• 제목/요약/키워드: Accelerated O3 Testing

검색결과 10건 처리시간 0.015초

고도수처리 환경에 노출된 에폭시 수지계 방수/방식재의 침식 저항성 평가에 관한 실험적 연구 (An Experimental Study on the Deteriorative Resistance of Epoxy Resin Waterproofing Phase under Advanced Water and Wastewater Treatment)

  • 오상근;장성주;김영삼;양승도
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2002년도 학술.기술논문발표회
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    • pp.59-62
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    • 2002
  • Recently, advanced system for water and wastewater treatment is introduced and operated because of water pollution and etc. One of this System makes use of O3(Ozone) for water and wastewater treatment. In airtight concrete structure, waterproofing phase as well as water are affected by strong oxidative O3 in the long-term. For this reason, material stability against O3 is examined. Consequently, the purpose of this study is to find out material stability an object of epoxy resin by way of accelerated O3 testing.

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SHS 공정으로 제조된 MoxW1-xSi2 발열체의 가속수명시험과 고장분석 (Failure Analysis and Accelerated Life Test of MoxW1-xSi2 Haters Fabricated by SHS process)

  • 이동원;이상헌;김용남;이희수;이성철;구상모;오종민
    • 전기전자학회논문지
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    • 제21권3호
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    • pp.252-255
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    • 2017
  • 고온자전합성과 후열처리 공정으로 $Mo_xW_{1-x}Si_2$ 발열체를 제조하였다. $Mo_xW_{1-x}Si_2$ 발열체의 신뢰성을 검증하기 위해 가속수명시험을 수행하였으며, 수명시간을 Minitab 프로그램으로 추정하였다. 또한, 가속수명시험 후의 $Mo_xW_{1-x}Si_2$ 발열체의 고장분석을 전기적과 구조적 특성으로부터 수행하였다. 그 결과, $Mo_xW_{1-x}Si_2$ 발열체의 지배적인 고장 유형은 발열체 내부의 크랙 형성과 $SiO_2$ 보호층의 박리임을 확인하였다.

오존 정수처리 음용수조 구조물에 사용하는 에폭시 수지 방수.방식재의 표면특성 평가 (A Study on the Surface Deterioration Evaluation of Epoxy Resin Coating as Anticorrosive Material of Concrete Water Tank Using Ozone($O_3$))

  • 오상근;강효진;곽규성
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2003년도 가을 학술발표회 논문집
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    • pp.513-518
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    • 2003
  • Recently, advanced systems for water treatment are introduced for water quality improvement. One of those systems is water treatment method using ozone($O_3$). For it has strong oxidizing energy, it is necessary to have materisl stability against $O_3$. In this paper, epoxy resin specimens using as anticorrosive material of concrete structure for drink water are used to serve as a material of deterioration evaluation. It is to be studied weight loss, surface corrosion of specimens, ingredient analysis of floating particle, a solute of chemical ingredient by way of accelerated ozone testing. As the results of experiment, specimen weight is decreased. The surface of specimen is eroded heavily and showed a loss of gloss and floating particle, and in the stability for drinking water, harmful ingredient is not detected in the water.

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가속노화에 따른 백색 연막수류탄(M8)의 화학적 구조 변화에 관한 연구 (A Study on Chemical Structure of White Smoke Grenade by Aging)

  • 박장호;조민수;김영대;이병택;장일호
    • 한국군사과학기술학회지
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    • 제14권6호
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    • pp.1186-1191
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    • 2011
  • Composition which was used as a white smoke grenade consists of Aluminium(Al), Hexachloroethane(HCE) and Zinc Oxide(ZnO), etc. there is a possibility of misfire due to long term storage and there are very few reports on the mechanism behind misfire. In this study, an experimental method known as accelerated degradation testing is used to investigate the chemical mechanism resulting in misfire. The mechanism of chemical change during long term storage was analyzed with XRD and FT-IR. Analysis results suggest that a part of HCE consisting of the white smoke grenade disappeared and the other part was combined into $ZnCl_2$, $AlCl_3$, as a recycled intermediate product under closed system.

