• 제목/요약/키워드: Adhesive layer

검색결과 544건 처리시간 0.023초

Surface Preparation and Activation Only by Abrasion and Its Effect on Adhesion Strength

  • Ali Gursel;Salih Yildiz
    • 접착 및 계면
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    • 제23권4호
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    • pp.101-107
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    • 2022
  • Adhesive joints have many advantages such as weight savings, corrosion and fatigue resistance and now developed even withstand of high impact and dynamic loads. However, an adhesion has cumbersome and complicated surface preparation processes. The surface preparation step is critical in adhesive joint manufacturing in order to obtain the prescribed strength for adhesive joints. In this study, it was attempted to simplify and reduce the number of surface preparation steps, and abrasion and rapid adhesive application (ARAA) process is developed for an alternative solution. The abrasion processes are performed only for creating surface roughness in standard procedures (SP), although the abrasion processes cause surface activation itself. The results showed that there is no need the long procedures in laboratory or chemical agents for adhesion. After the abrasion process, the attracted and highly reactive fresh surface layer obtained, and its effect on bonding success is observed and analyzed in this research, in light of the essential physic and adhesion theories. Al 6061 aluminum adherends and epoxy-based adhesives were chosen for bonding processes, which is mostly used in light vehicle parts. The adherends were cleaned, treated and activated only with abrasion, and after the adhesive application the specimens were tested under quasi-static loading. The satisfied ARAA results were compared with that of the specimens fabricated by the standard procedure (SP) of adhesion processes of high impact loads.

접착층에서 반사된 초음파 신호의 가시도 개선 (Visibility Enhancement of the Ultrasonic Signal Reflected from Adhesive Layers)

  • 신진섭;이정일
    • 한국인터넷방송통신학회논문지
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    • 제8권6호
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    • pp.153-157
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    • 2008
  • 최근 산업사회에서 널리 쓰이는 전자소자들은 다층구조로 제작되고 있는 실정이며 이러한 소자의 보이지 않는 층에 대한 해석은 비파괴 검사에서 중요한 일이다. 따라서 본 논문에서는 접착층이 존재하는 다층구조물에 초음파를 입사시켰을 때 반사되는 신호를 디지털 신호처리하여 가시도를 개선하였다. 이를 위하여 다층구조물에서 반사된 신호를 전력 켑스트럼 처리하여 각층에서 나타난 첫 번째 피크와 두 번째 피크를 구할 수 있었다. 실험을 위하여 일정한 두께를 갖는 에폭시층이 존재하는 다층구조물을 형성하였고 초음파 펄스-에코 방법에 의하여 얻어진 반사신호의 가시도를 개선하기 위해 전력 켑스트럼 처리하였다.

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Influence of the presence of defects on the stresses shear distribution in the adhesive layer for the single-lap bonded joint

  • Benchiha, Aicha;Madani, Kouider
    • Structural Engineering and Mechanics
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    • 제53권5호
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    • pp.1017-1030
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    • 2015
  • In this study, the finite element method was used to analyze the distribution of the adhesive shear stresses in the single-lap bonded joint of two plates 2024-T3 aluminum with and without defects. The effects of the adhesive properties (shear modulus, the thickness and the length of the adhesive were highlighted. The results prove that the shear stresses are located on the free edges of the adhesively bonding region, and reach maximum values near the defect, because the concentration of high stress occurs near this area.

복합재 연소관의 쐐기형 체결부 구조 해석 (The Structural Analysis of Wedge Joint in Composite Motor Case)

  • 황태경;도영대;김유준
    • 한국추진공학회지
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    • 제4권3호
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    • pp.64-73
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    • 2000
  • 본 체결부는 필라멘트 와인딩으로 제작된 연소관, 복합재 쐐기 그리고 알루미늄 내부 링으로 구성된다. 여기서 연소관은 헬리컬 층과 후프 층으로 이루어져 있다. 이러한 복합재 연소관의 성능 향상을 위해 체결부의 설계 변수에 따른 유한 요소 응력 해석이 수행되었다. 이때 접착 층을 난-소성 거동 재질로, 쐐기부와 알루미늄 링간의 접촉 상태는 ABAQUS의 접촉 표면 요소로 모사 되었다. 또한 해석 결과의 정확성을 입증하기 위해 내압에 의한 체결부 밀림 변위와 연소관 몸체의 원주 방향 변형도를 수압 시험과 비교하였다. 쐐기와 알루미늄 링간의 완벽 접착은 쐐기와 연소관간의 접착 층에 높은 전단 변형을 발생시켜 체결부 조기 파괴의 원인이 된다. 쐐기와 알루미늄 링간의 미 접착은 쐐기와 연소관사이의 접착 층 전단 응력을 감소시키는 반면 내부 알루미늄 링의 미끄러짐 거동으로 체결부 복합재의 반경 방향 변형을 증가시켜 파괴를 유발하였다. 그러나 쐐기부와 알루미늄 링간의 미접착 상태에서, 원주 방향 와인딩으로 체결부 지점을 보강한 경우, 알루미늄 링의 미끌어짐이 억제되어 체결부 지점의 복합재 원주 방향 변형값이 감소했다.

