• Korean Journal of Materials Research
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• v.27 no.7
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• pp.386-391
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• 2017

Using a customized diffusion bonder, we executed diffusion bonding for ring shaped white gold and red gold samples (inner, outer diameter, and thickness were 15.7, 18.7, and 3.0 mm, respectively) at a temperature of $780^{\circ}C$ and applied pressure of 2300 N in a vacuum of $5{\times}10^{-2}$ torr for 180 seconds. Optical microscopy, field emission scanning electron microscopy (FE-SEM), and energy-dispersive X-ray spectroscopy (EDS) were used to investigate the microstructure and compositional changes. The mechanical properties were confirmed by Vickers hardness and shear strength tests. Optical microscopy and FE-SEM confirmed the uniform bonding interface, which was without defects such as micro pores. EDS mapping analysis confirmed that each gold alloy was 14K with the intended composition; Ni and Cu was included as coloring metals in the white and red gold alloys, respectively. The effective diffusion coefficient was estimated based on EDS line scanning. Individual values of Ni and Cu were $5.0{\times}10^{-8}cm^2/s$ and $8.9{\times}10^{-8}cm^2/s$, respectively. These values were as large as those of the melting points due to the accelerated diffusion in this customized diffusion bonder. Vickers hardness results showed that the hardness values of white gold and red gold were 127.83 and 103.04, respectively, due to solid solution strengthening. In addition, the value at the interface indicated no formation of intermetallic compound around the bonding interface. From the shear strength test, the sample was found not to be destroyed at up to 100,000 gf due to the high bonding strength. Therefore, these results confirm the successful diffusion bonding of 14K white-red golds with a diffusion bonder at a low temperature of $780^{\circ}C$ and a short processing time of 180 seconds.

• Journal of the Korean Wood Science and Technology
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• v.22 no.4
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• pp.13-18
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• 1994

Sapwood samples of pitch pine were treated with disodium octaborate alone by dip-diffusion, or in combination with water-repellent preservative(WRP) and methyl metacrylate(MMA). Treated samples were subjected to an accelerated leaching test for determining the improvement of leaching resistance and to soft rot and mold tests for evaluating the increase in bioefficacy, due to the addition of WRP and MMA applied as a second treatment. The addition of WRP and MMA retarded leaching of boron to some extent from treated samples and this retardation can be explained by improved water repellency of WRP and MMA treated samples. Borate /WRP and borate /MMA systems will not qualify borate treated wood for ground and fresh water contact use but may improve performance of borate treated wood in above-ground applications not subjected to continuous wetting conditions. Bioefficacy against soft rot fungi and mold fungi was improved by a second treatment with WRP. However, improvement in the performance of borate /MMA systems was not observed. Considering improvement in both resistance of leaching and bioefficacy against micro fungi by the treatment of WRP and MMA, simultaneously, the dual treatment of borate treated wood by MMA containing co-biocides might be believed as an ideal treatment system.

• Nuclear Engineering and Technology
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• v.27 no.6
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• pp.825-832
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• 1995

The effect of loading variables and temperature on fatigue crack growth rate in SA508 Cl.3 nuclear pressure vessel steel was investigated in air environment Crack growth rate tests on compact tension specimen of thickness 12mm were conducted by using sinusoidal waveform. The crack length was monitored by compliance method. Test conditions were at 0.1 and 0.5 of load ratio, at 1 and 10 Hz of loading frequency, and at room temperature to 40$0^{\circ}C$. At the lower temperatures, the fatigue crack propagation was not affected by the frequency and temperature, while at the higher temperatures above 12$0^{\circ}C$, fatigue crack growth rate increased with decreasing loading frequency and increasing temperature. This accelerated fatigue crack propagation was associated with the increase of oxidation rate at the ahead of crack tip. Fatigue crack growth rate increased with in-creasing the load ratio. The effect of load ratio was more significant at the lower temperature, while the dependence on load ratio decreased with increasing temperature. The sensitivity of load ratio to temperature can be explained by crack closure with the oxidation process.

