• Title/Summary/Keyword: Al-Fe

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Assessment of Bottom NiFe Anomalous Exchange Bias by hi ion Beam Etching of Top NiFe in NiFe/FeMn/Al/NiFe (상부 NiFe의 Ar 이온빔 에칭에 의한 NiFe/FeMn/Al/NiFe 구조의 다층박막에서 하부 NiFe 교환바이어스 조사)

  • 윤상민;임재준;김철기;김종오
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.236-236
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    • 2003
  • 교환바이어스(exchange bias)현상은 강자성과 반강자성의 접합계면에서 강한 상호 교환결합력에 의해 발생하는 것으로 알려져 있다. 이 현상은 1956년 Meiklejohn과 Bean에 의해 CoO층으로 둘러싸인 Co 입자에서 발견된 이후[l], 강자성과 반강자성의 접합계면을 가지는 다층박막에서의 교환바이어스에 대한 연구가 진행되어왔다[2-6]. 이는 강자성/반강자성 박막의 교환바이어스 특성을 이용하여, 강자성 박막의 스핀방향을 고정시킬 수 있기 때문이다. 이러한 교환바이어스 특성은 하드드라이브의 고밀도 자기헤드소자 및 비휘발성 자기메모리소자에 응용되어지는 등 경제적 가치를 갖는 기술적인 면과 교환바이어스라는 자기특성의 학문적인 가치로 인해 이 분야에 대한 집중적인 투자와 연구가 이루어지고 있다. 최근에는 교환바이어스 현상의 원인과 형성기구에 대한 연구가 활발히 진행되고 있다. 그러나 강자성과 반강자성 박막의 단거리 상호 교환결합력에 의한 교환바이어스 현상은, 계면의 원자구조, 자기구조 및 각자성층의 여러 가지 인자들에 대해서 지속적으로 연구되고 있다.

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Aluminizing and Corrosion of Carbon Steels in N2/0.5%H2S Gas at 650-850℃

  • Abro, Muhammad Ali;Lee, Dong Bok
    • Journal of the Korean institute of surface engineering
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    • v.48 no.3
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    • pp.110-114
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    • 2015
  • The effect of hot-dip aluminizing on the corrosion of the low carbon steel was studied at $650-850^{\circ}C$ for 20-50 h in $N_2/0.5%\;H_2S$ gas. The aluminized steel consisted primarily of the Al topcoat and the underlying Al-Fe alloy layer. Aluminizing drastically improved the corrosion resistance by forming the ${\alpha}-Al_2O_3$ surface scale. Without aluminizing, the steel formed nonadherent, fragile, thick scales, which consisted of FeS as the major phase and iron oxides such as FeO, $Fe_3O_4$ and $Fe_2O_3$ as minor ones.

반사방지 VF2-TrFE 박막을 이용한 태양전지 특성

  • Jeong, Sang-Hyeon;Yeon, Je-Min;Min, Gwan-Hong;;Yu, Jeong-Jae;Kim, Gwang-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.315.2-315.2
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    • 2013
  • 본 논문에서는 반사방지 VF2-TrFE 박막을 이용한 MIS Solar cell을 제작하여 전기적, 구조적 특성을 평가하였다. ALD법을 이용하여 고유전율의 화학적 안정성이 우수한 산화알루미늄을 절연층으로 한 Al/Al2O3/Si(100)을 제작하였으며 cell의 효율을 향상시키기 위해 spin coating법을 이용하여 VF2-TrFE 반사방지막을 증착시켰다. 제작된 반사방지 VF2-TrFE 박막 MIS solar cell은 MIS 커패시터의 전류밀도-전계 특성, 커패시턴스-전압 특성과 반사방지막 열처리 조건에 따른 태양전지 효율을 Solar simulator 및 Quantum Efficiency system으로 측정하였다.

