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Age-hardening Behavior and Mechanical Properties of Cast AZ91-0.3Ca-0.2Y Alloy (AZ91-0.3Ca-0.2Y 마그네슘 합금 주조재의 시효경화 거동 및 기계적 특성)

  • H. J. Kim;J. H. Bae;Y. M. Kim;S. H. Park
    • Transactions of Materials Processing
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    • v.32 no.4
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    • pp.173-179
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    • 2023
  • In this study, the age-hardening behavior and tensile properties of a cast AZ91-0.3Ca-0.2Y (SEN9) alloy are investigated and compared with those of a commercial AZ91 alloy. Even after homogenization heat treatment, the SEN9 alloy contains numerous undissolved secondary phases, Al8Mn4Y, Al2Y, and Al2Ca, which results in a higher hardness value than the homogenized AZ91 alloy. Under aging condition at 200 ℃, both the AZ91 and SEN9 alloys exhibit the same peak-aging time of 8 h, but the peak hardness of the latter (86.8 Hv) is higher than that of the former (83.9 Hv). The precipitation behavior of Mg17Al12 phase during aging significantly differs in the two alloys. In the AZ91 alloy, the area fraction of Mg17Al12 discontinuous precipitates (DPs) increases up to ~50% as the aging time increases. In contrast, in the SEN9 alloy, the formation and growth of DPs during aging are substantially suppressed by the Ca- or Y-containing particles, which leads to the formation of only a small amount of DPs with an area fraction of ~4% after peak aging. Moreover, the size and interparticle spacing of Mg17Al12 precipitates of the peak-aged SEN9 alloy are smaller than those of the peak-aged AZ91 alloy. The homogenized AZ91 alloy exhibits a higher tensile strength than the homogenized SEN9 alloy due to the finer grains of the former. However, the peak-aged SEN9 alloy has a higher tensile elongation than the peak-aged AZ91 alloy due to the smaller amount of brittle DPs in the former.

EVALUATION OF SHEAR BEHAVIOR OF LARGE GRANULAR MATERIALS WITH DIFFERENT PARTICLE SIZES BY TRIAXIAL TEST AND NUMERICAL SIMULATION

  • Kim, Bum-Joo;Sagong, Myung
    • Proceedings of the Korean Geotechical Society Conference
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    • 2010.09c
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    • pp.55-60
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    • 2010
  • Rockfill zones in CFRD consist typically of large granular materials, usually the maximum particle size up to several meters, which makes laboratory testing to determine the mechanical properties of rockfill difficult. Commonly, the design strength of the rockfills is obtained by scaling down the original rockfill materials and performing laboratory strength tests for the reduced size materials. The objective of the present study is to investigate the effect of particle size on the shear behavior and the strength for granular materials. A series of large-scale triaxial tests was conducted on large granular materials with the maximum particle size varying from 20 to 50mm. The test results showed that overall shear behaviors were similar between the samples with different particle sizes while there were slight differences in the magnitudes of the peak shear stress between the samples. In addition, a simulation of the granular material with the max. particle size of 20mm was performed using DEM code, $PFC^{2D}$, and compared with the test results. The deviatoric stress versus strain behaviors of experimental and numerical tests were found to be matched well up to the peak stress state.

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Pulse-Sequence Analysis of Discharges in Air, Liquid and Solid Insulating Materials

  • Suwayno, Suwayno;Mizutani, Teruyoshi
    • Journal of Electrical Engineering and Technology
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    • v.1 no.4
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    • pp.528-533
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    • 2006
  • Electrical discharges may occur in gas, liquid as well as solid insulating materials. This paper describes the investigation results on the discharges in air, silicone oil and low density polyethylene (LDPE) using needle plane electrode system under AC voltage of 50 Hz. The experimental results showed that for discharge in air (corona), discharge pulses were concentrated around the peak of applied voltage at negative half cycle. For silicone oil positive as well as negative discharges were observed which concentrated around the peak of applied voltage. The positive pulse number was smaller but the magnitude was higher than that of negative discharge. Discharges in void took place at wider range of phase of applied voltage. The unbalance in pulse number and magnitude similar to that of oil discharges were observed. For electrical treeing in LDPE, the discharges were spread before the zero cross of the applied voltage up to the peak at both positive and negative half cycles. The discharge pulse sequence analysis indicated that the PD occurrence in air, oil and void were strongly affected by the magnitude of applied voltage. However, for electrical treeing it was observed that the discharge occurrence was strongly affected by the time derivative of the applied voltage (dv/dt).