CaO원 활성슬러지를 혼입한 시멘트 경화체 및 모르타르의 특성 (Characteristics of Cement Matrix/Mortar with CaO-based Activated-sludge)

  • 이용수;유성룡;신광호;추용식;김영엽
    • 콘크리트학회논문집
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    • 제29권4호
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    • pp.399-406
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    • 2017
  • CaO원 산업부산물은 CaO, $SO_3$$Al_2O_3$ 등으로 구성되어 있어 CaO 화합물의 원료로 사용되고 있다. 이러한 CaO원 산업부산물을 레미콘 회수수에 적용할 경우 슬러지수의 pH를 높여주어 콘크리트 분말원료의 수화 반응을 촉진 하여 콘크리트 조직을 치밀하게 하여 성능향상이 가능할 것이다. 본 연구에서는 레미콘 회수수에 CaO원 산업부산물 중 하나인 탈황석고를 혼입하여 제조된 활성슬러지의 효과를 확인하기 위하여 시멘트 경화체 및 모르타르의 특성을 분석하였다. 그 결과 시멘트 경화체의 경우 응결시간 단축 및 높은 안정성을 나타내었으며, 기기분석을 통해 수화반응이 촉진되었음을 확인할 수 있었다. 또한 활성 슬러지 제조를 위하여 CaO원으로서 사용된 탈황석고는 단위수량을 조절할 경우 작업성을 확보할 수 있을 뿐만 아니라 적절하게 혼입 될 경우 시멘트 사용량이 줄더라도 높은 강도 발현을 나타내는 것을 확인할 수 있었다.

옥외용 프라스틱 애자의 내구성과 평가 (Durability and Evaluation of Plastic Insulator for the Outdoor)

  • 조한구;강동필;한동희;김인성
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 1993년도 추계학술발표회논문집
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    • pp.97-102
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    • 1993
  • The application of epxy composite materials for the outdoor insulating systems has some significant advan-tages compared with conventional inorganic materials, that is low weight in combination with high mechanical strength, small dimensions and design versatility. The paper describes the results of high voltage investigations carried out different aging types of epoxy resin insulator and silicone grease coating. The insulators have been exposed 3000 hours to weather-o-meter and 12 months to outdoor. In this connection, the main study of paper is form the basis of develop-ment of principal technologies of epoxy composites which ard: (1)manufacturing of insulator, (2)high vol-tage testing under dry and wet condition, (3)mechani-cal properties, (4)accelerated weather-ometer test and outdoor exposed, artificial polution.

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Critical Cleaning Requirements for Flip Chip Packages

  • Bixenman, Mike;Miller, Erik
    • 한국마이크로전자및패키징학회:학술대회논문집
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    • 한국마이크로전자및패키징학회 2000년도 Proceedings of 5th International Joint Symposium on Microeletronics and Packaging
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    • pp.43-55
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    • 2000
  • In traditional electronic packages the die and the substrate are interconnected with fine wire. Wire bonding technology is limited to bond pads around the peripheral of the die. As the demand for I/O increases, there will be limitations with wire bonding technology. Flip chip technology eliminates the need for wire bonding by redistributing the bond pads over the entire surface of the die. Instead of wires, the die is attached to the substrate utilizing a direct solder connection. Although several steps and processes are eliminated when utilizing flip chip technology, there are several new problems that must be overcome. The main issue is the mismatch in the coefficient of thermal expansion (CTE) of the silicon die and the substrate. This mismatch will cause premature solder Joint failure. This issue can be compensated for by the use of an underfill material between the die and the substrate. Underfill helps to extend the working life of the device by providing environmental protection and structural integrity. Flux residues may interfere with the flow of underfill encapsulants causing gross solder voids and premature failure of the solder connection. Furthermore, flux residues may chemically react with the underfill polymer causing a change in its mechanical and thermal properties. As flip chip packages decrease in size, cleaning becomes more challenging. While package size continues to decrease, the total number of 1/0 continue to increase. As the I/O increases, the array density of the package increases and as the array density increases, the pitch decreases. If the pitch is decreasing, the standoff is also decreasing. This paper will present the keys to successful flip chip cleaning processes. Process parameters such as time, temperature, solvency, and impingement energy required for successful cleaning will be addressed. Flip chip packages will be cleaned and subjected to JEDEC level 3 testing, followed by accelerated stress testing. The devices will then be analyzed using acoustic microscopy and the results and conclusions reported.

