• Title/Summary/Keyword: 3-D Analytical Method

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Survey of ERETIC2 NMR for quantification

  • Hong, Ran Seon;Hwang, Kyung Hwa;Kim, Suncheun;Cho, Hwang Eui;Lee, Hun Joo;Hong, Jin Tae;Moon, Dong Cheul
    • Journal of the Korean Magnetic Resonance Society
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    • v.17 no.2
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    • pp.98-104
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    • 2013
  • The ERETIC (Electronic REference To access In vivo Concentrations)2 method is a new qNMR experimental technique to measure analytes based on the signal of the reference compound without additional hardware equipment. In this study, ERETIC2 method was validated, and we sought to identify whether it would be possible to apply this method to a specific compound analysis of metabolites in plant. The $90^{\circ}$ pulse value (P1) and spin-lattice relaxation time ($T_1$) of each compound were measured for ERETIC2. The $9^1H$ of 3-(trimethylsilyl) propionic-2,2,3,3-$d_4$ acid (TSP) was used as a reference peak for ERETIC 2, and then, a suitable solvent and pulse sequence for each compound were selected. Under the NOESY-presat sequence, the relative accuracy error for quantitative analyses of primary metabolites was within the range of 5%, with the exception of glucose, which showed ${\geq}$ 55% error due to saturation. It showed excellent results for the quantification of glucose by using a $30^{\circ}$ pulse sequence, which did not suppress the water peak. In addition, the quantitative accuracy for secondary metabolites was extremely accurate, with an error ${\leq}$5% when considering the purity of the standard sample. The ERETIC2 method showed outstanding linearity, precision, and accuracy.

A Study on 3D Visualization for Color Analysis of Multimedia Data (멀티미디어 데이터의 색상분포 분석을 통한 3차원 시각화 연구)

  • Seo, Sanghyun
    • Journal of Digital Contents Society
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    • v.19 no.8
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    • pp.1463-1469
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    • 2018
  • The development of multimedia devices with built-in cameras such as smart devices and various studies using video-related multimedia data such as images and video obtained from the devices have been actively conducted. These studies deal with image data. An image can be defined as a set of color information obtained from a digital sensor called a pixel. Images contain various cognitive information such as color, lighting, objects and so on. In order to extract or process such information, it is necessary to clearly understand the composition of colors. In this paper, we introduce 3-dimensional information visualization method which can effectively express the results of image processing together with color distribution. This study visualizes the characteristics of image related multimedia data as well as the characteristics of various analytical data derived from it, so that researchers can transmit the image information more clearly and effectively.

A Study on the Load Distribution Ratio and Axial Stiffness on Existing and Reinforcing-Pile in Vertical Extension Remodeling (수직증축시 기존말뚝과 보강말뚝의 하중분담율 및 축강성 분석)

  • Jeong, Sang-Seom;Cho, Hyun-Cheol
    • Journal of the Korean Geotechnical Society
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    • v.35 no.1
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    • pp.17-30
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    • 2019
  • This study presents the application of the numerical and analytical technique to simulate the Load Distribution Ratio (LDR) and to define axial stiffness on reinforcing pile foundation ($K_{vr}$) in vertical extension remodeling structure. The main objective of this study was to investigate the LDR between existing piles and reinforcing piles. Therefore, to analyze the LDR, 3D FEM analysis was performed as variable for elastic modulus, pile end-bearing condition, raft contacts, and relative position of reinforcing pile in a group. Also, using the axial stiffness ($K_{ve}$) of existing piles, the axial stiffness of reinforcing pile was defined by 3D approximate computer-based method, YSPR (Yonsei Piled Raft). In addition $K_{vr}$ was defined by reducing the $K_{ve}$considering the degradation of the existing piles.

Preliminary study on the use of near infrared spectroscopy for determination of plasma deuterium oxide in dairy cattle