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Ply-lam CLT의 합판 접합방식에 따른 휨 성능 평가 (Evaluation of Flexural Performance According to the Plywood Bonding Method of Ply-Lam CLT)

  • CHOI, Gyu Woong;YANG, Seung Min;LEE, Hyun Jae;KIM, Jun Ho;CHOI, Kwang Hyeon;KANG, Seog Goo
    • Journal of the Korean Wood Science and Technology
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    • 제49권2호
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    • pp.107-121
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    • 2021
  • 본 연구에서는 층재 수종과 길이방향의 합판 접합방식과 접합부의 접착제 도포 여부에 따른 휨 성능 및 파괴 양상 분석을 통하여 합판을 코어로 사용한 CLT에 적합한 합판의 접합 방식을 최적화 하고자 하였다. 더글라스 퍼 층재의 경우 길이방향 접합에 의해 휨탄성계수 약 11.5% 감소, 휨강도는 접착제 도포 및 접합방식에 따라 증가 또는 감소하였다. 접착제 미도포 butt joint, 접착제 도포 half lap joint, butt joint 조건이 최적조건으로 도출 되었다. 낙엽송 층재의 경우 길이방향 접합에 의해 휨강도는 약 15%, 휨탄성계수는 약 40% 감소하였으며 접합방식에 따른 차이를 나타내지 않았다. half lab joint와 tongue & groove joint 사용 시 합판 층의 접합부에서 휨에 파괴를 1차적으로 방지해줌으로써 중층의 층재로 전달되는 하중을 감소시켜 주는 것으로 판단된다. 본 연구 결과를 통해 Ply-lam CLT 제조과정에서 낙엽송 층재를 사용하는 경우 접합방법에 따른 차이를 나타내지 않았으며 더글라스퍼 층재를 사용할 경우 butt joint와 half lap 접합 방식이 적합할 것으로 판단된다.

Effect of irrigation protocols on smear layer removal, bond strength and nanoleakage of fiber posts using a self-adhesive resin cement

  • Rodrigo Stadler Alessi;Renata Terumi Jitumori ;Bruna Fortes Bittencourt;Giovana Mongruel Gomes ;Joao Carlos Gomes
    • Restorative Dentistry and Endodontics
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    • 제48권3호
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    • pp.28.1-28.13
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    • 2023
  • Objectives: This study aimed to investigate the effect of the application method of 2% chlorhexidine (CHX) and its influence on the adhesion of fiberglass posts cemented with a self-adhesive resin cement. Materials and Methods: Sixty human mandibular premolars were endodontically treated and divided into 5 groups (n = 12), according to the canal irrigant and its application method: 2 groups with conventional syringe irrigation (CSI)-2.5% sodium hypochlorite (NaOCl) (control) and 2% CHX- and 3 groups with 2% CHX irrigation/activation-by passive ultrasonic irrigation (PUI), Easy Clean file, and XP-Endo Finisher file. Two roots per group were evaluated for smear layer (SL) removal by scanning electron microscopy. For other roots, fiber posts were luted using a self-adhesive resin cement. The roots were sectioned into 6 slices for push-out bond strength (BS) (7/group) and nanoleakage (NL) (3/group). Data from SL removal were submitted to Kruskal-Wallis and Student-Newman-Keuls tests (α = 0.05). Data from BS and NL were evaluated by 2-way analysis of variance and Tukey's test (α = 0.05). Results: For SL removal and BS, the CHX irrigation/activation promoted better values than CSI with CHX (p < 0.05), but it was not significantly different from CSI with NaOCl (p > 0.05). For NL, the lowest values were obtained by the chlorhexidine irrigation/activation groups (p < 0.05). Conclusions: Active 2% CHX irrigation can be used to improve the post space cleaning and adhesion before fiber post cementation with self-adhesive resin cements.

실험적 접착레진의 단량체 조성비에 따른 중합률 및 전단결합강도 변화에 관한 연구 (CHANGES OF THE DEGREE OF CONVERSION AND SHEAR BOND STRENGTH ACCORDING TO THE MONOMER RATIO OF EXPERIMENTAL BONDING RESINS)

