• Title/Summary/Keyword: 2-Ethyl hexanol process

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Concentration of 2-Ethyl Hexanol Using an Energy-Efficient Distillation Column (에너지 절약형 증류탑을 이용한 2-에틸헥산올의 농축)

  • Kim, Dae-Hwan;Park, Jung-Woo;Kim, Young-Han
    • Clean Technology
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    • v.16 no.1
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    • pp.59-63
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    • 2010
  • The concentration process of 2-ethyl hexanol used for the intermediate material in the production of plasticizer is examined for the energy conservation of energy-efficient distillation system instead of the conventional two column system through numerical simulation. Some 41 % of energy conservation is expected from the proposed system, and its conservation principle is explained with column profiles. In addition, not only the operating cost but also investment cost can be reduced for the additional benefit of the column application when the thermally coupled distillation is implemented.

Volatile Flavor Components in Mash of Takju prepared by using Aspergillus oryzae Nuruks. (Aspergillus oryzae 누룩으로 담금한 탁주 술덧의 발효 과정 중 휘발성 향기성분)

  • Lee, Taik-Soo;Han, Eun-Hey
    • Korean Journal of Food Science and Technology
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    • v.33 no.3
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    • pp.366-372
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    • 2001
  • Volatile flavor components in the mash of Takjus prepared by using Aspergillus oryzae nuruk were identified by using Gas Chromatography and Gas Chromatography-Mass Spectrometry. Twenty-four esters, 21 alcohols, 10 acids, 9 aldehydes and 4 others were found in the mash of Takju. Thirty six components including 13 esters and 12 alcohols were detected in the beginning of fermentation. Twenty nine components were more detected after second day of fermentation and 68 components were detected after 12 days of fermentation. Thirty five flavor components including 12 alcohols such as ethanol, 2-methyl-1-propanol, 3-methyl-1-butanol and benzeneethanol, 13 esters such as ethyl acetate, ethyl caprylate, ethyl butyrate and isoamyl acetate, 4 aldehydes and 6 acids were usually detected in the fermentation process. Ethanol was predominantly found in the range of $79.86{\sim}89.54%$ as a major component by using relative peak area. 3-Methyl-1-butanol, ethyl caprylate and benzeneethanol were some of the major volatile components through the fermentation respectively. Peak area of 2-methyl-1-propanol, 1-hexanol, 1-dodecanol, ethyl acetate, monoethyl butanoate, acetic acid and isobutylaldehyde among the same group were higher than other components depending upon fermentation time.

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A Study on Heat and Mass Transfer Characteristics of LiBr-$H_2$O Solution with a Sufactant Flowing over a Cooled Horizontal Tube (계면활성제 첨가시 수평 냉각관 외부를 흘러내리는 LiBr수용액의 열 및 물질전달 특성에 관한 연구)

  • 김경희;설신수;이상용
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.14 no.4
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    • pp.341-349
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    • 2002
  • Heat and mass transfer characteristics of a surfactant-added LiBr-$H_2O$ solution flowing over a single horizontal tube were examined experimentally. The parameters considered were surfactant (2-ethyl-1-hexanol) concentration, solution temperature at the top of the tube and absorber pressure. Even with an amount of the surfactant below the solubility limit, heat and mass transfer performances were enhanced tremendously. The Nusselt and Sherwood numbers increased by about 70% and 340%, respectively, when 10 ppm of the surfactant was added. However, an excess amount of the surfactant in the solution did not bring a further enhancement. The absorption performance deteriorated when the non-condensable gases were extracted from the system (by a vacuum pump) since the vaporized surfactant was also extracted during the process. Therefore, it is desirable to add a sufficient amount of the surfactant (more than 10 ppm) to maintain high performance of absorption.