  • Purnomoadi, Agung;Nonaka, Itoko;Higuchi, Kouji;Enishi, Osamu;Amari, Masahiro;Terada, Fuminori
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.4101-4101
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    • 2001
  • Information of body composition (fat and protein) in living animal is important to determine the nutrients requirement. Deuterium oxide (D2O) dilution techniques, as one of isotope dilution techniques have been useful for the prediction of body composition. However, the determination of D2O concentration is time consuming and complicated. Therefore this study was conducted to develop a new method to predict D2O concentration in plasma using near infrared spectroscopy technique (NIRS). Four dairy cows in early lactation were used. They were fed total mixed ration containing conr silage, timothy hay, and concentrates to make 17.0%CP and 14.0 MJDE/kgDM. Dosing D2O was at week 1,3 and 5 after parturition. After dosing D2O, the blood was collected from hour 0 to 72. Blood samples were then centrifuge at 3,000 rpm for 10 minutes to obtain plasma. D2O concentration was analyzed by gas chromatograph (deuterium oxide analyzable system, HK102, Shokotsusyou) after extracted from plasma by liophilization. Plasma sample was scanned by NIRS using Pacific Scientific (Neotec) model 6500 (Perstorp Analytical, Silver Spring, MD) in the range of wavelength from 1100 to 2500 nm. Calibration equation was developed using multiple linear regression. Sample from one animal (cow #550; n: 74) was used for developing the calibration while the rest three animals were used for validating the equation. The range, R and SEC of the calibration set samples were 135-925 ppm, 0.93 and 48.1 ppm, respectively. Validation of the calibration equation for three individual cows was done and the average of NIR predicted value of D2O at each collection time from three weeks injection showed a high correlation. The range, r and 53 of plasma from cow #474 were 322-840 ppm,0.93 and 53.1; cow #478 were 146-951 ppm,0.95 and 39.8; cow #942 were 313-885 ppm,0.95 and 37.2, respectively. Judgement of accuracy based on ratio of standard deviation and standard error in validation set samples (RPD) for cow #474, #478 and #942 were 2.2,4.3 and 3.4, respectively. The error in application due to the variation between individual was considered smaller than the bias from collection period, however, this prediction can be overcome with correction of standard zero-minute concentration of blood. The results of this preliminary study on the use of NIRS for determination of D2O in plasma showed very promising as shown by a convenient and satisfy accuracy. Further study on various physiological stage of animal should be done.

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Investigation of the vibration of lattice composite conical shells formed by geodesic helical ribs

  • Nezamoleslami, Reza;Khadem, Siamak E.
    • Steel and Composite Structures
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    • v.24 no.2
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    • pp.249-264
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    • 2017
  • In this paper free linear vibration of lattice composite conical shells will be investigated. Lattice composite conical shell consists of composite helical ribs and thin outer skin. A smeared method is employed to obtain the variable coefficients of stiffness of conical shell. The ribs are modeled as a beam and in addition to the axial loads, endure shear loads and bending moments. Therefore, theoretical formulations are based on first-order shear deformation theory of shell. For verification of the obtained results, comparison is made with those available in open literature. Also, using FEM software the 3D finite element model of composite lattice conical shell is built and analyzed. Comparing results of analytical and numerical analyses show a good agreement between them. Some special cases as variation of geometric parameters of lattice part, effect of the boundary conditions and influence of the circumferential wave numbers on the natural frequencies of the conical shell are studied. It is concluded, when mass and the geometrical ratio of the composite lattice conical shell do not change, increment the semi vertex angle of cone leads to increase the natural frequencies. Moreover for shell thicknesses greater than a specific value, the presence of the lattice structure has not significant effect on the natural frequencies. The obtained results have novelty and can be used for further and future researches.

Simulation and Modeling of Polyethylene/Clay Nanocomposite for Dielectric Application

  • Zazoum, Bouchaib;David, Eric;Ngo, Anh Dung
    • Transactions on Electrical and Electronic Materials
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    • v.15 no.4
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    • pp.175-181
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    • 2014
  • In this paper, the simulation and modeling of a polyethylene/clay nanocomposite were undertaken to predict the nanocomposite's dielectric behavior and to help design a nanocomposite material with optimum electrical properties for electrotechnical or electronic applications. A 3-D simulation model using the finite elements method was employed in order to study the effective permittivity and electric field distribution of two-phase nanocomposite materials for ordered and random distributions of inclusions in a low-loss host matrix such as polyethylene. The influence of the dispersion of reinforcing particles, and of the permittivity and radius of the inclusions, was analysed. The simulation results were compared with alternative, known theoretical solutions obtained from classical models, and were found to be in good agreement. The numerical results also indicate that for fixed volume fractions of nanoparticles the effective permittivity of the mixture, for ordered and random distributions, does not vary with the degree of dispersion. The variation of the effective permittivity with the particle radius is shown, using numerical data, to agree with the analytical modules.

