• Applied Biological Chemistry
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• v.39 no.2
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• pp.123-126
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• 1996

Simple and rapid method of purification of plasma proteins from bloods of slaughtered animals was developed and the proteins were applied to plywood products as a blood 히ue to utilize waste materials. Plasma protein was obtained by adding 2% trichloroacetic acid (TCA) or 0.6 N HCI as optimal concentration to the supernatant, after centrifugation of bloods. Molecular properties of beef and pig plasma proteins were examined on SDS-PAGE. Application of blood glue to plywood was quite satisfactory compared to the synthetic amino resin by tensile-shear test for the strength of adhesive bonding.

• Journal of the Korean GEO-environmental Society
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• v.10 no.7
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• pp.167-177
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• 2009

This study investigates a failure mechanism of a tunnel shotcrete lining with respect to a concentrated load due to blocky rock mass. First of all, it is carried out to survey relevant researches to shotcrete failures by literature reviews and to numerically re-investigate the failure modes of shotcrete lining given by previous researches. Through this study, the failure modes are relocated with the conditions which induce each failure mode newly proposed by this study. In addition to this, the arching shape of tunnel lining, which has not been considered in the previous research despite of inherent geometrical characteristics in tunnels, is taken into consideration in numerical investigation on lining failure in this study. As a result, it is shown that more simplified failure modes can be found on the tunnel boundary condition and the corresponding failure condition to each mode can be different from ones of the previous study due to a tunnel arching effect.

• Journal of the Korea Concrete Institute
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• v.13 no.3
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• pp.221-227
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• 2001

Both strength and stiffness of RC structures strengthened by a steel plate greatly increase and however, their ductility might not be sufficient because premature failures usually occur at the adhesive-concrete interface. In this study, Mohr-Coulomb criterion was adopted to examine the bonding failure mechanism, and the diagonal shear bonding test, the direct shear bonding test, and the flexural test on RC beams strengthened by a steel plate were carried out to measure the bonding properties. It is found from the experimental and numerical results that the cohesive strengths of epoxy-concrete interfaces are ranging from 50 kgf/㎠ to 70 kgf/㎠ when the friction angle is 45°. Bonding failure loads can be predicted by applying the bonding properties to the structural analysis of RC beams strengthened by steel plate. By considering them in the design of strengthened beams, the premature failure would be effectively prevented.

• Composites Research
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• v.20 no.5
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• pp.26-33
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• 2007

Pull-out and shear strengths of insert Joints of sandwich structure were investigated by experiment. Specimens were prepared by cocuring of nomex honeycomb core and carbon-epoxy composite face using an adhesive FM73. A total of 75 specimens with 10 different types depending on the core height and density, face thickness, and loading direction were tested. In the test under pull-out loading, although both the core height and density affect the failure loads, the effect of cell density is more serious. Dominant factor fur failure loads of the joints under shear loading is face thickness and the effect of core height is negligible. In the joint with same dimension, failure loads vary depending on the potted area of the core, particularly in the pull-out test.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.19 no.1
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• pp.146-157
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• 2018

Over the last 10 years, the number of disasters has been increasing in Korea. As a result, the need for temporary residences or shelters for disaster conditions is increasing. In this study, post-disaster refugees housing was developed using lightweight composite panels that are lighter than the materials that make up the existing shelter. To accomplish this, the structural performance of the lightweight composite panel was validated. Among the performance tests on the panels, the transverse load test was conducted according to the ASTM E 72 criteria. As a result of the experiment, when each specimen was subjected to a uniformly distributed load, the allowable load was determined according to the span. All the experiments were ended due to a loss of adhesive at the junction of the skin and core. Further analysis was conducted to calculate the shear stress when the junction was dropped. The mean shear stress at the adhesive surface of a specimen, 150 mm and 200 mm in thickness, was 0.0170MPa and 0.0156MPa, respectively. This suggests that similar values were obtained from panels of equal thickness. In addition, this stress provides a criterion of judgment that could be used to inspect the structural performance of the panels. The performance of the panel was evaluated based on the allowable load, but it may be possible to increase the strength of the lightweight composite panel by improving the joining method to avoid separation from the junction.

• Journal of Adhesion and Interface
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• v.11 no.2
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• pp.41-49
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• 2010

Furan-containing epoxide monomers (8, 9) were designed and synthesized as carbon-neutral, environment-friendly adhesion material. Bicyclic skeleton were constructed using the Diels-Alder reaction of furan and methyl acrylate, both readily accessible starting material from a biomass via bio-refinery process. After reduction of ester functionality, resulting hydroxyl moieties were coupled to epichlorohydrin to provide the epoxy-functionalized furanic monomers (8, 9). The structure of new furanic monomers was confirmed by $^1H$ and $^{13}C$ NMR spectroscopy. As UV-curable monomers, basic properties such as UV curing time and the extent of UV curing were evaluated by photo DSC. Photo-curing shrinkages were measured by linear variable differential transformer transducer (LVDT) and the effect of molecular structure on shrinkage was considered. In addition, new synthetic compounds showed the shear strength over 3 MPa when they were photo-cured between polycarbonate plates, which indicates these compounds are feasible to use as photo-curable adhesive materials.

