• Journal of the Korean Ceramic Society
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• v.36 no.6
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• pp.662-670
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• 1999

Porous alumina was fabricated from pressureless powder packing forming method using powders granulated by spray drying. It was investigated the pore size distribution of fabricated porous alumina. The results of microstructural observation showed that intraganular pore size and intragranular pore size. At 1700$^{\circ}C$ there were no intragranular pores but it showed homogeneous distribution of intergranular pore size. The bending strength and shrinkage increased as porosity decreased. In case of thermal shock resistance sudden decrease of bending strength to $\Delta$T was not shown because intergranular large pore prevented sudden crack propagation.

• Journal of the Korean Society for Precision Engineering
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• v.23 no.1 s.178
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• pp.80-88
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• 2006

In this study, unsintered and presintered low purity alumina ceramics were machined with various tools to clarify the machinability and the optimum cutting conditions. The main conclusions obtained were as fellows. Machined with ceramic tool, the ceramics presintered at the temperature range of $1000\~1100^{\circ}C$ showed the best machinability due to the adhesion formed in weared surface within a certain cutting speed range. In the above combination and conditions, the ceramic tool showed the highest productivity through all experiments. The life of CBN tool was longer in machining of the ceramics presintered at $1000^{\circ}C$ than in the case of that presintered at $600^{\circ}C$, but the diamond tool showed adverse tendency. In machining of the ceramics presintered at $1000^{\circ}C$, the ceramic tool exhibits the longest tool life in high speed, the tool lives became extremely worse in the order of CBN tool and diamond tool. However, in the case of the ceramics presintered at $600^{\circ}C$, the diamond tool shows the longest tool life, the tool lives was much worse in the order of CBN tool and ceramic tool.

• Journal of the Korean Ceramic Society
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• v.39 no.2
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• pp.164-170
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• 2002

Measurements of sedimentation, solid loading, zeta potential, and viscosity were employed to determine a proper dispersant and its amount for a well dispersed alumina powders in aqueous alumina tape casting using acrylate as a binder. Polycarboxylic acid was the most effective one among various dispersants considered in the present study and its amount was 0.23∼0.24 g per 100 g alumina for a dispersion. Better dispersion was obtained as an increase of dispersant addition. However, the dispersion was hindered as the amount of dispersant was higher than the optimum amount because of bridging or tangling of polymer chains. Excellent aqueous alumina tapes were prepared from the slurry containing the optimum amount of the polycarboxylic acid (0.2g), alumina powders(100 g), acrylate and Benzoflex as binder and plasticizer, respectively. The viscosity of the slurry was 570 cps and the alumina loading in the tape was 57 vol%.

• Journal of the Korean Ceramic Society
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• v.36 no.10
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• pp.1062-1068
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• 1999

The flexural strength distribution of alumina ceramics was observed using ball-on-3 ball test after thermal shock into the distilled water of 25$^{\circ}C$ Crack distribution was also observed by dye-penetration after thermal shock test. Fracture probability of alumina ceramics by ball-on-3 ball test was studied and compared with that by 3-point bending test. The crack distance from the center of thespecimen showed the stronger effect on the flexural strength by ball-on-3 ball test than the crack density.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.8
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• pp.2073-2080
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• 1994

In this paper, a model of material removal in abrasive water jet machining of brittle material is developed, and experimentally evaluated. Abrasive water jet machining proved to yield better material removal rate than other machining techniques for hard and brittle material (alumina ceramics). It was also found that large scale fracture may develop at the exit of the jet from the material. The fracture size was predicted as a function of water jet pressure and size of the hole. Finally, the feasibility of using acoustic emission signals for in-process monitoring of the abrasive water jet machining process is investigated.

• Journal of the Korean Ceramic Society
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• v.30 no.9
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• pp.747-753
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• 1993

The investigation was carried out to study the behaviors of the pore size and porosity, the mechanical strength, the resistance to thermal spallings and slag attacks according to particle sizes of starting raw materials in porous high Alumina ceramics. This porous ceramics have been used in processing of the clean steel by the blowing of the inert gas. The required properties in the practice are the suitable pores size, the sharp pores distribution for a uniform blowing of the gas, the strong corrosion resistance to slags and molten metals and the resistance to thermal spalling. The optimized properties in porous high alumina ceramics of the specimen No. 3 was found to be the very low slag intrusion and the superior resistance to thermal spalling because of the suitable pore size of 2.5${\mu}{\textrm}{m}$, the porosity of 30% and the high sinterability.

• Journal of the Korean Society for Precision Engineering
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• v.24 no.2 s.191
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• pp.33-40
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• 2007

In this study, presintered and full sintered low purity alumina ceramics were machined with various tools to clarify the effect of cutting fluid in machinability. The main conclusions obtained were as follows. When the presintered ceramics were wet machined with sintered diamond tool, the tool wear becomes extremely large, and higher cutting speed can be used than in the case of full sintered ceramics. The productivity of wet cutting with the sintered diamond tool is much higher than that of dry cutting. In the case of the CBN and ceramic tools, the tool wear were smaller at wet cutting than at dry cutting, especially exhibiting considerably larger grooved tool wear in wet cutting with ceramic tool.

• Journal of the Korean Society for Precision Engineering
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• v.27 no.5
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• pp.14-21
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• 2010

In this study, presintered low purity alumina ceramics were machined with various tools to clarify the effects of the tool material, cutting condition and tool geometry on machinability. The main conclusions obtained were as follows. (a)The wear of tungsten carbide tool becomes smaller with the increase of the feed and clearance angle, and with the decrease of rake angle, especially exhibiting considerably smaller wear with both the decrease of rake angle and the increase of clearance angle. (b) So far as turning the ceramic presintered at low temperature, the diamond tool shows the best performance with higher feed. (c) The effect on the tool wear of the feed, clearance angle and rake angle becomes smaller in turning the ceramic presintered at higher temperature. (d) The tool wear is not severely affected by the depth of cut.

• Bulletin of the Korean Chemical Society
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• v.25 no.6
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• pp.843-846
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• 2004

Pt nanoparticles loaded on alumina through an impregnation at room temperature was prepared using $K_2PtCl_4$ and acrylic acid as capping material. Transmission electron microscopy showed that the deposited Pt particles indicate ca. 80% cubic shapes with a narrow distribution of 8-10 nm in size. Propylene hydrogenation over the catalyst has been carried out to evaluate their catalytic performance by the values of activation energy. It is determined from the initial rate, reaction order, and rate constant and is found to be $9.7{\pm}0.5$ kcal/mol. This value has been discussed by comparing to those of encapsulated- and truncated octahedral Pt nanoparticles deposited on alumina, respectively, to study influence of the particle size and shape, and capping material used on the activation energy.

• Journal of the Korean Ceramic Society
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• v.36 no.8
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• pp.871-875
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• 1999

Theoretical equation to calculate thermal fatigue life was derived in which slow crack growth theory was adopted. The equation is function of crack growth exponent n. Cyclic thermal fatigue tests were performed at temperature difference of 175, 187 and 200$^{\circ}C$ respectively. At each temperature difference critical thermal fatigue life cycles of the alumina ceramics were 180,37 and 7 cycles. And theoretical thermal fatigue life cycles were calculated as 172, 35 and 7 cycles at the same temperature difference conditions. Therefore thermal fatigue behavior of alumina ceramics can be represented by derived equation. Also theoretical single cycle critical thermal shock temperature difference can be calculated by this equation and the result was consistent with the experimental result well.