• 제목/요약/키워드: 6sigma

검색결과 1,210건 처리시간 0.033초

산소 유량에 따라 증착된 ITO (Indium Tin Oxide)의 전기적 특성 분석

  • 김동해;손찬희;윤명수;이경애;조태훈;조이현;노준형;유진혁;최은하;조광섭;엄환섭;전부일;권기청
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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    • pp.410-410
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    • 2012
  • 투명 전도성 TCO (Transparent Conductivity Oxide)박막 중 ITO (Indium Tin Oxide) 박막은 n-type의 전도특성을 갖는 산화물로서 가시광선 영역에서의 높은 투과율, 전기 전도도, 넓은 밴드갭을 나타내기 때문에 디스플레이 및 태양전지 분야에 널리 사용 되어 지고 있다. 이 실험에서는 ITO 증착시 산소 유량의 변화에 따라 특성의 변화를 관찰하고자 실험을 진행 하였다. 실험에서 산소 유량은 0 sccm에서 12 sccm까지 변화를 주었으며, ITO는 RF 마그네트론 스퍼터를 이용하여 유리위에 증착하였다. 실험에서 인가된 RF power는 2 kW, 13.56 MHz, 공정 압력은 $4.5{\times}10^{-6}torr$에서 진행하였다. 유리와 타겟 사이의 거리는 200 mm로 고정하였으며, 온도는 상온에서 공정을 진행하였다. 증착된 ITO의 전기전도도(${\sigma}$)는 3 sccm까지는 증가하는 경향을 보이다가 그 이후부터는 감소하는 것을 확인 할 수 있었다. 투과율과 이차전자방출계수의 결과 또한 전기전도도와 유사한 경향성을 보여 주었다. 이를 통해 3 sccm의 산소 유량으로 증착된 ITO의 전기적 특성이 가장 좋은 것으로 확인이 되었다.

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WASHINGTON CCD PHOTOMETRY OF THE OLD OPEN CLUSTER NGC 1245

  • WEE SUN-OK;LEE MYUNG GYOON
    • 천문학회지
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    • 제29권2호
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    • pp.181-194
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    • 1996
  • We present a study of the metallicity of the old open cluster NGC 1245 , based on the Washington CCD photometry obtained using the 0.6 m telescope at the Sobaeksan Observatory, Korea. NGC 1245 has been known to be a unique cluster among the known open clusters in the sense that the previous metallicity estimates for this cluster are much larger $(by\;\sigma)$ than the value expected from the radial metallicity gradient of the old open clusters in Our galaxy. We have estimated the metallicity of the cluster red giants using the four color-color diagrams, obtaining a value for the mean metallicity of $[Fe/H] = -0.04\pm0.05$ dex. The total error including the error of the metallicity calibration, 0.15 dex, is 0.16 dex. The metallicity estimate of NGC 1245 we have obtained in this study is smaller than previous estimates, and is consistent with the radial metallicity gradient of the old open clusters, showing that the mean metallicity of NGC 1245 is not abnormally high. The reddening, distance, and age of the cluster have also been derived using the isochrones based on the convective overshooting models: the reddening $E(B-V) = 0.28\pm0.03$; the distance $d = 2.5\pm0.2 kpc$ (the corresponding galactocentric distance is RGC = 10.7 kpc, and the distance from the galactic plane is z = -0.4 kpc); and the age $t = 1.1\pm0.1 Gyrs$.

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Investigation of Lattice Effects in Perovskites by $O-isotope^{18}$ Exchange

  • Itoh, Mitsuru;Mahesh, Rajappan;Wang, Ruiping
    • The Korean Journal of Ceramics
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    • 제6권3호
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    • pp.309-314
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    • 2000
  • In the present study, preliminary experimental results of the change in the properties of perovskite-type oxides caused by the $^{18}O$- exchange have been reported. Two systems were selected for the exchange, (1) $ATiO_3$(A=Ca,Sr,Ba) and (2) manganese perovskite. The dielectric properties of isotope-exchanged $SrTi^{18}O_3$showed a drastic change from a quantum paraelectricity below 3K to ferroelectric-like behavior with a peak at 23K and an enhanced dielectric constant, 35000 at the peak. On the contrary, the $T_c$ for $BaTiO_3$was found to increase by 0.9K. The observed isotope shift of $T_c$ as well as $T_co$ for the manganese perovskites is correlated with the key parameters controlling the lattice such as $Mn^{3+}$ content, average ionic radius of the A-site cation <$r_A$> ad A-site ionic disorder $\sigma^2$.

