• Title/Summary/Keyword: Age hardening

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The Effect of the Heating Conditions on the Warm Hydro-Formability of the Alumium Alloys (알루미늄합금의 열간 액압성형법 성형성에 대한 가열조건의 영향도 분석)

  • Kim, Bong-Joon;Park, Kwang-Su;Ryu, Jong-Soo;Son, Sung-Man;Moon, Young-Hoon
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.3
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    • pp.172-176
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    • 2005
  • Modern automobiles are built with a steadily increasing variety of materials and semifinished products. The traditional composition of steel sheet and cast iron is being replaced with other materials such as aluminum and magnesium. But low formability of these materials has prevented the application of the automotive components. The formability can be enhanced by conducting the warm hydroforming using induction heating device which can raise the temperature of the specimen very quickly. The specimen applied to the test is A6061, A7075 extruded tubes which belong to the age-hardenable aluminum alloys. But in the case of A6061 age hardening occurs at room temperature or at elevated temperatures before and after the forming process. In this study the effects of the heating condition such as heating time, preset temperature, holding time during die closing and forming time on the hydroformability are analyzed to evaluate the phenomena such as dynamic strain hardening and ageing hardening at high temperatures after the hydroforming process.

A Study on Forming of Al-Zn-Mg-Sc Aluminum Alloy Bolts (Al-Zn-Mg-Sc 알루미늄 합금 볼트 성형에 관한 연구)

  • Yoon, D.J.;Hahm, S.Y.;Lee, Y.S.
    • Transactions of Materials Processing
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    • v.21 no.7
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    • pp.447-452
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    • 2012
  • This paper is concerned with forming of Al-Zn-Mg-Sc aluminum alloy bolts, focusing on the effects of heat treatment and age-hardening on the formability and ductile damage evolution. Both experimental and finite element studies were performed. From the experiments, it is observed that the heat treatment or the normalization of Al-Zn-Mg-Sc aluminum alloy increases its formability dramatically resulting in successful bolt forming, while the effects of age-hardening at room temperature on the stress-strain relationship and formability are not very critical. Deformation characteristics such as distribution of effective stress and strain, material flow, and ductile damage evolution during bolt forming are examined using a commercial finite element package, Deform-2D. It should be noted that the extrusion load predicted by the finite element method matches well the experiment results. The finite element predictions on the deformation characteristics support the experimental observations such as fracture of bolt head flange, material flow, and distribution of hardness.

Assessment of Early-age Properties of Mortar by Monitoring of Ultrasonic Pulse Velocity (초음파 속도 모니터링에 의한 모르터의 초기재령 특성 평가)

  • 이회근;이광명
    • Proceedings of the Korea Concrete Institute Conference
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    • 2001.11a
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    • pp.245-250
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    • 2001
  • Ultrasonic pulse velocity(UPV) is a useful tool for examining the property of early-age mortar or concrete. Thus, UPV has been used for a long time to characterize setting and hardening of cementitious materials. In this study, in order to investigate the characteristics of setting for mortar, UPV was measured using automatic monitoring system up to 3 days after casting. Test results show that UPV of high water to binder ratio(w/b) mortar remained constant at the beginning of hydration and then abruptly began to increase. However, UPV of low w/b mortar gradually increase due to setting retard caused by use of superplasticizer. Furthermore, the development of UPV for mortar with fly ash is slower than that of mortar without fly ash. It was concluded that the property change of mortar or concrete, such as setting and hardening can be assessed by monitoring of UPV.

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Modeling of temperature history in the hardening of ultra-high-performance concrete

  • Wang, Xiao-Yong
    • Journal of the Korea Institute of Building Construction
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    • v.14 no.3
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    • pp.273-284
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    • 2014
  • Ultra-high-performance concrete (UHPC) consists of cement, silica fume (SF), sand, fibers, water and superplasticizer. Typical water/binder ratios are 0.15 to 0.20 with 20 to 30% silica fume. In the production of ultra-high performance concrete, a significant temperature rise at an early age can be observed because of the higher cement content per unit mass of concrete. In this paper, by considering the production of calcium hydroxide in cement hydration and its consumption in the pozzolanic reaction, a numerical model is proposed to simulate the hydration of ultra-high performance concrete. The heat evolution rate of UHPC is determined from the contributions of cement hydration and the pozzolanic reaction. Furthermore, by combining a blended-cement hydration model with the finite-element method, the temperature history in the hardening of UHPC is evaluated using the degree of hydration of the cement and the silica fume. The predicted temperature-history curves were compared with experimental data, and a good correlation was found.