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MAGNETIC PROPERTIES OF NANOCRYSTALLINE (Fe,Co)-B-Al-M (M=Nb/Mo/Ta) ALLOYS

  • Kang, D.B.;Cho, W.S.;Kim, T.K.;Cho, Y.S.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.483-486
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    • 1995
  • Soft magnetic properties of Fe-based (Fe,Co)-B-Al-M (M=Nb, Mo or Ta) nanocrystalline alloy have been investigated. The alloy obtained directly form the rapid solidification process. Microstructure of the alloy is a mixtu re of ultrafine bcc Fe(Co) nanocrystallines and a small amount of retained amorphous phase. Heat treatment of as-prepared alloys improves soft magnetic properties in high frequency range. ${(Fe_{.85}Co_{.15})}_{70}B_{18}Al_{10}Ta_{6}$ alloy alloy annealed at $500^{\circ}C$ for 1 h shows the most improved soth magnetic properties among the alloy examined. Average grain size of the nanocystalline is about 10 nm.

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Magnetic Characteristics of YIG ferrites with Sintering Temperature (소결온도에 따른 YIG 페라이트의 자기적 특성)

  • 양승진;윤종남;최우석;김정식
    • Journal of the Microelectronics and Packaging Society
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    • v.10 no.1
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    • pp.65-69
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    • 2003
  • Microstructural and electromagnetic properties of YIG ferrites, (Y, Ca)-(Fe, V, In, Al)-O for Isolator/Circulator were investigated with the sintering temperature. YIG ferrites of $Y_{2.1}Ca_{0.9}Fe_{4.4}V_{0.5}In_{0.05}Al_{0.05}O_{12}$ were fabricated by sintering at $1300^{\circ}C$, $1330^{\circ}C$, $1350^{\circ}C$, $1370^{\circ}C$. Crystallographic and microstructural properties were measured using XRD and SEM. Saturation magnetization$(4{\pi}M_s)$ were measured using VSM, and FMR(Ferromagnetic Resonance) experiment was conducted to measure ferromagnetic resonance line width$({\Delta}H)$. Microwave characteristics of YIG ferrites were measured using a Network Analyzer. The YIG ferrite of $Y_{2.1}Ca_{0.9}Fe_{4.4}V_{0.5}In_{0.05}Al_{0.05}O_{12}$, sintered at $1350^{\circ}C$, showed higher density, saturation magnetization and lower ferromagnetic resonance line width than those sintered at any other temperature.

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A Study of Acid Leaching for Metallurgical Grade Silicon Manufacturing Improved Purity (순도가 향상된 금속급 실리콘 제조를 위한 산침출 연구)

  • Um, Myeong-Heon;Ha, Beom-Yong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.11
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    • pp.118-123
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    • 2017
  • To manufacture MG-Si (Metallurgical grade silicon) for use in various industries, Acid leaching experiments were performed to remove aluminum (Al) and iron (Fe), which are the most common impurities found in the silicon raw material. The silicon raw material was reacted with five types of acids (HCl, HF, H2SO4, HNO3, H3PO4) at 1, 2, 4, and 6M; 1M HF showed the highest Al and Fe removal rates, 97.9% and 95.2%, respectively. HF, however, resulted in an 18% reduced yield due to the silicon corrosion properties. To minimize the yield reduction, 2M HCl, which has a second removal ratio result, was mixed with 1M HF and applied to the silicon raw material. The experiment was conducted to select the optimal conditions for the mixed solution, which were $80^{\circ}C$ and 2hr. Under the optimal conditions, the residual Al and Fe concentrations were 141 ppmw and 93 ppmw, respectively, and it very easy to produce MG-Si with 3N grade purity.

The Effects of Current Adjustment on the Preparation of Fe-Al Intermetallic Compounds by Field-Activated Combustion Synthesis (FACS법에 의한 Fe-Al계 금속간화합물의 제조시 통전방식의 영향)

  • Yun, Gi-Seok;Jeong, Jung-Chae;Won, Chang-Hwan
    • Korean Journal of Materials Research
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    • v.9 no.7
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    • pp.680-687
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    • 1999
  • Fe-Al intermetallic compounds were manufactured by using the field-activated combustion synthesis process. Effects of chemical composition(Fe:Al= 3: 1,2:1, 1:1, 1:2, 1:3), Compaction pressure(150, 250, 350MPa) and electrical resistance on the reaction were investigated in this system. As the molar ratio of Al, compaction pressure and electric field increased, the combustion temperature and velocity were increased. The influences for reaction with current adjust way were investigated in this system. But in the absence of a electric field, the reaction could sustain a nonsteady combustion wave and was not completed. The reaction products were characterized with X-ray, SEM and EDXS to determine the structure and composition.

