• Journal of the Microelectronics and Packaging Society
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• v.19 no.1
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• pp.55-60
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• 2012

In order to develop electroless-plated Nickel Phosphate (Ni-P) as a contact material for high efficient low-cost silicon solar cells, we evaluated the effect of ambient thermal annealing on the degradation behavior of interfacial adhesion energy between electroless-plated Ni-P and silicon solar cell wafers by applying 4-point bending test method. Measured interfacial adhesion energies decreased from 14.83 to 10.83 J/$m^2$ after annealing at 300 and $600^{\circ}C$, respectively. The X-ray photoelectron spectroscopy analysis suggested that the bonding interface was degraded by environmental residual oxygen, in which the oxidation inhibit the stable formation of Ni silicide phase between electroless-plated Ni-P and silicon interface.

• The Journal of Advanced Prosthodontics
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• v.11 no.4
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• pp.202-208
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• 2019

PURPOSE. Fabrication of zirconia restorations with ideal mechanical properties in a short period is a great challenge for clinicians. The purpose of the study was to investigate the effect of heating rate on the mechanical and microstructural properties of monolithic zirconia. MATERIALS AND METHODS. Forty monolithic zirconia specimens were prepared from presintered monolithic zirconia blanks. All specimens were then assigned to 4 groups according to heating rate as Control, Group $15^{\circ}C$, Group $20^{\circ}C$, and Group $40^{\circ}C$. All groups were sintered according to heating rates with the sintering temperature of $1500^{\circ}C$, a holding time of 90 minutes and natural cooling. The phase composition was examined by XRD analysis, three-point bending test was conducted to examine the flexural strength, and Weibull analysis was conducted to determine weibull modulus and characteristic strength. Average grain sizes were determined by SEM analysis. One-way ANOVA test was performed at a significance level of 0.05. RESULTS. Only tetragonal phase characteristic peaks were determined on the surface of analyzed specimens. Differences among the average grain sizes of the groups were not statistically significant. The results of the three-point bending test revealed no significant differences among the flexural strength of the groups (P>.05). Weibull modulus of groups was ranging from 3.50 to 4.74. The highest and the lowest characteristic strength values were obtained in Group $20^{\circ}C$ and Control Group, respectively. CONCLUSION. Heating rate has no significant effect on the flexural strength of monolithic zirconia. Monolithic zirconia restorations can be produced in shorter sintering periods without affecting the flexural strength by modifying the heating rate.

• Journal of Industrial Technology
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• v.9
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• pp.43-49
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• 1989

In this study, 3-point bending test for the mode I state and 4-point shear test for the mode II state were adopted to verify the crack initiation load level through comparing the test results of the acoustic emission and the ASTM testing criteria, using Jecheon granite, as the rock sample. The major result obtained in this study is that the crack initiation load levels obtained by using ASTM testing criteria and by measuring acoustic emissions showed analogous, roughly. However in case of demanding high safety, the crack initiation load level needs to be underestimated to the level that the crack begins to deform nonlinearly.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.32 no.2A
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• pp.65-73
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• 2012

In this study, we tested structural performance of Half-Decked PSC girder which was developed for applying to long span bridge. We operated 4 point bending test with 60 m span full scale girder designed as simple bridge with hinge-roller boundary condition. Actuators were set on the both sides of girder, 5.5 m away from the center, and 4 stages of cyclic loading was applied at rate of 1 kN/sec. Through stages 1 to 4, loading and unloading 1,000 kN, 1,200 kN, 1,500 kN, and 2,000 kN were repeated and displacement, strain of concrete and steel, crack of girder were checked. From these results, the strength of girder was assessed and resilience and ductility were observed after removing the load. Since initial flexural crack occurred in the vicinity of 1,400 kN, non-linearity of load-displacement curve appeared and definite residual strain was measured at that point. The test result showed that initial cracking load was over twice the DB-24 load which means the developed girder had sufficient strength. To verify the experimental results, we numerically analyze the test and confirmed that the data were similar with results from the test above. Half-Decked PSC type of 60 m-girder developed in this study showed its adequate structural capacity through static loading test, which proved that possibility of applying the girder to actual bridges practically.

• Journal of Korean Society of Steel Construction
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• v.28 no.3
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• pp.173-183
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• 2016

Various material characteristics of HSA800 steel were examined and a quantitative criteria about the homogeneity of the strength was proposed. Whether HSA800 steel is satisfied the criteria for homogeneity of the strength or not was also examined. From the test results, the material characteristics of 1/4 point from the extreme fiber in the Z-direction satisfied the KS requirements. The excellent directional properties and impact resistance at low temperatures were also showed from the test results. HSA800 steel satisfied the criteria of homogeneity for the strength of the steel. However, it showed that some structures were banded together at 2/4 point from extreme fiber in the Z-direction from the microscopic tests and attention is needed to be paid in that point.

• Corrosion Science and Technology
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• v.23 no.2
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• pp.113-120
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• 2024

An attempt was made to apply digital image correlation (DIC) strain analysis to in-situ scanning electron microscopy (SEM) observations of bending deformation to quantify local strain distribution inside a ZnMgAl-alloy coating in deformation. Interstitial-free steel sheets were hot-dipped in a Zn-3Mg-6Al (mass%) alloy melt at 400 ℃ for 2 s. The specimens were deformed using a miniature-sized 4-point bending test machine inside the SEM chamber. The observed in situ SEM images were used for DIC strain analysis. The hot-dip ZnMgAl-alloy coating exhibited a solidification microstructure composed of a three-phase eutectic of fine Al (fcc), Zn (hcp), and Zn2Mg phases surrounding the primary solidified Al phases. The relatively coarsened Zn₂Mg phases were locally observed inside the ZnMgAl-alloy coating. The DIC strain analysis revealed that the strain was localized in the primary solidified Al phases and fine eutectic microstructure around the Zn₂Mg phase. The results indicated high deformability of the multi-phase microstructure of the ZnMgAl-alloy coating.