RF Characterizations of Patterned CoNbZr Magnetic Thin Film on Transmission Line

  • Kim, Ki-Hyeon
    • Journal of Magnetics
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    • v.11 no.3
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    • pp.130-134
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    • 2006
  • The microwave power absorption for the patterned CoNbZr magnetic film has been investigated by coplanar waveguide method. The power absorption peaks of the patterned CoNbZr film (50 ${\mu}m$ ${\times}$ 2 mm ${\times}$ 2 ${\mu}m$), were observed at around 5.7 GHz. The observed resonance peak was in good agreement with calculated ferromagnetic resonance frequency including magnetic shape anisotropy effects. Compared with the coplanar waveguide without a magnetic film, the characteristic impedance of patterned film was shown to be increased. This resulted from the large increment of inductance up to 33 % without any significant changes of the capacitance.

Correlative Changes between Photosynthetic Activities and Chlorophyll Fluorescence in Wheat Chloroplasts Exposed to High Temperature

  • Young-Nam Hong
    • Journal of Plant Biology
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    • v.37 no.1
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    • pp.37-42
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    • 1994
  • Correlative changes between photosynthetic O2 exchange rates and room temperature Chl fluorescence were investigated in wheat (Triticum aestivum L.) chloroplasts treated with high temperature for 5 min. With increasing treatment temperature, photosynthetic O2 evolution rate mediated by PSII was decreased, showing 50% inhibition at 38$^{\circ}C$ (I50). But PSI activity measured by O2 uptake rates was stimulated as a function of increasing temperature. Dark level fluorescence (Fo)-temperature (T) analysis showed that fluorescence rising temperature (Tr), critical temperature (Tc), and peak temperature (Tp) was 38, 43, and 52$^{\circ}C$, respectively. Quenching analysis of Chl fluorescence showed that both the oxidized fraction of plastoquinone (qQ) and degree of thylakoid membrane energization (qNP) increased up to 4$0^{\circ}C$ and then declined dramatically. These results suggest that Tr is correlated with temperature showing a 50% of inhibition of photosynthesis and under mild high temperature stress, qNP is worth regarding as indicator for heat-induced damage of photosynthesis.

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테트라키스 피콜리나토류 텅그스텐(Ⅳ) 착물의 Inertness에 관한 연구

  • Jang, Ju Hwan;Ronald D. Archer
    • Journal of the Korean Chemical Society
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    • v.34 no.1
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    • pp.85-90
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    • 1990
  • The inertness of eight-coordinate tetrakis(picolinato)tungsten(IV) complex has been investigated by spectroscopic method in nonpolar solvent at 60$^{\circ}C$, 75$^{\circ}C$, 90$^{\circ}C$, 120$^{\circ}C$, and reflux condition. Until 2 days, showed the inertness whether existance of oxygen or not. After 2 days, showed the oxidation of W(IV) complex much more rapidly than substitution, which had $k_{obs}(sec^{-1}) {\varpropto} 1/[ligand]^2$. On sealing the sample under Ar gas, showed the inertness until 50 days, which had $k_{obs}(sec^{-1}) = 8.8{\times} 10^{-7}$. The$^1H$-NMR peak of $H_6$ in complex was diminished, otherwise that of free ligand was grown up. This result indicated that this complex was very inert.

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Gelatinization Properties of Starch during Steeping of Potato (감자의 수침에 따른 전분의 열 호화 특성)

  • 정난희;김경애;김성곤;서복영;전은례
    • Korean journal of food and cookery science
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    • v.14 no.3
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    • pp.213-218
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    • 1998
  • The changes in gelatinization patterns of potato were investigated while steeping in water for 7 days at 30${\pm}$1$^{\circ}C$. The transmittance of 0.1% starch suspension was increased rapidly from 60$^{\circ}C$ in raw starch and the starch steeped for 2 days, and increased rapidly from 65$^{\circ}C$ in the starch steeped for 4 and 6 days. As the steeping period increased, the transmittance was decreased at above condition. The gelatinization temperature of the starch measured by differential scanning calorimetry was increased from 62.79$^{\circ}C$ to 63.72$^{\circ}C$ as the steeping period increased. The gelatinization enthalpy reached the maximum in the starch steeped for 4 days. By amylograph, the initial gelatinization temperature was increased from 66$^{\circ}C$ to 84$^{\circ}C$ as the steeping period increased. Peak viscosity was decreased during steeping and the starch steeped for 5 days had no peak viscosity. Peak height after cooling to 50$^{\circ}C$ was increased up to the 4th day and began to decrease. As the steeping period increased, there was much loss of birefringence at higher temperature. The crystallinity by X-ray diffraction disappeared from 65$^{\circ}C$.