  • 문은재;김병현;조병훈;권혁춘
    • Restorative Dentistry and Endodontics
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    • 제24권1호
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    • pp.26-39
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    • 1999
  • Bis-GMA, the representative monomer of bonding resin, contributes to the rigidity of bonding layer. Hydrophilic monomer contributes to the permeability into dentin substrates while weaken the bonding layer due to its small molecular weight. The degree of conversion also contributes to the ultimate strength of the bonding layer. This study was performed for the correlation analysis of monomer ratio and dentin bonding strength via degree of conversion. 7 experimental bonding resins were prepared with Bis-GMA, ratio from 20% to 80% by 10% increment, and hydrophilic HEMA monomer. Their degree of conversion and shear bond strength to dentin were compared with Scotchbond Multi-Purpose adhesive, and the fractured surfaces were examined microscopically. The results were as follows; 1. The degree of conversion increased when, the ratio of Bis-GMA increased from 20% to 70%, whereas it decreased when the ratio of Bis-GMA was 80%. 2. Shear bond strengths of the experimental bonding resins of 80%, 70%, 60% ratio of Bis-GMA were significantly higher than those of the experimental bonding resin of 50% ratio of Bis-GMA and Scotchbond Multi-Purpose adhesive. Lower shear bond strengths were obtained with the experimental bonding resins of 40%, 30%, 20% ratio of Bis-GMA (p<0.05). 3. Adhesive fractures were associated with the bonding resins of the lower bond strength, while cohesive fractures within the bonding resin layer were associated with the bonding resins of higher bond strength. Bonding resins with shear bond strength higher than 18MPa showed some cohesive fractures within the composite resin or within the dentin. 4. Correlations between Bis-GMA ratio and the degree of conversion (r=0.826), between Bis-GMA ratio and shear bond strength (r=0.853), and between the degree of conversion and shear bond strength (r=0.786) were significant (p<0.05).

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국소치료용 구강점막패취의 제제설계 및 약제학적 특성 (Formulation and Pharmaceutical Properties of Local Mucoadhesive-Patch Preparation)

  • 이계주;서현주;이덕근;박종범;신광현;황성주
    • 약학회지
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    • 제42권2호
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    • pp.187-195
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    • 1998
  • In order to ameliorate disadvantages of buccal ointments and mucoadhesive tablets used for the treatment of aphthosis, a thin mucoadhesive patch containing triamcinolone acetoni de was designed and evaluated for the pharmaceutical properties. The adhesive gel layer consisting of Noveon AA-1, hydroxypropylcellulose-M and ethylcellulose N 100, and the protective gel layer of ethylcellulose N 100, Eudragit RSPO and castor oil have been formulated and various properties such as viscosity of drug gel layer, thickness, in vitro adhesion time, adhesive strength, surface pH, content uniformity and drug release are tested. The mean viscosity of drug-containing gel layer was found to increase with increasing amount of Noveon OAA-1 or hydroxypropylcellulose-M. The optimum formulation showed the thickness of 171 ${\mu}$m, surface pH of 4.6, in vitro adhesion time of 8 hours and adhesive strength of 272.7g/sheet. The drug content of each patch was relatively homogeneous with the value of 273${\pm}$6.77g. Drug release study showed that compared to mucoadhesive tablet, the patch showed a faster drug release. Drug release was delayed by hydroxypropylcellulose-M, but not by ethylcellulose N 100. The patches prepared were nonirritant and the muco adhesion was better than the commercial product (AftachR) on the market. Based on these results, this mucoadhesive patch is expected to be an effective dosage form for the treatment of aphthosis.

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이중절연 자기융착테이프 제조기술 (Manufacturing technology of two-layer self bonding insulating tape)

  • 조용석;이철호;심대섭
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.890-893
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    • 2001
  • Two-layer self bonding insulating tape consists of butyl rubber(IIR ; Isobutylene-isoprene rubber) adhesive layer and polyethylene protective film. Butyl rubber have inherent characteristics such as resistance to corrosion and water, low temperature flexibility, excellent electrical insulating properties also resistance to environmental effect such as ozone and ultraviolet. Polyethylene film was used for the purpose of good insulating properties and resistance to ozone and ultraviolet. The tape was manufactured using extrusion and calender method.

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응집영역모델을 이용한 섬유금속적층판 접착층의 모드 I, II 파괴 거동 물성평가 (Evaluation of Fracture Behavior of Adhesive Layer in Fiber Metal Laminates using Cohesive Zone Models)

  • 이병언;박으뜸;고대철;강범수;송우진
    • Composites Research
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    • 제29권2호
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    • pp.45-52
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    • 2016
  • 섬유금속적층판과 같은 하이브리드 소재는 여러 방향의 하중에 의한 접착층의 파괴로 인해 층간분리가 발생할 수 있다. 모든 하중은 수직 방향의 응력과 면내 두 방향의 전단 응력으로 분해할 수 있으며, 이러한 하중은 접착층의 모드 I, II, III 파괴를 일으킨다. 따라서 하중에 의한 층간분리 현상을 예측하기 위해, 접착층의 모드별 임계 에너지 해방률을 도출하는 것이 중요하다. 본 연구에서는 접착층의 모드 I 임계 에너지 해방률을 측정하기 위해 double cantilever beam 시험을 수행하였으며, 모드 II 임계 에너지 해방률을 측정하기 위해 end-notched flexure 시험을 수행하였다. 또한, 실험으로부터 도출한 임계 에너지 해방률을 ABAQUS의 응집영역모델에 적용하여 유한요소해석을 수행하였으며, 실제 실험 결과와의 비교를 통해 층간분리 현상에 대한 수치해석 기법 적용의 유효성을 입증하였다.