• Journal of the Korean Chemical Society
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• v.37 no.6
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• pp.612-617
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• 1993

Some vanadium(III) complexes have been prepared from the reaction of VC$l_3$ with N, P, O-donating ligands and characterized by elemental analysis, $^1$H-NMR infrared and UV-Visible spectroscopy. 3,5-Lutidine, 1,2-phenylenediamine, 8-hydroxyquinoline, 9,10-phenanthrenequinone, triphenylphosphine, 1,2-bis(diphenylphosphino)ethane, 1,3-bis(diphenylphosphino)propane and 1,1'-bis(diphenylphosphino)ferrocene were chosen as coordinating ligands. Stretching frequency ${\nu}g$(V-Cl) of complexes appears) at 298∼367 cm-1, which show octahedral geometries. Stretching frequency of ${\nu}g$(V-X) (X = N, P, O) indicates that ligands are coordinated to vanadium(III). Stretching frequency ${\nu}g(C{\equiv}N)$ of acetonitrile in these complexes are characteristically shifted to about 70 c$m^{-1}$ higher compared with that of a free ligand (2260 c$m^{-1}$). Bending frequency of $\delta(C{\equiv}N)$ is also shifted to about 60 c$m^{-1}$ higher compared with that of a free ligand (377 c$m^{-1}$). Finally each vanadium(III) complex showed the following formulation; [VC$l_3$(L)$_2$MeCN] or [VC$l_3$(L-L)MeCN].

• Journal of KSNVE
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• v.5 no.2
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• pp.257-264
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• 1995

We designed the cutter profile for symmetric screw rotor and did vibration experiment of screw rotor manufactured by the designed cutter profile. The results of this study are summarized as follows. (1) We designed the cutter profile of screw rotor (4-6)(5-6) by using numerical analysis program. (2) The maximum amplitude and variation of amplitude of 5-6 profile rotor are about 30 - 36.7% and 10 - 25% smaller than those of 4-6 profile rotor, respectively. (3) As the angular velocity of rotor changes from 100 to 300 rpm, the vibration of X, Y axis in driving shaft of 5-6 profile rotor is about 10 - 20% smaller than that of 4-6 profile rotor.

• Korean Journal of Agricultural Science
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• v.27 no.1
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• pp.48-53
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• 2000

The various errors existing in a weight measurement system in most automatic egg sorting system available in Korean poultry farms have caused a large amount of economic losses to the egg producers. The object of this study was an importance of egg measurement system by changing both the number and the arrangements of load cells to reduce measuring errors. The results obtained were summarized as follow : 1. Four arrangements of load cells were selected as follows : layout I : Conventional one load cell method layout II : One load cell located as egg moving direction layout III : Two load cells located facing each other layout IV : Two load cells located as parallel with egg moving direction 2. The results of egg weight measurement according to four arrangements (Layout I, II, III, IV) showed that the average errors were 1.1218g, 0.5953g, 0.7786g, 0.2793g respectively. This indicated that the Layout IV (measuring by 2 load cells located parallel with the egg moving direction) caused the lowest average error and the best in precision. 3. The average vibration of axis X, y, Z were resulted as $5.1937{\times}10^{-3}G$, $9.3604{\times}10^{-3}G$, and $16.8657{\times}10^{-3}G$ respectively when sorting large sized egg. This indicated that the vibration of axis-Z was relatively higher than those of axis-X, and axis-Y.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2004.05a
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• pp.125-130
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• 2004

The vibration and buckling characteristics of the capsule for fuel irradiation test are studied. The natural frequencies of the capsule in air and under water are obtained by modal testing and finite element(FE) analysis using ANSYS program, and accelerations with flow are measured to estimate the compatibility with the operation requirement of the HANARO reactor. The experimental fundamental frequency of the capsule in the x and z direction is 8.5Hz and 8.75Hz in air, and 7.5Hz and 7.75Hz under water, respectively. The maximum amplitude of accelerations under the normal operating condition is measured as 11.0m/s$^2$ that is within the allowable vibrational limit(18.99m/s$^2$) of the reactor structure. Also, the maximum displacement at 100% flow is calculated as 0.13mm which is not interference with other nearby structures. FE analysis results show that the natural frequencies are found to be similar to those of the modal testing when three supporting parts are considered as simply supported conditions. From the buckling analysis, when the loading tool is applied, the critical buckling load of the capsule is 233N.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.14 no.8
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• pp.741-748
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• 2004

The vibration and buckling characteristics of the capsule for fuel irradiation test are studied. The natural frequencies of the capsule in air and under water are obtained by modal testing and finite element (FE) analysis using ANSYS program, and accelerations with flow are measured to estimate the compatibility with the operation requirement of the HANARO reactor. The experimental fundamental frequencies of the capsule in the x and z direction are 8.5 Hz and 8.75 Hz in air, and 7.5 Hz and 7.75 Hz under water, respectively. The maximum amplitude of accelerations under the normal operating condition is measured as 11.0 m/s$^2$ that is within the allowable vibrational limit(18.99 m/s$^2$) of the reactor structure. Also, the maximum displacement at 100％ flow is calculated as 0.13 mm which is not interference with other nearby structures. FE analysis results show that the natural frequencies are found to be similar to those of the modal testing when three supporting parts are considered as simply supported conditions. From the buckling analysis, when the loading tool is applied, the critical buckling load of the capsule is 233 N.