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Autonomous Real-time Relative Navigation for Formation Flying Satellites

  • Shim, Sun-Hwa;Park, Sang-Young;Choi, Kyu-Hong
    • Journal of Astronomy and Space Sciences
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    • 제26권1호
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    • pp.59-74
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    • 2009
  • Relative navigation system is presented using GPS measurements from a single-channel global positioning system (GPS) simulator. The objective of this study is to provide the real-time inter-satellite relative positions as well as absolute positions for two formation flying satellites in low earth orbit. To improve the navigation performance, the absolute states are estimated using ion-free GRAPHIC (group and phase ionospheric correction) pseudo-ranges and the relative states are determined using double differential carrier-phase data and singled-differential C/A code data based on the extended Kalman filter and the unscented Kalman filter. Furthermore, pseudo-relative dynamic model and modified relative measurement model are developed. This modified EKF method prevents non-linearity of the measurement model from degrading precision by applying linearization about absolute navigation solutions not about the priori estimates. The LAMBDA method also has been used to improve the relative navigation performance by fixing ambiguities to integers for precise relative navigation. The software-based simulation has been performed and the steady state accuracies of 1 m and 6 mm ($1{\sigma}$ of 3-dimensional difference errors) are achieved for the absolute and relative navigation using EKF for a short baseline leader/follower formation. In addition, the navigation performances are compared for the EKF and the UKF for 10 hours simulation, and relative position errors are mm-level for the two filters showing the similar trends.

제미니형 양이온 계면활성제 합성 및 Spacer 길이에 따른 물성 (Synthesis of Gemini Type Cationic Surfactants and Properties of Spacer Length)

  • 박종권;정노희
    • 한국응용과학기술학회지
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    • 제31권1호
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    • pp.1-6
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    • 2014
  • Gemini type of cationic surfactant, namely ${\alpha},{\omega}$-alkane-bis(N-lauroyloxyethyl-N,N-dimethyl)-diammonium bromide was synthesized and confirmed by FT-IR and $^1H$-NMR spectroscopy. Their inhibition effect on corrosion of mild steel in 1 M HCl solution was tested by weight loss method. Surface tensions were measured by surface tensiometer Sigma 70. Their c.m.c. values evaluated by surface tension method was $4.01{\times}10^{-5}{\sim}4.99{\times}10^{-5}mol/L$. The Krafft point of the these surfactants were < $0^{\circ}C$. The emulsifying properties of synthesized cationic gemini surfactants and sodium dodecyl sulfate (SDS), tetradecyl trimethyl ammonium bromide (TTAB) was investigated. Of these, ${\alpha},{\omega}$-alkane-bis(N-lauroyloxyethyl-N,N-dimethyl)-diammonium bromide has been confirmed as a good emulsifier. The inhibition efficiency increases by increasing cationic gemini surfactant concentration. As a result, these surfactants are expected to be applied as corrosion inhibitors.

Kinetics and Mechanism of the Benzylaminolysis of O,O-Diethyl S-Aryl Phosphorothioates in Dimethyl Sulfoxide

  • Adhikary, Keshab Kumar;Lee, Hai-Whang
    • Bulletin of the Korean Chemical Society
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    • 제32권10호
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    • pp.3587-3591
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    • 2011
  • The reactions of O,O-diethyl Z-S-aryl phosphorothioates with X-benzylamines are kinetically investigated in dimethyl sulfoxide at $85.0^{\circ}C$. The Hammett (log $k_2$ vs ${\sigma}x$) and Br$\ddot{o}$nsted [log $k_2$ vs $pK_a$(X)] plots are biphasic concave downwards for substituent X variations in the nucleophiles with a break point at X = H. The signs of the cross-interaction constants (${\rho}xz$) are positive for both the strongly and weakly basic nucleophiles. Considerably great magnitude of ${\rho}xz$ (= 6.56) value is observed with the weakly basic nucleophiles, while ${\rho}xz$ = 0.91 with the strongly basic nucleophiles. Proposed reaction mechanism is a stepwise process with a rate-limiting leaving group expulsion from the intermediate involving a backside nucleophilic attack with the strongly basic nucleophiles and a frontside attack with the weakly basic nucleophiles. The kinetic results are compared with those of the benzylaminolysis of O,O-diphenyl Z-S-aryl phosphorothioates.

