• Title/Summary/Keyword: 3D microstructures

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Effects of Sputtering Parameters on the Properties of Co/Pd Multilayered Films

  • Shin, J. N.;Hong, D. H.;Lee, T. D.
    • Journal of Magnetics
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    • v.8 no.4
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    • pp.146-148
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    • 2003
  • Multilayered films of Co/Pd have been studied as a candidate material for a high density perpendicular recording medium due to higher anisotropy energy. However, high exchange coupling among grains results in large transition noise. To reduce the exchange coupling and grain size, addition of 3rd elements and physical separation of grains have been attempted. In the present paper, effects of sputtering pressure, Co sublayer thickness and Pd underlayer thickness on magnetic properties and microstructures were studied. It was found that by increasing sputtering pressure from 5 mTorr to 25 mTorr, Ms decreased to one half and coercivity increased more than 5000 Oe. The increase of the coercivity is associated with physical separation of grains by high pressure sputtering. Ms per volume of Co for Co/Pd multilayered film deposited at 25 mTorr shows continuous decrease with increasing Co sublayer thickness. This was related to void formation and intermixing of Co/Pd interface. Also, effect of Pd underlayer thickness on magnetic properties will be discussed.

Microstructures and Electrical Properties of PSN-PZT Ceramics for Piezoelectric Speaker (압전 스피커 응용을 위한 PSN-PZT계 세라믹스의 미세구조 분석 및 전기적 특성 평가)

  • Kim, Sung-Jin;Kweon, Soon-Yong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.32 no.2
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    • pp.110-115
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    • 2019
  • $Pb(Sb_{0.5}Nb_{0.5})_x(Zr_{0.51}Ti_{0.49})_{1-x}O_3$ (abbreviation: PSN-PZT) ceramics were synthesized, using conventional bulk ceramic processing technology, with various PSN doping contents. The maximum density of PSN-PZT was 97% of the theoretical density in the samples sintered at $1,250^{\circ}C$. The maximum values of the piezoelectric properties achieved using the conventional processes were: $k_p$ of 0.625, $d_{33}$ of 531 pC/N, and $g_{33}$ of $33mV{\cdot}m/N$. Finally, we fabricated a piezo-speaker with the optimized PSN-PZT ceramics. The SPL of the speaker was measured at a distance of 1 m, with a driving voltage of $40V_{rms}$ in the frequency range of ~300 Hz to 9 kHz. The measured $SPL_{max}$ was at a very high level (95 dB), which was superior in quality in comparison with those of other commercial products.

Phage Assembly Using APTES-Conjugation of Major Coat p8 Protein for Possible Scaffolds

  • Kim, Young Jun;Korkmaz, Nuriye;Nam, Chang Hoon
    • Interdisciplinary Bio Central
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    • v.4 no.3
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    • pp.9.1-9.7
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    • 2012
  • Filamentous phages have been in the limelight as a new type of nanomaterial. In this study, genetically and chemically modified fd phage was used to generate a biomimetic phage self-assembly product. Positively charged fd phage (p8-SSG) was engineered by conjugating 3-aminopropyltriethoxysilane (APTES) to hydroxyl groups of two serine amino acid residues introduced at the N-terminus of major coat protein, p8. In particular, formation of a phage network was controlled by changing mixed ratios between wild type fd phage and APTES conjugated fd-SSG phage. Assembled phages showed unique bundle and network like structures. The bacteriophage based self-assembly approach illustrated in this study might contribute to the design of three dimensional microporous structures. In this work, we demonstrated that the positively charged APTES conjugated fd-SSG phages can assemble into microstructures when they are exposed to negatively charged wild-type fd phages through electrostatic interaction. In summary, since we can control the phage self-assembly process in order to obtain bundle or network like structures and since they can be functionalized by means of chemical or genetic modifications, bacteriophages are good candidates for use as bio-compatible scaffolds. Such new type of phage-based artificial 3D architectures can be applied in tuning of cellular structures and functions for tissue engineering studies.