• Journal of KSNVE
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• v.7 no.1
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• pp.43-53
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• 1997

This paper investigated the practical use for measuring the structural intensity (power flow per width of cross section) in a uniform semi-infinite beam in flexural vibration. The structural intensity is obtained as a vector at a measurement point, One-dimensional structural intensity can be obtained from 4-point cross spectral measurement, or 2-point measurement on the assumption of far field. The measurement errors due to finite difference approximation and phase mismatch of accelerometers are examined. For precise measurements, it would be better to make the value of k$\delta$(wave number x space between accelerometers) between 0.5 and 1.0. Formulation of the relation between bending waves in structures and structural intensity makes it possible to separate the wave components by which one can get a state of the vibration field. Experimental results are obtained from 2- and 4-point measurement performed at 200mm (near field) and 400mm (far field) apart from excitation point in random excitation. the results are compared with the theoretical values and measured values of input power spectrum in order to verify the accuracy of structural intensity method, 2-point method is suggested as the practical structural intensity method.

• Journal of the Microelectronics and Packaging Society
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• v.7 no.4
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• pp.1-5
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• 2000

Properties of AC applied hot pressed ($Pb_{1-x}Sn_{x}$) Te thermoelectrics were investigated. Mechanical alloying process used to produce alloyed powder to reduce the inhomogeneity and to avoid vaporization of constituents. It showed an increase in the mechanical alloying time with increasing of Sn contents in ($Pb_{1-x}Sn_{x}$)Te. ($Pb_{1-x}Sn_{x}$)Te were sintered at 873 to 923K for 1-4 minutes, under 150 kgf/$\textrm{cm}^2$ by AC applied hot pressng method. The short sintering time of AC applied hot pressing process could reduce the vaporization of Te. The density of ($Pb_{1-x}Sn_{x}$) Te was more dependent on the sintering temperature than the sintering time. The p-n transition was observed at x=0.1 but only p type conduction behavior was observed at more than 20 mol% of Sn compositions. The maximum value of Seebeck coefficient is 250 $\mu$V/K for x=0.2 at 500K. As the amount of Sn increases, the peak value of Seebeck coefficient drops and shifts to higher temperature and the peak value of electrical conductivity decreased with increasing temperature.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2007.05a
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• pp.983-986
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• 2007

In this paper, we addressed the IEEE 1451.x that can organize a sensor network for efficient measurement system. IEEE 1451 provides standard interface, specification and Object model for example Network Capable Application Processor(NCAP), Transducer Electronic Data Sheet(TEDS), Smart Transducer Interface Module (STIM) and so on. Especially IEEE 1451.2 defines the TEDS Formats and STIM. The TEDS makes transducer to be used independently from device. NCAP makes the component of measurement system to be handled as an object. Therefore each function block constructs system by using Add-on. IEEE 1451.x can be expend the system with Add-on and Plug-and-Play by using smart sensor and connected with current network. We expect that this method can provide the efficiency and convenience when using the measurement system.

• Journal of KSNVE
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• v.10 no.2
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• pp.299-305
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• 2000

In this study, the characteristics of transmitted vibration on hand-arm system are examined when operating electric hand tools. Also through the correlation analysis between anthroponetric data and transmitted vibration, and comparison study with appropriate amount of work done based on the ISO criteriaa, the basic data for the ergonomic work design can be presented. The types of electric tools and works for the experiment are drill (general type and impact type), grinder, wire brush and steel to analyze the characteristics of transmitted vibrations, the amount of transmitted vibrations in X, Y and Z direction at tool(T), hand(H), wrist(W), and the joint between foream and upper arm(A) were measured at the frequency range of 6.3∼1000[HZ]. Also, the limit of human exposure to vibration, and the response of frequency were conducted.

• Journal of KSNVE
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• v.10 no.2
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• pp.269-279
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• 2000

This paper deals with the development of biomechanical model on a seat with backrest support in the vertical direction. Four kinds of biomechanical models are discussed to depict human motion. One DOF model mainly describes z-axis motion of hip, two and three DOF models describe z-axis of hip and head, and while nine DOF model suggested in this study represents more motion than the otehr model. Three kinds of experiments were executed to validate these models. The first one was to measure the acceleration of the floor and hip surface in z-axis, the back surface in x-axis, and the head in z-axis under exciter. From this measurement, the transmissiblities of each subject were obtained. The second one was the measurement of the joint position by the device having pointer and the measurement of contact position between the human body and the seat by body pressure distribution. The third one was the measurement of the seat and back cushion by dummy. The biomechanical model parameters were obtained by matching the simulated to the experimental transmissiblities at the hip, back, and head.