• Biomedical Science Letters
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• v.14 no.2
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• pp.105-113
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• 2008

The objective of this study was to evaluate the influence of surface modifications on the bonding characteristics and cytotoxicity of specific titanium porcelain bonded to milling titanium and cast titanium. Milling titanium and cast titanium samples were divided into 8 test groups. These groups are as follow: i) sandblasted with particles of different size of $220{\mu}m\;and\;50{\mu}m$, ii) different sequences of sandblasting treatment and etching treatment, iii) etched with different etching solutions, and iv) preheated or not. The surface characteristics of specimens were characterized by the test of mean roughness of surface and SEM. The bond strength of titanium-ceramic systems was measured by using three-point bending test and SEM. The results show that the mean roughness of surface of sample sandblasted with $220{\mu}m$ aluminum oxide increased and bond strength were higher than sample sandblasted with $50{\mu}m$ aluminum oxide. The mean roughness of surface decreased, but the bond strength increased when the samples sandblasted with $220{\mu}m$ aluminum oxide were preheated. The sample sandblasted with $220{\mu}m$ aluminum oxide after oxidized with occupational corrosive agent I (50% NaOH, 10% $CuSO_4{\cdot}5H_2O$) and II (35% $HNO_3$, 5% HF) showed higher bond strength than sample oxidized with 30% $HNO_3$ after sandblasted with $220{\mu}m$ aluminum oxide. Group NaCuNF220SP (milling Ti: 35.3985 MPa, casting Ti: 37.2306 MPa) which was treated with occupational corrosive agent I (50% NaOH, 10% $CuSO_4{\cdot}5H_2O$) and II (35% $HNO_3$, 5% HF), followed by sandblasting with $220{\mu}m$ aluminum oxide and preheating at $750^{\circ}C$ for 1 hour showed the highest bond strength and significant differences (P<0.05). The method for modifying surface of titanium showed excellent stability of cells.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.48 no.7
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• pp.505-511
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• 2020

The circular composite tubes have been used as a main spar of HALE-UAV(High Altitude Long Endurance-Unmanned Air Vehicle). In this paper, an analytical model is presented for the prediction of the failure load of unsymmetrically stiffened circular spar using a modified Brazier approach. This model was used to predict the moment carrying capacity of the unsymmetrically stiffened circular spar. From the results, we can know that a stiffened cap placed in the top sector of a spar increased the bending capabilities. Four point bending tests were conducted to estimate the effect of the cap on the failure load and compared with the proposed model. And numerical simulations were performed to analyze the behavior of stiffened circular spar. Comparisons of the results from the proposed model with those from experiments and numerical modes show good correlation.

• Journal of Mechanical Science and Technology
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• v.20 no.7
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• pp.1002-1011
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• 2006

In this study, we describe the conventional hot pressing (CHP) of layered $Al-B_4C$ composites and their characterization. The matrix alloy Al-5 wt.%Cu was prepared from elemental powder mixtures. The metal and B4C powders were mixed to produce either $Al-Cu-10vol.%B_4C$ or $Al-Cu-30vol.%B_4C$ combinations. Then, these powder mixtures were stacked as layers in the hot pressing die to form a two-layered composite. Hot pressing was carried out under nitrogen atmosphere to produce $30\times40\times5mm$ specimens. Microstructural features and age hardening characteristics of composites were determined by specimens cut longitudinally. The flexural strength of both layered composites and their monolithic counterparts were investigated via three point bending tests. In the case of layered specimens of both $10vol.%B_4C$ and $30vol.%B_4C$ containing layers were loaded for three-point test. The results show that a homogeneous distribution of $B_4C$ particles in the matrix alloy which is free of pores, can be obtained by CHP method. The ageing behavior of the composites was found to be influenced by the reinforced materials, i.e. higher hardness values were reached in 8 hrs for the composites than that for the matrix alloy. Flexural strength test showed that two-layered composites exhibited improved damage tolerance depending on layer arrangement. Microstructural investigation of the fracture surfaces of the bending specimens was performed by means of scanning electron microscope (SEM). While layer with lower reinforcement content exhibited large plastic deformation under loading, the other with higher reinforcement content exhibited less plastic deformation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.12
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• pp.1849-1856
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• 2010

Glass/resin/glass laminate structures are used in the automobile, biological, and display industries. The sandwich structures are used in the micro/nanoimprint process to fabricate a variety of functional components and devices in fields such as display, optics, MEMS, and bioindustry. In the process, micrometer- or nanometer-scale patterns are transferred onto the substrate using UV curing resins. The demodling process has an important impact on productivity. In this study, we investigated the fracture behavior of glass/resin/glass laminates fabricated via UV curing. We performed measurements of the adhesion force and the interfacial energy between the mold and resin materials using the four-point flexural test. The bending-test measurements and the load-displacement curves of the laminates indicate that the fracture behavior is influenced by the interfacial energy between the mold and resin and the resin thickness.