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초고온용 발열체 (Mo1-xWx)Si2의 산화거동에 대한 연구 (Oxidation behavior of (Mo1-xWx)Si2 high-temperature heating elements)

  • 이성철;명재하;김용남;전민석;이동원;오종민;김배연
    • 한국결정성장학회지
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    • 제30권5호
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    • pp.200-207
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    • 2020
  • SHS 법으로 MoSi2 분말, (Mo1/2W1/2)Si2 분말 및 WSi2 분말을 합성하고 이 분말들을 500℃, 1,000℃, 1,200℃, 1,300℃, 1,400℃, 1,500℃ 및 1,600℃에서 열처리한 다음, 결정구조 및 열중량 변화 등을 관찰하였다. Mo-W-Si계의 silicide 분말은 500℃의 저온에서도 산화 반응이 일어나며, 저온 산화 및 분해로 생성되는 결정상은 MoO3이었다. 1,200℃ 이상에서 열처리를 한 경우에 분해반응으로 생성된 SiO2의 결정상은 상온에서 흔히 관찰되는 α-quartz가 아닌 α-cristobalite 상으로 생성되었다. W이 포함되면 저온과 고온에서 분해 반응이 더 많이 일어나는 것으로 나타났으며, 분말을 성형하여 소결한 시편의 경우에 MoSi2와 (Mo1/2W1/2)Si2는 저온이나 고온에서 1시간 열처리를 하더라도 저온산화에 의한 분해와 그에 따른 질량 변화 반응을 관찰하기 어려웠지만 WSi2는 저온 산화에 의하여 소결 자체가 어려웠다.

살균제 Tolclofos-methyl의 화학적 처리에 의한 분해 (Degradation of Fungicide Tolclofos-methyl by Chemical Treatment)

  • 신갑식;전영환;김효영;황정인;이상만;신재호;김장억
    • 한국환경농학회지
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    • 제29권4호
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    • pp.396-401
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    • 2010
  • 살균제 tolclofos-methyl은 인삼 및 인삼 경작지 토양에서 빈번히 검출되고 있어 그 안전성이 문제시되고 있다. 이에 tolclofos-methyl을 토양 slurry조건에서 여러 종류의 화학적 처리를 통하여 분해되는 정도를 조사하였다. ZVI를 처리한 경우 uZVI가 aZVI보다 tolclofos-methyl의 분해를 촉진 하였으며 uZVI와 ZVZn의 경우에는 ZVZn가 더 촉진시키는 것으로 나타났다. uZVI와 ZVZn 처리구에서는 처리량이 증가할수록 그리고 입경이 작을수록 더 잘 분해되는 것으로 나타났다. pH 4.0 이하의 산성 조건하에서 처리된 ZVI는 tolclofos-methyl의 분해를 더욱 촉진시켜 수용액에서 24시간 만에 94.4%까지 분해시켰다. Fenton 반응을 이용한 tolclofos-methyl의 분해는 iron source로 $Fe_2(SO_4)_3$가 가장 효과적이었으며, $H_2O_2$ 500 mM 처리구에서 93.5%까지 분해되었다. Sodium bisulfite를 이용한 토양 slurry 중의 tolclofos-methyl의 분해는 처리량이 증가할수록 분해가 촉진되었으며 50 mM 처리구에서 52.9%가 분해되었다.

자동차 엔진부품용 Shaft에 플라즈마 산질화기술 적용 (The Application of Plasma Nitrocarburizing and Plasma Post Oxidation Technology to the Automobile Engine Parts Shafts)

  • 전은갑;박익민;이인섭
    • 한국재료학회지
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    • 제16권11호
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    • pp.681-686
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    • 2006
  • Plasma nitrocarburising and plasma post oxidation were performed to improve the wear and corrosion resistance of S45C and SCM440 steel by a plasma ion nitriding system. Plasma nitrocarburizing was conducted for 3h at $570^{\circ}C$ in the nitrogen, hydrogen and methane atmosphere to produce the ${\varepsilon}-Fe_{2-3}$(N, C) phase. Plasma post oxidation was performed on the nitrocarburized samples with various oxygen/hydrogen ratio at constant temperature of $500^{\circ}C$ for 1 hour. The very thin magnetite ($Fe_3O_4$) layer $1-2{\mu}m$ in thickness on top of the $15{\sim}25{\mu}m$ ${\varepsilon}-Fe_{2-3}$(N, C) compound layer was obtained by plasma post oxidation. A salt spray test and electrochemical testing revealed that in the tested 5% NaCl solution, the corrosion characteristics of the nitrocarburized compound layer could be further improved by the application of the superficial magnetite layer. Throttle valve shafts were treated under optimum plasma processing conditions. Accelerated life time test results, using throttle body assembled with shaft treated by plasma nitrocarburising and post oxidation, showed that plasma nitrocarburizing and plasma post oxidation processes could be a viable technology in the very near future which can replace $Cr^{6+}$ plating.