Changes in Hardness and Damping Capacity of Aged Mg-5%Sn Alloy (시효한 Mg-5%Sn 합금의 경도와 진동감쇠능 변화)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.5
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    • pp.255-261
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    • 2022
  • In this work, the strain-amplitude independent and strain-amplitude dependent damping capacities of Mg-5%Sn alloy have been investigated as a function of its age-hardening response. The hardness increased with an increase in aging time, reached a peak value after 48 h, and then it gradually decreased. The damping capacities of the Mg-5%Sn alloy exhibited a decreasing tendency in the order of solution-treated, under-aged, peakaged, and over-aged states in the strain-amplitude dependent region, whereas they increased continuously with aging time in the strain-amplitude independent region. The microstructural examination during aging revealed that the lower concentration of Sn solutes in the α-(Mg) matrix and the lower density of the Mg2Sn precipitate particles may well be the crucial factors for better damping values in the strain-amplitude independent and strain-amplitude dependent regions, respectively.

Phase transformation and grain boundary precipitation related to the age-hardening of an Au-Ag-Cu-Pt-Zn alloy for crown and bridge fabrication (관교의치용 Au-Ag-Cu-Pt-Zn 합금의 시효경화성과 관련된 상변태와 입계석출)

  • Cho, Mi-Hyang
    • Journal of Technologic Dentistry
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    • v.34 no.4
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    • pp.345-352
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    • 2012
  • Purpose: The age-hardening mechanism of an Au-Ag-Cu-Pt-Zn alloy for crown and bridge fabrication was investigated by means of hardness test, X-ray diffraction study and field emission scanning electron microscopic observation. Methods: Before hardness testing, the specimens were solution treated and then were rapidly quenched into ice brine, and were subsequently aged isothermally at $400-450^{\circ}C$ for various periods of time in a molten salt bath and then quenched into ice brain. Hardness measurements were made using a Vickers microhardness tester. The specimens were examined at 15 kV using a field emission scanning electron microscope. Results: By the isothermal aging of the solution-treated specimen at $450^{\circ}C$, the hardness increased rapidly in the early stage of aging process and reached a maximum hardness value. After that, the hardness decreased slowly with prolonged aging. However, the relatively high hardness value was obtained even with 20,000 min aging. By aging the solution-treated specimen, the f.c.c. Au-Ag-rich ${\alpha}_0$ phase was transformed into the Au-Ag-rich ${\alpha}_1$ phase and the AuCu I ordered phase. Conclusion: The hardness increase in the early stage of aging process was attributed to the formation of lattice strains by the precipitation of the Cu-rich phase and then subsequent ordering into the AuCu I-type phase. The decrease in hardness in the later stage of aging process was due to the release of coherency strains by the coarsening of tweed structure in the grain interior and by the growth and coarsening of the lamellar structure in the grain boundary. The increase of inter-lamellar space contributed slightly to the softening compared to the growth of lamellar structure toward the grain interior.

Grain Refining and Age Hardening of Mg-Zn Alloys by Addition of Cu and Si (Cu 및 Si첨가에 의한 Mg-Zn합금계의 입자미세화 및 시효경화)

  • Hwang, Jin-Hwan;Nam, Tae-Hyeon;An, In-Seop;Kim, Yu-Gyeong;Heo, Gyeong-Cheol;Heo, Bo-Yeong
    • Korean Journal of Materials Research
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    • v.5 no.6
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    • pp.682-689
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    • 1995
  • In order to refine the grain size of Mg-Zn alloy 0.5 to 6wt.%Cu or Si elements were added. Alloy ingot was made under vacuum atmosphere of 4 ${\times}$ 10$\^$-4/ Torr in the quartz tube coated by BN. Grain size and hardness were measured after solution treatment for 8 hours at 435$^{\circ}C$. Optimal condition for grain size refining effect was obtained at the minimum composition of 2wt.%Cu or 1.5wt.%Si addition to Mg-6wt%Zn alloy. Age hardening behavior was experimented at the optimal compositions of the Mg-6wt.%Zn, Mg-6wt.% Zn-2wt.%Cu and Mg-6wt.% Zn-1.5wt.%Si. The hardness increment due to fine grain size was higher at the Mg-Zn-Cu alloy system, but that due to age hardening was higher at the Mg-Zn-Si alloy system.