• Journal of the Korean Ceramic Society
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• v.49 no.6
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• pp.608-613
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• 2012

We investigated the property changes of MgO powders sintered at temperatures ranging from $700^{\circ}C$ to $1900^{\circ}C$ for 5minutes at a pressure of 2.7 GPa for a high-pressure high-temperature(HPHT) diamond synthesis process. The physical properties of the sintered MgO powders were characterized by optical microscopy, field emission scanning electron microscopy (FE-SEM), Vickers hardness tests, and by the apparent density, and X-ray diffractometry. An optical micro-analysis showed that white MgO powders became black after sintering due to carbon contamination from the graphite heat source. FE-SEM revealed the growth in the grain size of the MgO powders from $0.3{\mu}m$ to $50{\mu}m$ after sintering at $1700^{\circ}C$. The hardness and apparent density increased to $1800^{\circ}C$ while the samples were dedensified at $1900^{\circ}C$ due to the growth of isolated pores. According to the XRD analysis, no phase transformation occurred in the MgO powders. These results suggest that HPHT-sintered MgO powders can show an accelerated sintering process characterized by grain neck growth, pore connections, isolated pore growth and dedensification in 5 minutes, while these processes with the conventional sintering process take at least 5 hours.

• Journal of Biosystems Engineering
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• v.34 no.2
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• pp.71-76
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• 2009

This study was conducted to investigate the load acting on a tractor engine when it delivers the maximum power at drawbar. The results of the drawbar tests on the 5 locally-made and 14 imported tractors conducted at NIAE in 2004, and the 15 tractors tested at OECD test stations in foreign countries were analyzed and presented by the torque load ratio, defined as a ratio of the engine torque load caused by drawbar pull to its full-load capacity, as a function of pull speed. The NIAE test results showed that the torque load ratio increased from 20 to 80% with pull speed less than 5 km/h. At speeds faster than 5 km/h, it was 80${\sim}$110% regardless of the pull speed. However, the OECD test results showed that the torque load ratio was evaluated mostly to be 70${\sim}$90% in the entire pull speed range. The same trend was also shown for the maximum drawbar load. The difference in the torque load ratio may be attributable to bias-ply tires for locally-made and some imported tractors. It is also suggested that the input torque load may be increased safely up to 120% of the full load capacity of the tractor engine for an accelerated life test of tractor transmissions.

• Journal of Electrical Engineering and Technology
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• v.9 no.5
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• pp.1686-1693
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• 2014

In this paper, oil-paper samples composed of transformer windings were used to investigate the insulation degradation process subjected to partial discharge (PD), with artificial defects inside to simulate the PD induced insulation degradation. To determine appropriate test voltages, the breakdown time obtained through a group of accelerated electrical degradation tests under high voltages was firstly fitted by two-parameter Weibull model to acquire the average breakdown time, which was then applied to establish the inverse power law life model to choose advisable test voltages. During the electrical degradation process, PD signals were synchronously detected by an ultra-high frequency (UHF) sensor from inception to breakdown. For PD analysis, the whole degradation process was divided into ten stages, and chaos theory was introduced to analyze the variation of three chaotic parameters with the development of electrical degradation, namely the largest Lyapunov exponent, correlation dimension and Komogorov entropy of PD amplitude time series. It is shown that deterministic chaos of PD is confirmed during the oil-paper degradation process, and the obtained results provide a new effective tool for the diagnosis of degradation of oil-paper insulation subjected to PD.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.5
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• pp.3633-3642
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• 2015

Single-base propellants contain a single energetic component: nitrocellulose. Accurate predictions of propellant shelf-life should result in cost savings in terms of human and material resources. This study derived an optimized kinetic model reaction order that described stabilizer consumption and estimated propellant shelf-life. High temperature accelerated aging tests gave an optimum reaction order value of 1.15481, from which the minimum standard error of a linear regression estimate of 16.284 was obtained. At normal storage temperature of $21-30^{\circ}C$, propellants should have a safe shelf-life of 140 years, and a minimum of 35 years. It is necessary to consider the temperature range in ammunition storage areas to predict propellant shelf-life more accurately.

