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    • pp.477-484
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    • 1994
  • The yttria stabilized zirconia(YSZ) thin films for solid oxide fuel cell (SOFC) were fabricated by an electrochemical vapor deposition(EVD) technique using YCl3+ZrCl4+H2O gas system. The YSZ films were deposited under reduced pressure at the temperature of 1000~120$0^{\circ}C$ on the porous alumina substrates. The deposition rate, chemical composition and growth morphology were investigated by SEM, XRD, EDS. The growth rates of the films obeyed a parabolic rate law, representing that the growing process is controlled by an electrochemical transport through the YSZ film. The Y2O3 content of the films was about 10 mol%, equal to the composition of metal chloride reactant gases, approximately. The YSZ films were highly dense, the growing features showed columnar structure and surface morphologies were changed with the EVD conditions.

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