Microstructures and Electrical Conducting Properties of $Gd_24$O_3$-$Y_2$$O_3$-$CeO_2$Solid Electrolyte ($Gd_24$O_3$-$Y_2$$O_3$-$CeO_2$계 고체 전해질의 미세구조 및 전기전도 특성)

  • 장복기;신동선;임용무
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.12 no.1
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    • pp.44-49
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    • 1999
  • In this study, microstructure and electrical conductivity of {(G $d_2$ $O_3$)$_{0.75}$( $Y_2$ $O_3$)$_{0.25}$}$_{x}$ (Ce $O_2$)$_{1-x}$ (0.01$\leq$x$\leq$0.25) was investigated as a function of composition x. GYO addition(x) increased the bulk density and G $d_2$ $O_3$ was found to be monoclinic at x>0.15. From the change of the lattice parameter with the addition(x), GYO solution limit for ceria was exceeded in the range of x=0.05 to 0.09. Thermal expansion coefficient(15~17$\times$10$^{-6}$ $^{\circ}C$) of GYC samples at x=0.01 to 0.07 was higher in value than that of 8YSZ(10.8$\times$10$^{-6}$ $^{\circ}C$). The electrical conductivity of GYC samples at x=0.05 showed the maximum(0.01S/cm) in value at 1073K which was 2 times higher than that of 8YSZ. The activation energy for the electrical conduction was determined to be 0.60eV in the temperature range of 1073K.3K..3K.

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Effect of CuO Additions on Microstructures and Piezoelectric Properties of the 0.4Pb$(Mg_{1/3}Nb_{2/3})O_3-0.25PbZrO_3-0.35PbTiO_3$ Ceramics (CuO 첨가에 따른 0.4Pb$(Mg_{1/3}Nb_{2/3})O_3-0.25PbZrO_3-0.35PbTiO_3$ 세라믹스의 압전특성과 미세조직의 변화)

  • Jeon, So-Hyun;Kim, Min-Soo;Jeong, Soon-Jong;Kim, In-Sung;Song, Jae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.194-194
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    • 2008
  • Lead oxide based ceramics, represented by PZT, are the most widely used materials for piezoelectric actuators, sensors, and transducers due to their excellent piezoelectric properties. In particular, high-performance multilayered piezoelectric ceramics for advanced electronic components have drawn great attention. In order to develop piezoelectric ceramics capable of being sintered at low temperature for multilayer piezoelectric device applications, the effect of CuO additions on the microstructures and electromechanical properties of the 0.4Pb$(Mg_{1/3}Nb_{2/3})O_3-0.25PbZrO_3-0.35PbTiO_3$ ceramics was investigated. The samples with CuO addition were synthesized by ordinary sintering technique. X-ray diffractions indicated that all samples formed a single phase perovskite structure. The addition of CuO improved the sinterability of the samples and caused an increase in the density and grain size at low temperature. The optimum sintering temperature was lowered by CuO additions. Excellent piezoelectric and electromechanical responses, $d_{33}$ ~ 663 pC/N, $k_p$ ~ 0.72, were obtained for the samples of high density with 0.1 wt% CuO addition sintered at $1050^{\circ}C$ for 4 h in air. These results show that the piezoelectric properties of PMNZT ceramics can be improved by controlling the microstructure and this system is potentially a good candidate as multilayer piezoelectric device for a wide range of electro-mechanical transducer applications.

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Improvement of Bonding Strength Uniformity in Silicon-on-glass Process by Anchor Design (Silicon-on-glass 공정에서 접합력 균일도 향상을 위한 고정단 설계)

  • Park, Usung;An, Jun Eon;Yoon, Sungjin
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.41 no.6
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    • pp.423-427
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    • 2017
  • In this paper, an anchor design that improves bonding strength uniformity in the silicon-on-glass (SOG) process is presented. The SOG process is widely used in conjunction with electrode-patterned glass substrates as a standard fabrication process for forming high-aspect-ratio movable silicon microstructures in various types of sensors, including inertial and resonant sensors. In the proposed anchor design, a trench separates the silicon-bonded area and the electrode contact area to prevent irregular bonding caused by the protrusion of the electrode layer beyond the glass surface. This technique can be conveniently adopted to almost all devices fabricated by the SOG process without the necessity of additional processes.

Piezoelectric Properties and Microstructures of $Li_2O$ excess $(Na_{0.47}K_{0.47}Li_{0.06})NbO_3$ Ceramics ($Li_2O$ 첨가에 따른 $(Na_{0.47}K_{0.47}Li_{0.06})NbO_3$ 세라믹스의 압전특성과 미세조직의 변화)

  • Kim, Min-Soo;Jeon, So-Hyun;Park, Jeong-Joo;Jeong, Soon-Jong;Min, Bok-Ki;Song, Jae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.256-256
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    • 2007
  • As a candidate for lead-free piezoelectric materials, dense ($(Na_{0.47}K_{0.47}Li_{0.06})NbO_3$ (LNKN6) ceramics were developed by conventional sintering process. Sintering temperature was lowered by adding $Li_2O$ as a sintering aid. Abnormal grain growth in the LNKN6 ceramics was observed with varying $Li_2O$ content. The electrical properties of LNKN6 ceramics were investigated as a function of $Li_2O$ concentration. When the sample sintered at $1000^{\circ}C$ for 4h with the addition of 1 mol% $Li_2O$, electromechanical coupling factor ($k_p$) and piezoelectric coefficient ($d_{33}$) of LNKN6 ceramics were found to reach the highest values of 0.40 and 184 pC/N, respectively.