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An Experimental Study on the Properties of Ultra Rapid Hardening Mortar Using Magnesia-Phosphate Cement (마그네시아 인산염 시멘트를 사용한 보수용 초속경 모르타르의 특성에 관한 실험적 연구)

  • Ahn, Moo-Young;Jung, Sang-Jin
    • Journal of the Korea Institute of Building Construction
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    • v.7 no.4
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    • pp.109-116
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    • 2007
  • Building structures are generally large in size and have a long life, and the construction of such structures requires the investment of a huge amount of money and social infrastructure. Furthermore, building structures are closely related to people's life. Recently, however, the rapid development of society has been worsening air pollution, which is in turn accelerating the degradation of building structures. Thus, the safety of building structure is emerging as a critical issue. To cope with this problem, the government enacted "The Special Act on Safety Control for Infrastructure" but we need engineers' higher concern over the maintenance and reinforcement of existing structures. Recently researches are being made actively on repair mortar using ultra rapid hardening cement for recovering the performance of structures. The present study conducted an experiment on the basic physical properties of ultra rapid hardening mortar for repairing and reinforcing building structures using magnesia cement and mono-ammonium phosphate. In the experiment, we changed the water-cement ratio and carried out replacement at different ratio of MAP/MgO(%). We used retarder to have working life, and made comparative analysis through evaluating working life and fluidity and measuring strength by age.

Effect of Curing Temperature on Mechanical Properties of Polymer Mortar for Urgent Repairing (양생온도가 긴급 보수용 폴리머 모르타르의 역학적 특성에 미치는 영향)

  • Cho, Yong In;Hong, Ki Nam;Kim, Min Sung;Park, Jae Kyu
    • Journal of the Korean Society of Safety
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    • v.31 no.5
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    • pp.109-116
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    • 2016
  • This study presents the results of experiments to investigate the effect of polymer type and curing temperature on the mechanical properties of polymer mortar. Setting time of two types of polymers, hardening-delayed polymer(HDP) and rapid hardening polymer(RHP), was tested to check the working time. Additionally, flexural strength, compressive strength, and splitting tensile strength was investigated for mortars using these polymers. From these results, it was confirmed that, irrespective to curing temperature, RHP mortar at the curing age of 24h develops the similar mechanical properties to maximum properties and HDP mortar is more sensitive to the curing temperature. In addition, it should be noted that RHP mortar and HDP mortar are suitable in winter and summer, respectively.

Microstructure and Mechanical Properties of Aluminum Alloy Composites Strengthened with Alumina Particles (알루미나입자로 강화된 알루미늄합금 복합재료의 미세조직과 기계적 성질)

  • Oh, Chang-Sup;Han, Chang-Suk
    • Korean Journal of Materials Research
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    • v.23 no.3
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    • pp.199-205
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    • 2013
  • The mechanical properties and microstructures of aluminum-matrix composites fabricated by the dispersion of fine alumina particles less than $20{\mu}m$ in size into 6061 aluminum alloys are investigated in this study. In the as-quenched state, the yield stress of the composite is 40~85 MPa higher than that of the 6061 alloy. This difference is attributed to the high density of dislocations within the matrix introduced due to the difference in the thermal expansion coefficients between the matrix and the reinforcement. The difference in the yield stress between the composite and the 6061 alloy decreases with the aging time and the age-hardening curves of both materials show a similar trend. At room temperature, the strain-hardening rate of the composite is higher than that of the 6061 alloy, most likely because the distribution of reinforcements enhances the dislocation density during deformation. Both the yield stress and the strain-hardening rate of the T6-treated composite decrease as the testing temperature increases, and the rate of decrease is faster in the composite than in the 6061 alloy. Under creep conditions, the stress exponents of the T6-treated composite vary from 8.3 at 473 K to 4.8 at 623 K. These exponents are larger than those of the 6061 matrix alloy.