Lateral-torsional buckling of prismatic and tapered thin-walled open beams: assessing the influence of pre-buckling deflections

  • Andrade, A.;Camotim, D.
    • Steel and Composite Structures
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    • v.4 no.4
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    • pp.281-301
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    • 2004
  • The paper begins by presenting a unified variational approach to the lateral-torsional buckling (LTB) analysis of doubly symmetric prismatic and tapered thin-walled beams with open cross-sections, which accounts for the influence of the pre-buckling deflections. This approach (i) extends the kinematical assumptions usually adopted for prismatic beams, (ii) consistently uses shell membrane theory in general coordinates and (iii) adopts Trefftz's criterion to perform the bifurcation analysis. The proposed formulation is then applied to investigate the influence of the pre-buckling deflections on the LTB behaviour of prismatic and web-tapered I-section simply supported beams and cantilevers. After establishing an interesting analytical result, valid for prismatic members with shear centre loading, several elastic critical moments/loads are presented, discussed and, when possible, also compared with values reported in the literature. These numerical results, which are obtained by means of the Rayleigh-Ritz method, (i) highlight the qualitative differences existing between the LTB behaviours of simply supported beams and cantilevers and (ii) illustrate how the influence of the pre-buckling deflections on LTB is affected by a number of factors, namely ($ii_1$) the minor-to-major inertia ratio, ($ii_2$) the beam length, ($ii_3$) the location of the load point of application and ($ii_4$) the bending moment diagram shape.

Static analysis of non-uniform heterogeneous circular plate with porous material resting on a gradient hybrid foundation involving friction force

  • Rad, A. Behravan;Farzan-Rad, M.R.;Majd, K. Mohammadi
    • Structural Engineering and Mechanics
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    • v.64 no.5
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    • pp.591-610
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    • 2017
  • This paper is concerned with the static analysis of variable thickness of two directional functionally graded porous materials (FGPM) circular plate resting on a gradient hybrid foundation (Horvath-Colasanti type) with friction force and subjected to compound mechanical loads (e.g., transverse, in-plane shear traction and concentrated force at the center of the plate).The governing state equations are derived in terms of displacements based on the 3D theory of elasticity, assuming the elastic coefficients of the plate material except the Poisson's ratio varying continuously throughout the thickness and radial directions according to an exponential function. These equations are solved semi-analytically by employing the state space method (SSM) and one-dimensional differential quadrature (DQ) rule to obtain the displacements and stress components of the FGPM plate. The effect of concentrated force at the center of the plate is approximated with the shear force, uniformly distributed over the inner boundary of a FGPM annular plate. In addition to verification study and convergence analysis, numerical results are displayed to show the effect of material heterogeneity indices, foundation stiffness coefficients, foundation gradient indices, loads ratio, thickness to radius ratio, compressibility, porosity and friction coefficient of the foundation on the static behavior of the plate. Finally, the responses of FG and FG porous material circular plates to compound mechanical loads are compared.

NEW SPECTROSCOPIC METHODS FOR THE SIMULTANEOUS ESTIMATION OF FUNDAMENTAL ATMOSPHERIC PARAMETERS USING THE LINE DEPTH RATIOUS

  • Kim, Chul-Hee;Moon, B.K.;Lee, I.H.
    • Journal of The Korean Astronomical Society
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    • v.45 no.2
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    • pp.25-29
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    • 2012
  • New methods are developed to estimate the effective temperature (Te), surface gravity (log g), and metallicity ([A/H]) simultaneously with the spectral line depth ratios. Using the model atmosphere grids, depth values are calculated for the wavelength range of $4000{\AA}-5600{\AA}$ for various temperatures, gravities, and metallicities. All possible different combinations of line depth ratios for different pairs of ratios are investigated. A graphical 3D figure is produced with X, Y, and Z axes corresponding to Te, log g, and [A/H], respectively. By reading a cross point of two curves plotted by a connection of three parameters obtained from spectral line depth ratio pairs on each of the three projected planes, Te, log g, and [A/H] are determined simultaneously. In addition, an analytical method is devised based on the similar algorithm developed for the graphical method. Our methods were applied to estimate the fundamental atmospheric parameters of the Sun and Arcturus.

The Calculation of Inductance to verify the Parameters in Interior Permanent Magnet Motor (매입형 영구자석 전동기의 파라미터 검증을 위한 인덕턴스 산정)

  • Lee, Suk-Hee;Lee, Sang-Ho;Bahn, Ji-Hyoung;Hong, Jung-Pyo
    • Proceedings of the KIEE Conference
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    • 2006.07b
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    • pp.783-784
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    • 2006
  • In case of a difference exist between the experimental value and estimated value of back-emf, there can be a difference of turn number or residual flux density of permanent maget of the motor. In order to presume the turn number, the average length for each coil is used to calculate the resistance. However in producing the motor, doc to the tension of coil, the outer diameter of coil becomes smaller, and then the resistance estimated by average length for each coil is not correct. Therefore in this paper, through the comparison of experiment value and estimated value of inductance, a method of presuming the turn number and PM's residual flux density of an IPM motor is presented. The inductance of IPM motor changes with the rotor position, therefore the rotor part is taken out and then the inductance in open circuit condition is measured. In the analytical calculation, 3D FEM(Finite Element Method) is used, which can consider the leakage flux of end turns in frinzing effect.

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