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Analyses of Creep Properties of Ni-base Superalloy Powders as Cooling Rate after Solid Solution Heat Treatment (니켈기 초내열합금 분말의 고용화 열처리 후 냉각속도에 따른 크리프특성 분석)

  • Jun, Chan;Lee, Youngseon;Bae, Byeong Beom;Kim, Hong-Kyu;Hong, Seong Suk;Kim, Donghoon;Yun, Jondo;Yoon, Eun Yoo
    • Journal of Powder Materials
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    • v.23 no.3
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    • pp.247-253
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    • 2016
  • In this study, solid solution heat treatment of consolidated nickel-based superalloy powders is carried out by hot isotactic pressing. The effects of the cooling rate of salt quenching, and air cooling on the microstructures and the mechanical properties of the specimens are analyzed. The specimen that is air cooled shows the formation of serrated grain boundaries due to their obstruction by the carbide particles. Moreover, the specimen that is salt quenched shows higher strength than the one that is air cooled due to the presence of fine and close-packed tertiary gamma prime phase. The tensile elongation at high temperatures improves due to the presence of grain boundary serrations in the specimen that is air cooled. On the contrary, the specimen that is salt quenched and consists of unserrated grain boundaries shows better creep properties than the air cooled specimen with the serrated grain boundaries, due to the negative creep phenomenon.

Influence of Vertical Centrifugal Casting (V.C.C) Conditions and Alloying Elements on Microstructures of High Speed Steel (고속도강의 미세조직에 미치는 합금원소 및 수직원심주조 조건의 영향)

  • Kim, Sug-Won;Lee, Ui-Jong;Woo, Kee-Do;Kim, Dong-Keon
    • Journal of Korea Foundry Society
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    • v.20 no.5
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    • pp.323-329
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    • 2000
  • The HSS consists of hard carbide and matrix of martensite, and so its characteristics of wear resistance, fracture resistance, and surface roughness are good. This study was undertaken to investigate the influence of Nb and V and manufacturing conditions on microstructural behaviors and characteristics in the HSS cylindrical specimens(90 $mm^{O.D.}$ ${\times}$ 60 $mm^{I.D.}$ ${\times}$ 50 $mm^H$) manufactured using VCC(Vertical Centrifugal Casting). In the specimen of Fe-2C-6Cr-1.5W-3Mo-4V alloy, the amount of MC carbide was increased and $M_7C_3$ carbide was decreased with the increase of V and Nb contents. The primary VC carbide was formed and followed by the rod-type eutectic MC carbide was formed in the cell boundary in 9%V added specimen. MC carbide was increased, and $M_7C_3$ carbide was decreased with the addition of Nb content. In the specimen containing more than 3%Nb, primary NbC carbide was formed within the cell of matrix. With increase in rpm, cell and carbides became fine, and amount of carbide $M_7C_3$ was decreased due to increase in cooling rate.

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Microstructure and Electromagnetic Characteristics of MWNT-filled Plain-Weave Glass/Epoxy Composites (다중벽 탄소나노튜브가 첨가된 평직 유리섬유/에폭시 복합재료의 미세구조 및 전자기적 특성)

  • Lee, Sang-Eui;Park, Ki-Yeon;Lee, Won-Jun;Kim, Chun-Gon;Han, Jae-Hung
    • Composites Research
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    • v.19 no.1
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    • pp.36-42
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    • 2006
  • MWNT(multi-walled carbon nanotube)-filled plain-weave glass/epoxy composites were fabricated and electromagnetic characteristics of the composites were investigated. The observation of the microstructures of the composites revealed that MWNTs are mostly distributed in matrix rich region and the interface between glass fiber yarns in warp and fill direction. The permittivity of the composites, measured in X-band (8.2-12.4 GHz) frequency range, increased with weight fraction of MWNTs and remained almost constant with frequency. The measured permittivity was used to investigate the reflection loss of radar absorbing structures (RAS) composed of MWNT-filled composites according to thickness and a RAS were constructed with 10 dB absorbing bandwidth 4.2 GHz and 3.3 mm in thickness.