• Journal of the Korea institute for structural maintenance and inspection
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• v.20 no.2
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• pp.10-17
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• 2016

Steel corrosion is a very significant problem both to durability and structural safety since reinforcement has to support loads in tensile region in RC(Reinforced Concrete) member. In the paper, newly invented FRP Hybrid Bar and normal steel are embedded in RC beam member, and ICM (Impressed Current Method) is adopted for corrosion acceleration. Utilizing the previous theory of Faraday's Law, corrosion amount is calculated and flexural tests are performed for RC beam with FRP Hybrid Bar and steel, respectively. Corrosion amount level of 4.9~7.8% is measured in normal RC member and the related reduction of flexural capacity is measured to be -25.4~-50.8%, however there are no significant reduction of flexural capacity and corrosion initiation in RC samples with FRP Hybrid Bar due to high resistance of epoxy-coated steel to corrosion initiation. In the accelerated corrosion test, excellent performance of anti-corrosion and bonding with concrete are evaluated but durability evaluation through long-term submerged test is required for actual utilization.

• Transactions on Electrical and Electronic Materials
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• v.18 no.4
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• pp.207-210
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• 2017

The suspension arrangement of insulators provides flexibility and assists in power transmission in transmission lines. The performance of the insulator string is strongly influenced by the environmental conditions to which it is exposed, its shape and the inherent material properties of suspension-type insulators. The suspension-type insulators are mostly made from glass, porcelain and ceramic material due to their high resistivity. Irregularity in charge distribution throughout the porcelain insulator may lead to accelerated aging and electrical breakdown. A very high and steep lightning impulse voltage may also cause breakdown of suspension-type insulators. We investigated various material characteristics such as alumina addition, surface morphology, x-ray diffraction pattern and relative density of suspension porcelain insulators manufactured in 1989 (36,000 lbs.), 1995 (36,000 lbs.) and 2001 (36,000 lbs.) by the KRI Company for use in 154 kV high power transmission lines. We compared the material characteristics of these porcelain insulators with that of the top-of-the-line porcelain insulators (36,000 lbs.) manufactured by the NGK Company in 2000. These suspension-type porcelain insulators were exposed to arc and flashover tests to examine their electrical and mechanical strength. It was noted that alumina addition (17 wt.%) for K-2001 was one of the major contributors to the enhancement of the performance of the porcelain insulators and to their ability to withstand very high current generation during the arc test. The porcelain insulators manufactured during 2001 also showed the highest relative density of 95.8% as compared to the other insulators manufactured in 1989 and 1995 respectively 94.2% and 91.5%. We also discuss reports of various failure modes of suspension-type porcelain insulators.

• Journal of the Korea institute for structural maintenance and inspection
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• v.14 no.1
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• pp.78-83
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• 2010

This paper discusses the surface roughness of corroded reinforcement rebar in reinforced concrete structures focusing on the quantitative measurement technique for rebar corrosion. Reinforcement rebar was corroded using accelerated corrosion induced method and corrosion rates were 0%, 1%, 2%, 3%, 5%, and 10% of mass losses. Using 3-dimensional scanner each surface profile of reinforcement rebar was established, and surface roughness was measured. Through tests and analyses of corroded reinforcement rebar, the following topics were particularly discussed: measurement of surface roughness, relationship between area and surface roughness, relationship between surface roughness and bond performance. As a result, surface roughness of corroded rebar was found to be very effective to bond strength until 2% of corrosion rate. It was also discussed how to relate surface roughness of corroded rebar to bond strength of reinforced concrete structures.