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Extra-Anatomic Ascending Aorta to Abdominal Aorta Bypass in Takayasu Arteritis Patients with Mid-Aortic Syndrome

  • Kim, Hak Ju;Choi, Jae-Woong;Hwang, Ho Young;Ahn, Hyuk
    • Journal of Chest Surgery
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    • v.50 no.4
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    • pp.270-274
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    • 2017
  • Background: We evaluated the operative outcomes of an extra-anatomic bypass from the ascending aorta to the abdominal aorta in patients with type II or III Takayasu arteritis (TA) with mid-aortic syndrome. Methods: From 1988 to 2014, 8 patients with type II (n=2) or III (n=6) TA underwent an ascending aorta to abdominal aorta bypass. The mean patient age was $43.5{\pm}12.2years$ and the mean peak pressure gradient between the upper and lower extremities was $54.8{\pm}39.0mm\;Hg$. The median follow-up duration was 54.4 months (range, 17.8 to 177.4 months). Results: There were no cases of operative mortality. The mean peak pressure gradient significantly decreased to $-2.4{\pm}32.3mm\;Hg$ (p=0.017 compared to the preoperative value). Late death occurred in 2 patients. The symptoms of upper extremity hypertension and claudication improved in all patients. The bypass grafts were patent at $47.1{\pm}58.9months$ in 7 patients who underwent follow-up imaging studies. Conclusion: An extra-anatomic ascending aorta to abdominal aorta bypass could be an effective treatment option for severe aortic steno-occlusive disease in patients with type II or III TA, with favorable early and long-term outcomes.

Retention and Fatigue Properties of MFS Devices using Ferroelectric $LiMbO_3$ Thin Films ($LiMbO_3$ 강유전체 박막을 이용한 MFS 디바이스의 Retention 및 Fatigue 특성)

  • 정순원;김채규;김용성;김진규;이남열;김광호;유병곤;이원재
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.17-20
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    • 1999
  • The retention and fatigue properties of ferroelectric LiNbO$_3$ thin films were studied. Metal-ferroelectric-semiconductor(MFS) devices by using rapid thermal annealed LiNbO$_3$/Si structures were successfully fabricated and demonstrated nonvolatile memory operations of the MFS devices. The I$_{D}$-V$_{G}$ characteristics of MFSFET\`s showed a hysteresis loop due to the ferroelectric nature of the LiNbO$_3$ thin film. The ferroelectric capacitors showed practically no polarization degradation up to about 10$^{10}$ switching cycles when subjected to symmetric bipolar voltage pulse (peak-to-peak 6V, 50% duty cycle) in the 500kHz. The retention properties of the LiNbO$_3$ thin films were quite good up to about 10$^{3}$ s . s .

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Evaluate the usefulness of Coincidence Summing Correction Factors for Cylinder and Extended Source Penelope Simulation (실린더 및 확장 소스 PENELOPE 시뮬레이션에 대한 동시합성보정 계수 유용성 평가)

  • Jang, Eun-Sung;Chang, Bo-Seok
    • Journal of the Korean Society of Radiology
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    • v.15 no.6
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    • pp.821-831
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    • 2021
  • In order to calibrate energy and efficiency using the PENELOPE Code, a PENELOPE simulation was performed using a volume source. Here, we want to verify peak efficiency and usefulness by performing simultaneous measurement and correction. calculate the coincident sum correction for all volumes, first subdivide the volumes of the cylinder and the four Marinelli beakers into three heights again. Therefore, the simultaneous measurement correction coefficient in three areas and the simultaneous measurement correction coefficient for the entire volume source are calculated as output. At low energies, the j value for each source volume (50-300 ml) is small and increases significantly in the high energy range. Simulation results showed good agreement within 2.5% for all source volumes except for 50 ml and 300 ml, which were up to 4%. This means that the correction for the simultaneous measurement effect during measurement is effective. In addition. Based on this, it can be confirmed that there is an advantage to improve the detection efficiency when measuring various sources and environmental samples.