• The Journal of Korean Academy of Prosthodontics
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• v.46 no.5
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• pp.511-519
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• 2008

Statement of problem: An incompatibility between the initiator systems of self-curing composite resins and light-curing adhesives was supposed recently. Purpose: The purpose of the study was to evaluate the influence of activators for self/dual bonding on dentin shear bonding strengths. Material and methods: Fifty human molars were divided into 5 groups. A flat dentin surface was created for each tooth. A self-curing composite resin (Luxacore) was bonded with the following adhesives (n = 10); One-Step, Prime&Bond NT, AdheSE, Prime&Bond NT and AdheSE were also used in combination with activators. Shear bond strengths were measured after 24 hours of water storage. The specimens were loaded in shear in the Instron until failure at a 1 mm/min crosshead speed. Data were compared using one-way ANOVA and Tukey HSD test (${\alpha}$= 0.05). Results: The dentin adhesive systems in order of decreasing median bond strength were One-Step > Prime&Bond NT with activator, AdheSE with activator > Prime&Bond NT, AdheSE. Among adhesives, One-Step had the highest bond strength. Prime&Bond NT with activator had higher bond strengths than Prime&Bond NT that was used alone, and so was AdheSE. Conclusion: Shear bond strengths were increased in Prime&Bond NT and AdheSE when these were used with activators comparing used without activators. But using activators was not effective clinically comparing One-Step.

• The korean journal of orthodontics
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• v.39 no.4
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• pp.225-233
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• 2009

Objective: The purpose of this study was to investigate the effect of thermocycling and type of porcelain restoration on shear bond strength (SBS) and mode of failure of monocrystalline ceramic brackets. Methods: A total of 60 porcelain discs were made and divided into three equal groups as follows: Ceramco 3, IPS Empress II, Zi-ceram/Vintage ZR. ceramic brackets were bonded to the prepared porcelain surfaces in the same manner. Each group was divided randomly into two subgroups: thermocycled group and non-thermocycled group (control). All samples were tested in shear mode on an universal testing machine. Results: SBS of the non-thermocycled group was clinically acceptable (Ceramco 3: $7.06\;{\pm}\;1.76\;MPa$, IPS Empress II: $7.55\;{\pm}\;2.38\;MPa$, Zi-ceram/Vintage ZR: $7.19\;{\pm}\;1.38\;MPa$). But, SBS of the thermocycled group was significantly reduced (Ceramco 3: $4.88\;{\pm}\;1.00\;MPa$, IPS Empress II: $5.46\;{\pm}\;1.35\;MPa$, Zi-ceram/Vintage ZR: $4.84\;{\pm}\;1.01\;MPa$, p < 0.05). There was no difference between the shear bond strength by type of porcelain restoration. All bonding failure occurred between bracket base and adhesive, except for 2 samples. Conclusions: The results of this study suggest that the type of porcelain restoration did not affect SBS, but thermocycling weakened SBS. Therefore, the effect of thermocycling should be considered when using ceramic brackets in practice.

• Journal of the korean academy of Pediatric Dentistry
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• v.30 no.1
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• pp.54-60
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• 2003

This study evaluated the influence of chemomechanical caries removal agent $Carisolv^{TM}$(MediTeam, Sweden) for composite resin adhesion to sound human permanent and primary dentin. The buccal/labial surfaces of 80 permanent molars and 80 primary incisors were used. Four types of adhesives and one composite resin were used; AQ Bond(Sun Medical, Japan), Clearfil SE Bond(Kuraray, Japan), Single Bond(3M, USA), Scotchbond Multi-Purpose(3M, USA) and Z100(3M, USA). One drop of $Carisolv^{TM}$(MediTeam, Sweden) was pretreated on the dentin for 0 second(control) and 60 seconds. The specimens were thermocycled for 1,000 times in baths kept 5 degrees C and 55 degrees C with a 30 seconds dwell time. Shear bond strengths were tested and the data was statistically analyzed using one-way ANOVA with subsequent post hoc Scheffe test at p<0.05. $Carisolv^{TM}$ treatment significantly decreased the shear bond strength. Shear bond strength of permanent dentin was significantly higher than that of primary dentin. Clearfil SE Bond treatment groups showed the highest shear bond strength and AQ Bond treatment groups showed the lowest shear bond strength.

• Journal of dental hygiene science
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• v.14 no.1
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• pp.29-34
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• 2014

The purpose of this study was to evaluate the influence of low temperature degradation (LTD) on the bonding strength of yttria-stabilized tetragonal zirconia polycrystal (Y-TZP). The push-shear bond test method was used to investigate the core-veneer bonding strength of industrially manufactured Y-TZP core ceramic and manufacturer recommended veneering ceramic. Four groups from ceramic-zirconia specimens (n=28; n=7 per group) were assigned into four experimental aging conditions, namely storage in an autoclave at $134^{\circ}C$ for 0, 3, 5, 10 hours. Bonding strength was obtained using a universal testing machine with crosshead speed 0.5 mm/min. Data were statistically analyzed using one-way ANOVA and Tukey's test (${\alpha}=0.05$). In bonding strength test, the group which was treated with LTD showed lower bonding strength than no treated group. The ceramic-zirconia bonding strength was affected by LTD (p<0.05). Digital microscope examination of the fracture surface showed mixed failures with adhesive and cohesive types in LTD with treated Y-TZP groups.