Effect of Thermal History on Pitting Corrosion of High Nitrogen and Low Molybdenum Stainless Steels

  • Kim, Kwangsik;Chang, Hyunyoung;Kim, Youngsik
    • Corrosion Science and Technology
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    • 제2권2호
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    • pp.75-81
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    • 2003
  • Chromium, molybdenum. and nitrogen are very important alloying elements in stainless steels and its effect was approved in pitting resistance equivalent (PRE) equations and many experimental results. However, Cr can improve the corrosion resistance, but facilitate the formation of sigma phase. Also. Mo has the same effect in stainless steels. If Cr and Mo are added at high amount to increase the corrosion resistance of stainless steel, corrosion resistance in annealed alloys can be improved, but in case of welding or aging heat treatment. its resistance will be drastically decreased. In this work, increasing Cr and N contents but decreasing Mo than the commercial alloys made the experimental alloys. Typical alloys are 25Cr-4.5Mo-0.43N alloy, 27Cr-4.7Mo-0.4N alloy, 27Cr-5.3Mo-0.25N alloy, 32Cr-2.6Mo-0.36N alloy. After annealing and aging heat treatment, microstructures, anodic polarization test, and pitting corrosion test were performed. Annealed alloys showed $100^{\circ}C$ of CPT and aged alloys showed the different tendency depending upon Cr and Mo contents(SFI)

GPS-Based Orbit Determination for KOMPSAT-5 Satellite

  • Hwang, Yoo-La;Lee, Byoung-Sun;Kim, Young-Rok;Roh, Kyoung-Min;Jung, Ok-Chul;Kim, Hae-Dong
    • ETRI Journal
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    • 제33권4호
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    • pp.487-496
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    • 2011
  • Korea Multi-Purpose Satellite-5 (KOMPSAT-5) is the first satellite in Korea that provides 1 m resolution synthetic aperture radar (SAR) images. Precise orbit determination (POD) using a dual-frequency IGOR receiver data is performed to conduct high-resolution SAR images. We suggest orbit determination strategies based on a differential GPS technique. Double-differenced phase observations are sampled every 30 seconds. A dynamic model approach using an estimation of general empirical acceleration every 6 minutes through a batch least-squares estimator is applied. The orbit accuracy is validated using real data from GRACE and KOMPSAT-2 as well as simulated KOMPSAT-5 data. The POD results using GRACE satellite are adjusted through satellite laser ranging data and compared with publicly available reference orbit data. Operational orbit determination satisfies 5 m root sum square (RSS) in one sigma, and POD meets the orbit accuracy requirements of less than 20 cm and 0.003 cm/s RSS in position and velocity, respectively.

Study on uplift performance of stud connector in steel-concrete composite structures

  • Ju, Xiaochen;Zeng, Zhibin
    • Steel and Composite Structures
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    • 제18권5호
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    • pp.1279-1290
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    • 2015
  • The main role of studs, which act as connectors of the steel-concrete composite structures, is to ensure that the steel and the concrete work together as a whole. The studs in steel-concrete composite structures bear the shearing force in the majority of cases, but in certain locations, such as the mid-span of a simply supported composite beam, the studs bear axial uplift force. The previous studies mainly focused on the shearing performance of the stud by some experimental and theoretical effort. However, rare studies involved the uplift performance of studs. In this paper, the single stud uplift test on 10 composite specimens was performed. Meanwhile, based on the test, numerical analysis was introduced to simulate the concrete damage process due to the stud uplifted from concrete. The static ultimate bearing capacity, under which the stud connector was pulled out from the damaged reinforced concrete, is much larger than the cyclic ultimate bearing capacity, under which the weld joint between stud and steel plate fractured. According to the fatigue test results of 7 specimens, the fatigue S-N curve of the construction detail after minus 2 times standard deviation is $logN=24.011-9.171\;log{\Delta}{\sigma}$, the fatigue strength corresponding to $2{\times}10^6$ cycles is 85.33 MPa.

SiC-$Si_3 N_4$ 세라믹공구를 위한 소결시간과 조성변화의 최적화 (Optimization of the Sintering Time and Composition for SiC-$Si_3 N_4$ Ceramic Tool)

  • 김경재;박준석;이성구;권원태;김영욱
    • 한국공작기계학회논문집
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    • 제10권6호
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    • pp.78-84
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    • 2001
  • In the present study, SiCSi-$Si_3 N_4$-SiC ceramic composites that contained up to 30 wt% of dispersed SiC particles were fabricat-ed cia hot-pressing with an oxynitride glass. The microstructure, the mechanical properties and the cutting performance of resulting ceramic composites were investigated. By fixing the composition as $Si_3 N_4$-20wf%SiC, the effect of sintering time on the microstructure, the mechanical properties and the cutting performance were also investigated. The longer sir-tering time is, the bigger the grain size of SiC is. The fracture toughness(-$K_k$) of the $Si_3 N_4$-SiC ceramic composites increased with the increase of gain size, while the flexural strengthh($\sigma$) decreased. For machining SCM440, the insert with 20wt%r SiC sintered for 8 hours showed the longest tool life while the insert with 20wt% SiC sintered for 12 hours showed the longest tool life for machining gray cast iron.

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