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The Behavior of Carbon on the Damping Characteristics of Fe-5.7% Al Alloy (Fe-5.7% Al 합금의 제진특성에 미치는 탄소의 거동)

  • Lee, J.H.;Lee, M.J.;Lee, K.H.;Shin, M.C.
    • Analytical Science and Technology
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    • v.8 no.2
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    • pp.195-203
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    • 1995
  • Carbon and small amounts of alloying elements were added in Fe-5.7% Al ferromagnetic damping alloy. The specific damping capacities(SDC) of these alloys were investigated in relation to the grain size and the magnetic hysteresis loops. The behavior of carbon was analysed by XRD and EDS. These alloys showed characteristic damping nature of ferromagnetic damping materials. The alloying elements decreased SDC and especially the carbon was remarkable. The SDC was observed to be not related with the grain size but with the magnetic hysteresis loop area. The remarkable decrease of SDC by carbon addition was attributed to the locking migration of $90^{\circ}$ magnetic domain wall by the interstitial carbon in Fe-Al solid solution. However, the carbides also seems to decrease the SDC.

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Electrochemical Corrosion Characteristics of the Iron-based Damping Alloy (철기제진합금의 전기화학적 부식특성)

  • Shim, Hyun Yee;Jee, Choong Soo;Lee, Jin Hyung;Lee, Kyu Hwan;Shin, Myung Chul
    • Analytical Science and Technology
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    • v.8 no.1
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    • pp.85-90
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    • 1995
  • Corrosion characteristics of 4 kinds of the Fe-Al damping alloys has been studied in the 3.5% NaCl solution and compared with a cold rolled mild steel and pure Ti, No passivation, besides Ti, was observed in the Fe-Al damping alloys and a cold rolled mild steel. Corrosion rate was decreased with lower carbon concentration. In the case of Mn addition for improving damping capacity, corrosion rate was decreased in scrap iron but was not decreased in electrolytic iron. It has been shown that corrosion rate of Fe-Al damping alloys lays between that of the pure Ti and that of a cold rolled mild steel.

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Estimation of Heavy Metal Loads at Plain Area of the Rural Watersheds during Farming Season (영농기 농촌 평야지 유역의 중금속 부하량 산정)

  • Kim, Jin-Ho;Han, Kuk-Heon
    • Journal of The Korean Society of Agricultural Engineers
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    • v.50 no.1
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    • pp.85-92
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    • 2008
  • This study was carried out to estimate heavy metal loads at plain area of the rural watersheds during farming season in 2006. The experimental area was belonging to Geum River watershed. That was located at the center of South Korea. Water samples were corrected at two kinds of aspects. One is regular sampling(every two month) and the other is irregular sampling(every rainfall event). The result showed that heavy metal properties of regular samples were highest at May and June with lively agricultural activities. Heavy metal concentration of irregular samples was lower than that of regular samples. But the heavy metal loads of irregular samples were high. The correlation between each heavy metals of regular samples was following as Mn-Cd > Mn-Fe > Mn-Al > Fe-Al > Al-Cd. The correlation of irregular samples was following as Fe-AI > Zn-Mn > Fe-Cd > Cd-Al. Loading rates of daily discharge the plain area of designed rural watershed during farming season were Al 3.070 kg/day, Cu 0.526 kg/day, Fe 0.745 kg/day, Zn 0.314 kg/day, Cd 0.010 kg/day, Cr 0.055 kg/day, Mn 0.140 kg/day and Pb 0.098 kg/day. Loading rate of discharge with heavy metals during the survey period was Al(577.23 kg) > Fe(140.08 kg) > Cu(98.93 kg) > Zn(58.99 kg) > Mn(26.34 kg) > Pb(18.51 kg) > Cr(10.34 kg) > Cd(1.93 kg).